S-布洛芬印迹复合膜的吸附及拆分性能

以聚偏氟乙烯（PVDF）微孔滤膜为基膜,S-布洛芬为模板分子,丙烯酰胺为功能单体,乙二醇二甲基丙烯酸酯为交联剂,采用热引发表面自由基聚合的方式制备了S-布洛芬印迹复合膜,并研究了其对布洛芬外消旋体的吸附及拆分性能。结果表明,该印迹膜对S-布洛芬具有一定的特异性吸附能力,当布洛芬异构体浓度在0.1~0.5mmol/L范围内逐渐增大时,吸附量也逐渐增大,吸附选择性因子则由1.68降至1.14;该膜对布洛芬异构体具有一定的拆分能力,渗透实验进行7h,膜对R-布洛芬及S-布洛芬的渗透量分别为0.378和0.313μmol/(cm²·h),分离因子可达到1.21。     

基于多传感器的卫星容错自主导航系统

在由星敏感器、红外地平仪、雷达高度计、紫外敏感器组成的卫星多传感器容错自主导航系统中,采用容错联邦滤波算法,突出了多传感器系统信息冗余的优势,数据处理速度快,算法计算量小,具有较高的工程实用价值.仿真结果表明,该方案能够获得较高的定轨精度,当1个或多个导航子系统出现故障时,系统能够检测并隔离相应的故障子系统,同时还能利用隔离后的子系统获得局部导航最优解,从而有效提高了卫星导航系统的可靠性和精度.     

西天目山土壤线虫区系与生态的初步探讨

1987年5月由中国自然科学基金会资助,开始了“亚热带森林土壤动物区系及其在森林生态平衡中的作用”的研究工作,开选定浙江西天目山作为研究点之一。本工作在西天目山选定5个采样区。经鉴定,西天目山土壤线虫可分5目23属40种,其中有13种仅鉴定到属,并认为,土壤线虫数量的变化,主要与海拔高度、温度、土壤pH值、降水量等因素有关。     

高层框架—核心筒体减震结构模型试验

通过单层，三层结构模型的动力试验结果，表明在框架－核心筒体结构体系内安装减震器后，减震效果显著，试验与计算结果吻合较好，说明了计算理论的正确性。     

The determination of atmospheric phosphine in Ny-Ålesund

Phoshpine (PH3), a volatile and toxic gas, has been proved to commonly exist in the environment. The determination of gaseous phosphine and its emission fluxes in Ny-Ålesund is reported in this paper. Results showed that gaseous phosphine exist in Arctic atmosphere commonly and the concentration of phosphine ranged from 16.3–600.2 ng/m³, with the maximum concentration of phosphine in tundra areas and the minimum in surface air of ocean. The concentration of phosphine ranged from 65.79–1259 ng/m³ in colliery atmosphere at different altitudes and the maximum was found in the center of colliery. Emission fluxes of phosphine were different in various Arctic areas. Emission fluxes of phosphine from protected areas, with average concentration of 32.13±5.353 ng m^–2 h^–1, were higher than from other areas. And the flux of phosphine from ocean was lower.     

钢—混凝土组合梁的研究与发展

文章对钢—混凝土组合梁的研究和发展进行了分析,并介绍了有关钢—混凝土组合梁的研究方法及值得进一步研究的问题。     

1-苄基-4-甲氧羰基-4-苯胺基哌啶的微波合成研究

1-苄基-4-甲氧羰基-4-苯胺基哌啶是合成芬太尼类化合物的重要中间体,本文采用微波辐射技术,合成了1-苄基-4-甲氧羰基-4-苯胺基哌啶.利用正交实验设计法对影响收率诸因素进行了考察,确定了最佳反应条件：辐射温度为120℃、辐射时间为1.5 h、辐射功率为30 W,反应时间从常规加热反应的36 h缩短到了1.5 h,降低了反应的危险性同时,提高了反应收率.     

单模激光线性模型瞬态的随机共振

根据线性化的单模激光输出光强方程,运用计算光强的相关函数,得到光强的功率谱及信噪比的方法,计算了在δ函数形式关联的两白噪声驱动下单模激光线性模型瞬态的功率谱及信噪比,发现了瞬态的随机共振,研究了信噪比随时间的演化及到达定态的时间,分析了参数对随机共振的影响。     

东海PN断面障碍层和水团的季节变化特征及其可能联系

本文利用PN断面的高分辨率海水温-盐-深剖面测量仪(CTD)温度、盐度和密度资料进行分析,发现PN断面处的水团有明显的陆架水和黑潮水的交汇特征,且随着季节的变化PN断面处的水团特征也发生明显的变化.通过观测资料还确定了PN断面处障碍层是常年存在的而且具有显著的季节变化.采用曲线族拟合的水团分析方法,根据不同季节PN断面上陆架水和黑潮水的混合特征,证明了水团混合在障碍层形成及季节变化中的重要作用,发现障碍层的季节变化与陆架水团和黑潮水团混合的季节变化密切相关.夏季,陆架水团向外海延伸,浮置于黑潮水之上,此时障碍层深度最浅,障碍层厚度最大;秋季,黑潮水离岸最近,将黑潮水与陆架水的交汇处向西压迫至陆架内,此时几乎不存在障碍层,零星存在的障碍层深度较深,厚度是一年当中最薄的;冬季,由于黑潮水的核心相对于秋季向深海移动,使得陆架混合水也相应地向外海拓展,而且此时陆架水与黑潮水的交汇处不只在混合层内而是影响到跃层,此季节障碍层是一年当中深度最深,厚度最厚的;春季,黑潮水的核心以及两种水团的交汇处相对于冬季的位置更向深海移动,所以此时PN断面上的障碍层深度和厚度相对于冬季变化不大,只是位置东移.海面风场和净热通量场通过改变...     

Strategy for the mapping of interactive genes using bulked segregant analysis method and Mapmaker/Exp software

A qualitative trait is usually controlled by a single gene, but it may be sometimes controlled by two or even more genes. This phenomenon is called gene interaction. Rapidly searching for linked mo- lecular markers via bulked segregant analysis (BSA) and then constructing regional linkage map with Mapmaker/Exp has become a common approach to mapping single major genes. However, methods and computer programs developed for mapping single major genes cannot be simply applied to interactive genes because the genetic patterns of gene interac- tions are quite different from that of single-gene in- heritance. Up to now, experimental methods for quickly screening molecular markers linked to inter- active genes and statistical methods and corre- sponding computer softwares for simultaneously analyzing the linkage relationships of multiple mo- lecular markers to an interactive gene have not been available. To solve this problem, in this paper, we propose a strategy for mapping interactive genes using BSA and Mapmaker/Exp. We demonstrate that all interactive genes can be mapped by the 'BSA Mapmaker/Exp' strategy using F2 generation (in a few cases, F3 generation is also needed). As BSA and Mapmaker/Exp have been broadly used in gene mapping studies and are well known by many re- searchers, the strategies proposed in this paper will be useful for practical researches.