倍频光栅的莫尔条纹研究

用傅里叶频谱分析方法研究了横向莫尔条纹中一个光栅倍频时莫尔条纹的变化，论证了倍频光栅形成的莫尔条纹方向与等周期两RoncK光栅形成的莫尔条纹方向相同，其周期与两小周期光栅的莫尔条纹周期相同，其对比度随倍率的增加而减小的特点，呈现莫尔条纹效应的主要是等栅距光栅和二倍频光栅，介绍了产生倍频光栅的一些方法，如采用滤波的方法，消去光栅的0级衍射波，形成倍频光栅；采用球面波照明光栅，形成倍频的光栅的自成像等，举例说明了其应用，这些应用表明二倍频光栅莫尔条纹可使结构紧凑，测量简单，或使分辨率提高一倍。     

一个新混沌系统不稳定平衡点的镇定

用线性反馈控制和自适应控制方法研究了一个新的混沌系统不稳定平衡点的镇定问题.当系统参数已知时,借助系统在平衡点附近的线性化模型,利用状态线性反馈控制器可以镇定系统所有的平衡点;当参数未知时,利用自适应控制策略,可以把系统镇定到期望的不稳定平衡点.利用Lyapunov函数和LaSalle不变原理对结论给予了严格证明,并用数值仿真说明了这种方法的有效性.     

稻壳混凝土配合比设计及对工作性能的影响

以稻壳、粉煤灰、硅灰及水泥等为原料,用全计算配合比法配制稻壳混凝土,试验研究C30稻壳混凝土性能.结果表明:合理的稻壳掺量对混凝土的工作性能有一定的改善作用;适量掺入粉煤灰可以润滑集料颗粒,使混凝土具有更好的黏聚性和可塑性;硅灰和粉煤灰双掺,可以改善稻壳混凝土的黏聚性和保水性,比单掺粉煤灰效果更好.     

Crystallographic texture and earing behavior analysis for different second cold reductions of double-reduction tinplate

Since the production of tinplate with non-earing properties is difficult, especially when it is produced via the double-reduction process, the optimal degree of second cold reduction is particularly important for achieving desirable drawing properties. The evolution of texture and the earing propensity of double-reduction tinplate with different extents of second reduction were investigated in this study. Optical microscopy and scanning electron microscopy were used to observe the changes in the microstructure at various extents of reduction. Two common testing methods, X-ray diffraction (XRD) and electron backscatter diffraction, were used to investigate the texture of the specimens, which revealed the effects of deformation percentage on the final texture development and the change in the grain boundary. The earing rate was determined via earing tests involving measurement of the height of any ear. The results obtained from both XRD analyses and earing tests revealed the same ideal value for the second cold reduction on the basis of the relationship between crystallographic texture and the degree of earing.     

一种新型冷轧辊用钢的组织演变

本文以一种新型冷轧辊用钢为研究对象,借助金相显微镜和扫描电子显微镜分析了试验钢在正火、球化退火、淬火、回火过程中的组织演变,研究了碳化物的成分变化和溶解析出行为。结果显示,试验钢正火后得到马氏体+部分颗粒状和少量块状碳化物的显微组织;球化退火后的显微组织为铁素体基体上分布有大量颗粒状碳化物+少量块状碳化物,球化退火组织评定为为2~3级;淬火后的组织为马氏体+部分颗粒状和少量块状碳化物;三次回火后的组织为回火马氏体+部分颗粒状和少量块状碳化物。试验钢中的块状碳化物在整个热处理过程中始终存在,1100℃以下奥氏体化时只发生边缘部分的少量溶解。颗粒状碳化物主要为M23C6型,在热处理过程中存在明显的溶解和析出行为,1100℃以下奥氏体化时部分溶解。     

La掺杂对SrTiO_3纳米颗粒光催化性能的影响

采用高温固相反应法,向SrTiO_3中掺杂不同含量La制备光催化剂,通过XRD、SEM、UV-Vis等手段对其结构和形貌进行表征,并以罗丹明B(RhB)为模拟污染物,研究掺杂不同含量La所制催化剂对RhB的光催化降解能力的影响,从而评价所制催化剂的光催化性能。结果表明,随着掺La含量的增加,所制催化剂的晶体结构从SrTiO_3的立方晶系逐步向La_2Ti_2O_3的单斜晶系转变;La掺杂使得所制催化剂的禁带宽度减小、对紫外光的吸收阈值增大,使其光催化性能得到显著提升;掺La含量越高,所制催化剂的光催化性能越好。     

Synthesis and luminescence properties of Mn4+-dopant Ca14Zn6Ga10−xAlxO35 solid solution

Mn~(4+)-activated oxide phosphors,owing to their desirable spectral features,eco-friendly and low cost,are emerging as a new class of non-rare-earth red phosphors for warm white LEDs.However,these phosphors possess low photoluminescence quantum efficiency excited by blue chip currently.Herein we report an isostructural solid solution of Ca_(14)Zn_6Ga_(10-x)Al_xO_(35):0.15Mn~(4+)(0≤x≤10)synthesized by a traditional solidstate reaction route.The microstructure and luminescent performance of this red-emitting phosphor are investigated in detail with the aids of X-ray diffraction,diffuse reflection spectra,photoluminescence spectra/decay/QE,and temperature-dependent PL/QE measurements.Blue shift of energy peaks of~4A_2→~4T_1and~4A_2→~4T_2transition is illustrated by the Tanabe–Sugano diagram and the configurational coordinate diagram.The crystal field strength(Dq)and the Racah parameters(B and C)are carefully calculated to estimate the nephelauxetic effectβrespectively.Particularly we achieve external and internal quantum efficiencies as high as26.1%and 40.3%for Ca_(14)Zn_6Ga_6Al_4O_(35):0.15Mn~(4+)excited by 466 nm,the highest one ever reported in Mn~(4+)activated oxide phosphors under the similar condition.     

一种适用于牧区的新型太阳能系统

我国是世界上地质灾害最严重的国家之一,对人民群众的生命财产安全构成了极大的威胁.湖南省又是我国地质灾害较严重的省份之一,且水系发育,河湖地地质灾害较多.本文以澧县为例,介绍了河湖地区管涌、岸崩的发育特征、分布规律及形成因素等,并提出了相应的防治措施,最后对河湖地质灾害进行了易发性分区,取得了较好的实际效果.结果表明:文中提出的方法对河湖地区的地质灾害防治具有一定的实际指导意义.     

功能化聚丙烯酸酯乳液的表面改性及产物性能

丙烯酸酯单体添加量达到70%时,加入γ-甲基丙烯酰氧基丙基三甲氧基硅烷(KH570)与剩余单体发生共聚制备表面SiOH功能化聚丙烯酸酯乳液(PAES),产物与正硅酯乙酯(TEOS)发生溶胶-凝胶反应,制备PAES/SiO2杂合乳液.透射电镜分析显示,乳胶粒表面被一层无机硅覆盖.傅里叶变换红外光谱结果表明,KH570与丙...     

喷雾干燥-碳热还原法制备介孔球形LiFePO4/C正极材料

以聚乙二醇(PEG)为辅助模板剂和碳源,以廉价的三价铁为铁源,采用喷雾干燥-碳热还原法制备了LiFePO4/C正极材料,并对该材料的微观结构及PEG添加量、焙烧温度等对材料结构和性能的影响进行了表征和研究.结果表明:制得的LiFePO4/C材料呈介孔结构,具有漂亮的差级球状形貌、高的比表面积和容量、优异的循环性;PEG...