THE TRANSFER BEHAVIOUR OF SOME CATIONS AT WATER／NITROBENZENE INTERFACE BY SEMIDIFFERENTIAL CYCLIC VOLTAMMETRY

The transfer of Sr~(2+) and Ba~(2+) ion, facilitated by 18-Crown-6 present in the aqueous phase, and of succinylcholine ion at w/nb interface were investigated by semi-differential cyclic voltammetry. A good polarographic curve of succinylcholine ion dissolved in water was obtained in the system of 0.01 mol/l LiCl (w)——0.01 mol/l TBATPB (nb). The peak current is directly proportional to the concentration of SC~(2+) ion. It can be used for the determination of SC and the detection limit is 1.05×10~(-5) mol/l.The apparent D~w and D~(nb) have been estimated. The transfer of Sr~(2+) and of Ba~(2+) at the interface are facilitated by 18-Crown-6 present in the aqueous phase and the peak current is directly proportional to the concentration of 18-Crown-6 in water. This method can be used for the determination of the complexing agent and for the stability constant of the complex formed in the aqueous phase.All the experimental results are in keeping with the theoretical.     

造纸污冷凝水中挥发醇的测定

本实验用自行研制的简易气提－浓缩装置，与气相色谱仪联用，在适当的实验条件下，对造纸污冷凝水中微量低沸点挥发醇的混合物进行了有效的测定。检测下限为～１０μｇ／Ｌ，变异系数＜１０％，加标回收率＞８１％。     

格兰·泰勒棱镜两类视场角的比较研究

以格兰·泰勒棱镜为例 ,推导了沿主截面和垂直主截面两正交方向的最大视场角 ,并在常用结构角下比较了两类视场角的大小及它们随波长的变化关系 ,得知沿主截面的视场角对光路调整影响较大     

新型延缓交联体系

用氧氯化锆和柠檬酸钠反应制得一种新型的延缓交联的交联剂──柠檬酸锆。用正交设计和粘度法得到了制备柠檬酸锆的最佳条件，即：氢氯化锆与柠檬酸钠的摩尔比为２：１．ｐＨ值为７．试验结果表明，柠檬酸锆可以延缓锆对聚丙烯酰胺、瓜尔胶、羟甲基瓜尔胶、羟乙基瓜尔胶、羟丙基瓜尔胶的交联速度。交联速度随聚合物浓度、柠檬酸锆对聚合物的质量比、温度、水的矿化度的增加而增加．柠檬酸锆对ＰＡＭ通过羧基交联，对瓜尔胶通过羟基交联。     

浅析普通机床的数控改造

论述了普通机床数控改造的可行性、必要性和经济性，并对C620-1型普通机床的数控改造过程进行了较详细的总结和论述，对普通机床的数控改造具有实际的指导作用。     

21世纪党校图书馆工作面临的挑战与对策

针对21世纪党校图书馆工作面临的挑战与目前的现状，提出了适应时代新要求的党校图书馆工作管理的对策。     

应用全谱直读光谱仪测定原油中铁和钙元素的含量

提出了利用电感耦合等离子发射光谱ICP -AES法测定原油中铁、钙元素含量的方法 ,考察了雾化压力、RF功率等对被测元素分析线强度的影响 ,确定了仪器的最佳使用条件。试验表明 ,该方法简便、快速、精密度和准确度均令人满意 ,能满足实际应用的要求     

Amniotic membrane transplantation for porous sphere orbital implant exposure

Objective: This study is aimed at describing the clinical outcome of amniotic membrane transplantation for exposure of porous sphere implants. Methods: A retrospective review of consecutive cases of porous sphere orbital implant exposure was carried out. Eight cases were presented between May 2004 and Oct. 2006 (5 males, 3 females; mean age 44.5 years). Six had enucleation and two had evisceration. Exposure occurred in two primary and six secondary. Orbital implant diameter was 22 mm in seven cases and 20 mm in one case. Six patients are with hydroxyapatite and two with high-density porous polyethylene (Medpor) orbital implants. The mean time from implantation to exposure was 1.1 months (range 0.8~2 months). All patients required surgical intervention. Results: The time of follow-up ranged from 3.0 to 28.0 months (mean 16.5 months). Amniotic membrane grafting successfully closed the defect without re-exposure in all of these patients. The grafts were left bare with a mean time to conjunctiva of about 1 month (range 0.8~1.5 months). Conclusion: Exposed porous sphere implants were treated successfully with amniotic membrane graft in all of patients. The graft is easy to harvest. This technique is useful, dose not lead to prolonged socket inflammation and infection, and it is valuable application extensively.     

The Design of Behavior Management Institution Based on Special Symbols and Measure Optimizing-Taking the Design of the Institution of Controlling the Pollution Behavior of Enterprises as an Example

Taking the institution design of controlling the pollution behavior of enterprises as an example, the symbol system specialized for the design and analysis of behavior management institution is put forward, which predigests the institution design greatly and make the process of institution design much like the engineering design. The measure combination method for improving the parameters of the institution, the arithmetic for calculating the validity of the institution and the arithmetic for calculating the behavior probability of the irrational managed are also put forward, which make the design and analysis technology of behavior management institution more practical.     

浅议我国建筑垃圾产业化中存在的关键问题

阐述了我国建筑垃圾产业化的重要性与必要性,利用两个建筑垃圾产业化企业实例从正反两方面论述了我国建筑垃圾产业化中存在的关键问题是相应的法律法规和标准规范的及时制定、政府的政策导向和相关部门工作的协调、公众宣传教育的加强。