Mineral-phase evolution and sintering behavior of MO-SiO2-Al2O3-B2O3 (M=Ca,Ba) glass-ceramics by low-temperature liquid-phase sintering

In this work, network former SiO₂ and network intermediate Al₂O₃ were introduced into typical low-melting binary compositions CaO·B₂O₃, CaO·2B₂O₃, and BaO·B₂O₃ via an aqueous solid-state suspension milling route. Accordingly, multiple-phase aluminosilicate glass-ceramics were directly obtained via liquid-phase sintering at temperatures below 950℃. On the basis of liquid-phase sintering theory, mineral-phase evolutions and glass-phase formations were systematically investigated in a wide MO-SiO₂-Al₂O₃-B₂O₃ (M=Ca, Ba) composition range. The results indicate that major mineral phases of the aluminosilicate glass-ceramics are Al₂₀B₄O₃₆, CaAl₂Si₂O₈, and BaAl₂Si₂O₈ and that the glass-ceramic materials are characterized by dense microstructures and excellent dielectric properties.     

鲢鱼鱼鳞蛋白提取工艺研究

以鲢鱼鱼鳞为研究对象,研究了提取温度,提取时间,料液比对鱼鳞蛋白质提取率的影响,并进一步通过正交实验对其提取工艺进行了优化。研究结果表明:鱼鳞蛋白质提取率随着提取温度、提取时间、料液比的增加而提高。其提取的最佳条件是:提取温度90℃,提取时间6 h,料液比1:25,在此条件下鲢鱼鱼鳞蛋白质的提取率为77.41%。     

空间数据与GIS技术支撑的重庆市县域旅游竞争力研究

以第一次全国地理国情普查数据资料为基础,构建了一套融合空间数据与GIS分析技术的县域旅游竞争力评价指标体系,从旅游资源产品竞争力、市场服务竞争力、旅游保障竞争力3个方面对重庆市各区县旅游竞争力差异进行定量化分析,了解各区县旅游产业发展的优劣势.加权综合发现,各区县综合旅游竞争力划分为3类:一类包括渝中、九龙坡、渝北等12个区县;二类包括大足、万州、巴南等9个区县;三类包括开州、丰都、铜梁等17个区县.最后提出重庆市县域旅游竞争力提升策略.     

Effect of particle size distribution on the microstructure,texture,and mechanical properties of Al–Mg–Si–Cu alloy

The effect of particle size distribution on the microstructure,texture,and mechanical properties of Al–Mg–Si–Cu alloy was investigated on the basis of the mechanical properties,microstructure,and texture of the alloy.The results show that the particle size distribution influences the microstructure and the final mechanical properties but only slightly influences the recrystallization texture.After the pre-aging treatment and natural aging treatment(T4 P treatment),in contrast to the sheet with a uniform particle size distribution,the sheet with a bimodal particle size distribution of large constituent particles and small dispersoids exhibits higher strength and a somewhat lower plastic strain ratio(r) and strain hardening exponent(n).After solution treatment,the sheet with a bimodal particle size distribution of large constituent particles and small dispersoids possesses a finer and slightly elongated grain structure compared with the sheet with a uniform particle size distribution.Additionally,they possess almost identical weak recrystallization textures,and their textures are dominated by CubeND {001}310 and P {011}122 orientations.     

相干测风激光雷达带通采样方法的仿真研究

根据相干测风雷达回波信号载频高、带宽窄的特点,尤其星载相干测风雷达回波信号数千兆赫兹,采用传统采样方式对采集卡的采样率要求很高.鉴于采集卡的采样率和分辨力互相制约,提出将带通采样引入到相干测风雷达系统.本文以1.5 μm全光纤相干测风激光雷达的实测数据作为仿真输入,经Simulink滤波、带通采样,结果表明,在对探测距离影响不大的情况下,与低通采样方式相比径向风速反演结果最大相差0.5 μm/s;数据处理的时间复杂度降低,其下降值是带通采样频率与低通采样频率的比值;但信噪比会恶化,其下降值介于1~3 dB.      

高压天然气管道喷射火热辐射计算

天然气燃爆喷射火事故可能造成人员建筑严重损害,为研究大型天然气喷射火燃爆特性,使用CFD计算软件,对质量流量在5 kg/s以上,压力分别为12 MPa与6 MPa,泄漏孔径在25 mm、50 mm与100 mm时的高压天然气喷射火进行仿真,得到这六种工况下喷射火火焰尺寸、温度分布和近地热辐射强度分布曲线,并得到喷射火长度与宽度和泄漏孔直径的线性变化关系.与喷射火常用的Thornton模型对比,仿真结果计算的火焰长度基本符合,热辐射结果在泄漏中心30 m以外基本相近,两种方法都可用于估算远距离喷射火热辐射强度,为天然气设施安全设计提供参考.     

UHPLC-MS/MS法同时测定大鼠血浆中汉黄芩素、隐绿原酸和白杨素-7-O-葡萄糖醛酸苷含量

建立了UHPLC-MS/MS同时测定大鼠血浆中的汉黄芩素、隐绿原酸和白杨素-7-O-葡萄糖醛酸苷含量的方法。以芹菜苷为内标,采用ACQUITY UPLC HSS T3色谱柱(2.1 mm×100 mm, 1.8 μm),乙腈和0.1％甲酸溶液为流动相,流速为0.2 mL·min^-1。结果表明,汉黄芩素、隐绿原酸和白杨素-7-O-葡萄糖醛酸苷线性范围为1～1 000 ng·mL^-1(R2>0.99),最低定量浓度为1 ng·mL^-1,提取回收率、基质效应均符合生物样品分析要求。建立的方法灵敏、准确,可用于大鼠血浆中汉黄芩素、隐绿原酸和白杨素-7-O-葡萄糖醛酸苷的测定及其药代动力学研究。     

Effect of cold rolling process on microstructure and mechanical properties of high strength β titanium alloy thin sheets

The microstructure and mechanical properties of Ti-3.5Al-5Mo-6V-3Cr-2Sn-0.5Fe high strength titanium alloy sheets prepared by unidirectional cold rolling and two-step cross cold rolling were investigated. Results showed that the β phase grains were refined significantly by cold rolling followed by solution treatment for a short time.Compared to unidirectional cold rolling, the short time solution treatment after two-step cross rolling could significantly reduce the non-uniformity of the microstructure of the alloy sheets. After aging treatment at 550 ℃,the anisotropy of the mechanical properties still existed in the unidirectional rolled sheets, and the tensile strength was highest along the rolling direction. After solution and aging treatment, the anisotropy of the mechanical properties of the two-step cross rolling process sheet was not obvious than unidirectional cold rolling,and alloy had good strength and plasticity matching.     

The hidden disintegration of cluster heterogeneity in Fe-based glass-forming alloy melt

The evolution of liquid metal at high temperature is known much less than their solid states. This is partially due to that the message concerning clusters, metastable phase or heterogeneity in liquid is usually too slight to be traced. Here, we shed some light on the nature of structural evolution of Fe-based glass-forming alloy during overheating process by the investigation of high-temperature melt viscometry and first principles simulations. It was found that a structural transition around 1400 ℃ occurred in the melts of initial homogeneous ingot, heterogeneous ingot and amorphous ribbons jointly, and was confirmed by the results from differential scanning calorimeter(DSC), and ab initio molecular dynamics(AIMD). Combining these results with Fe-Si-B ternary phase diagram and the melting characteristics of Fe-B compounds, it is safe to conclude that the disintegration of Fe_2B type clusters to Fe_3B-type clusters leads to the observed transition. These results offer a significant reference for the preparation and property control of Fe-based amorphous alloys.     

思想政治教育融入城市型、应用型大学英语教学的有效路径探析

将思想政治教育融入大学英语教学是新形势下对大学英语教师提出的要求。城市型、应用型大学英语教师应切实认识到语言传递意识形态的本质,深刻领会思想政治教育宽泛的育人内涵。从教学大纲修订环节入手,开发编写包含思想政治教育内容的教材及讲义。大学英语教师在英语教学过程中应该采取多种教学方法,从爱国主义、人格品质、理想信念、中国文化等方面对学生进行思想政治教育,帮助他们树立社会主义核心价值观,培养出符合城市型、应用型大学培养目标的合格人才。