大叶羊蹄甲中黄酮类化合物提取方法的初步研究

采用正交试验,分别用醇提法和超声波提取大叶羊蹄甲中的黄酮类化合物,比较2种方法的提取效果及黄酮类化合物的含量,从而得到最佳的工艺方案.实验结果表明:超声提取法效果较好,其最佳条件是:固液比1∶15,乙醇体积分数为90%,超声时间15 min,超声频率为500W,提取率为14.56%.     

钻井泥浆泵泵冲流量测量系统的研制

钻井泥浆泵泵冲流量测量系统是石油钻(修)井行业中一种重要的泥浆泵冲和入口测量的测量仪表.文章介绍了泵冲流量测量系统的原理,阐述了该仪表系统的设计原理及关键技术.该系统能为钻(修)井泥浆注入量提供准确显示.便于司钻和钻(修)井监督们第一时间了解泥浆泵的工作情况和掌握井筒内泥浆的压力状态.实验证明,该系统测量精度.可靠性均很理想,值得推广应用.     

Banach空间中非扩张映射的黏性逼近方法

借助Banach空间中非扩张映射的黏性逼近方法,在范数一致Gateaux可微的Banach空间中,提出一种改进的黏性迭代算法,证明了由该黏性迭代算法生成的序列强收敛于一类非扩张映射的不动点.推广了一些文献中的研究成果.     

高强再生混凝土常规三轴受压本构曲线试验

为了研究高强再生混凝土单轴及常规三轴应力状态下的受压应力-应变全曲线特征,通过RMT - 201完成43个Φ50 mm× 100 mm圆柱体试验,分析了不同围压、不同再生粗骨料取代率对高强再生混凝土强度、峰值应变以及全曲线的影响,提出了高强再生混凝土应力-应变曲线本构方程.试验结果表明:高强再生混凝土试件破坏形态与普通...     

Film Morphology, Emulsification of Dodecyl/Carboxyl Modified Polysiloxane and Its Application Performance on Cotton Fabrics

The film morphology of dodecyl/carboxyl modified polysiioxane (RCAS) on cotton fabric or the silicon wafer was investigated and characterized by field emission scanning electron microscopy ( FESEM ),atomic force microscope ( AFM ),and Fourier transform infrared spectrometer (FTIR).Experimental results indicate that RCAS is a good film forming material on different substrates.Relatively smooth film was formed on cotton fabric surface,on which the grooves disappeared.In addition,RCAS formed a micromorphology inhomogeneous and unsmooth film on the silicon wafer.Many high or low bright peaks distributed randomly on the film surface,especially as the field was 2μm ×2 μmand the date scale was 5 nm in AFM observation.Then RCAS was emulsified with nonionic surfactant alkyl polyoxyethylene ether in order to achieve a transparent organosilicon emulsion-RCAS emulsion ( RCSE),which possessed good stability.The properties of RCSE and its application performance on cotton fabrics were investigated and characterized by transmission electron microscope (TEM),particle size analysis,and voltage test instrument.The results show that the average particle size of RCAS emulsion is 28.32 nm,while the ζ voltage is - 37.88 mV.Compared with untreatd cotton fabric,the.softness of treated fabric can be improved with RCSE to a certain extent.At the.same time,the fabric treated with RCSE acquires unique fluffy and soft handle.     

矩值法和图解法计算山区河流沉积物粒度参数的差异

在宜昌市山区小河莲沱溪采集一组以粗砂和极粗砂为优势粒度组成的沉积物样品,在筛析法进行粒度分析的基础上,用矩值法和图解法分别计算沉积物的粒度参数,并对两种方法所得的结果进行对比.两种计算方法得到的平均粒径和分选系数十分接近,基本上可以互相替代.峰态呈一定的相关性,但不可互相代替.偏态较为离散,不具有明显的相关性.分析发现...     

紫外光照射下钴钼杂多酸降解有机染料SRB

制备了不同配比的钴钼杂多酸（CoMox Heteropoly acids,CoMox）,在紫外光（λ≤387 nm）照射下,以有机染料酸性桃红（Sulforhodamine B,SRB）的光催化降解为探针反应,研究了CoMox杂多酸不同配比及用量和体系介质pH值对其降解行为的影响.结果表明,最佳配比的钴钼杂多酸为CoMo12,在pH=3.0,CoMo12用量为1.0 g/L时,对SRB降解效果最好.在紫外光照射下,CoMo12活化O2,3.5 h内SRB脱色率达到96%.通过紫外-可见吸收光谱（UV-vis absorption spectrum）,红外光谱（FTIR）和总有机碳（TOC）测定分析钴钼杂多酸对SRB的降解特性,同时采用苯甲酸荧光光度法跟踪测定降解过程中产生的活性氧化物种,表明CoMo12多酸对SRB的光催化降解过程主要涉及.OH氧化历程.     

Research on stateful public key based secure data aggregation model for wireless sensor networks

Data aggregation technology reduces traffic overhead of wireless sensor network and extends effective working time of the network,yet continued operation of wireless sensor networks increases the probability of aggregation nodes being captured and probability of aggregated data being tampered.Thus it will seriously affect the security performance of the network.For network security issues,a stateful public key based SDAM (secure data aggregation model) is proposed for wireless sensor networks (WSNs),which employs a new stateful public key encryption to provide efficient end-to-end security.Moreover,the security aggregation model will not impose any bound on the aggregation function property,so as to realize the low cost and high security level at the same time.     

Deterioration Process of the Hybrid Films during Wear Test——Polyacrylate Emulsion Modified by Silica Particles

The hybrid materials are widely used in various fields for excellent performance. However, there are few researches studying their failure process. In order to prepare the hybrid materials with better performance, the failure process needs to be well studied. Two kinds of silica/polyacrylate films are successfully prepared to study the effect of organic-inorganic interaction on performance. The average diameter of silica particles is measured to be around 342 nm by scanning electron microscope (SEM). Wear test demonstrates the hybrid film, which is obtained by grafting polyacrylate onto silica particles, possesses more excellent properties than the one filled directly with silica particles. The stronger interaction between organic and inorganic components leads to a better distribution of inorganic particles within the polymer matrix. In this work, a model is presented to illustrate the deterioration process of the hybrid films, which allows us to further understand the hybrid materials.     

金属材料点蚀缺陷的无损检测方法综述

点蚀缺陷会直接影响金属材料的使用性能与服役寿命,对其进行有效的无损检测与评估为预测疲劳寿命提供数据支撑具有重要意义。通过阐述点蚀缺陷的特点,指出了点蚀缺陷参数与疲劳性能之间的对应关系。通过介绍以漏磁、脉冲涡流和超声导波为主的点蚀缺陷无损检测基本原理,总结了这些方法用于点蚀缺陷无损检测的现状,对比分析了多种无损检测方法从理论模型、信号分析到工业应用的关键环节。通过分析点蚀缺陷检测时不同无损检测方法在信号处理方面的特殊性,指出了点蚀缺陷的可视化成像结合图像处理与信号分析是准确提取点蚀缺陷信息和定量化分析的关键基础问题,积极开展非接触式点蚀无损检测方法研究对提升检测精度与工业应用推广具有重要意义。