纳米压痕法测量纳米晶金属Cu薄膜力学性能的研究

采用纳米压痕法测量了不同厚度（180～1000nm）的纳米晶Cu膜的硬度和弹性模量.结果表明,Cu膜硬度与厚度的关系类似于Hall-Petch关系,而弹性模量与厚度无关,其值相比块体粗晶Cu下降了约20%,分析位移-载荷曲线发现晶粒尺寸越大的Cu膜其位移跳跃现象越明显.另外,对于不同厚度的Cu膜其临界剪切应力的范围约在3.02～4.07GPa之间,基本接近粗晶Cu的理论剪切强度,位错塞积依然是其塑性变形的主要机制.     

基于二阶锥规划的峰值旁瓣抑制滤波器设计

针对相位编码信号的高旁瓣问题,提出一种基于二阶锥规化的峰值旁瓣抑制滤波器设计方法。将最大增益处理损失约束下的最小峰值旁瓣滤波器设计转化为二阶锥规化问题,采用内点法进行高效求解。与已有方法相比,所提方法可以兼顾峰值旁瓣、处理增益损失和滤波器长度三方面的指标,具有设计灵活、精度高和收敛性好的优点。最后仿真和实测数据结果验证了方法的有效性。     

2-硝基丙烯热解反应机理和电子密度拓扑研究

采用密度泛函DFT（B3LYP）方法,在6311G＊＊,6—311＋＋G＊＊以及cc-pvtz基组水平上,计算了2-硝基丙烯在热解反应过程中反应物、过渡态和中间体的几何结构,研究了各反应沿极小能量途径反应分子几何构型的变化,并通过电子密度拓扑分析,讨论了反应过程中化学键断裂、生成的变化规律．结果表明,2-硝基丙烯的热解反应存在2种反应机理,一是甲基上的H原子进攻硝基上的O原子直接生成CH2CCH2和HNO2,反应位垒为199．6kJ/mol;二是O原子进攻亚甲基C原子首先生成四元环状中间体,住垒为200．3kJ／mol,环状中间体进一步发生C—C键和N-0断裂生成CH2CNO和CH2O,此反应是一个一步反应,位垒为144．7M／mol,所得环状中间体的分解反应机理与现有的AM1的研究结果不同．     

一种微弧氧化逆变电源控制系统

为满足微弧氧化工艺要求,设计出一种两级逆变式微弧氧化电源,介绍了该电源的控制系统.它以高性能DSP作为控制核心,通过调节输出两组4路PWM (脉宽调制)信号分别驱动前级功率逆变电路和后级斩波逆变电路.功率逆变电路采用有限双极性的控制方式以实现电压的调节,通过控制斩波逆变电路可以得到所需的各种电压波形.同时,该电源控制系统还具有过流、过欠压、过热、参数超限等故障诊断与保护功能.试验结果表明,该控制系统可以实现精密、稳定的电源控制,提高电源的适应能力.     

哈尔滨市城市边缘区环境灾害和环境风险探讨

通过对哈尔滨城市边缘区土地利用状况和工业布局的调查,分析出可能出现的环境灾害,对其潜在的环境风险进行定性的评价.同时针对边缘区生态环境现状提出相应的防治对策,为哈尔滨城市边缘区生态环境管理提供可行性建议.研究表明：哈尔滨城市边缘区的环境灾害类型主要有环境污染灾害、生态破坏灾害和突发性灾害,其中环境污染灾害的环境风险最大,如不及时采取相应防治措施,日后将对边缘区乃至整个城区生态环境造成较大危害.     

磁选铁尾砂选锌小型试验研究

尾矿的再利用越来越引起人们的重视,这是因为尾矿既是丰富的二次资源,又是潜在的、严重的环境污染源,再回收其中的有用成分是对日益减少的矿产资源的重要补充,利用不好又会给社会带来沉重的负担,文章阐述了磁选铁尾矿再选回收金属锌的试验研究.     

天堂鸟翼凤蝶平板模型绕流特性实验研究

蝴蝶的扑翼飞行因其相对翼展较大、扑翼频率低等特点引起广泛关注, 尤其是具有越 洋迁徙特性的蝴蝶更是备受瞩目. 本文以天堂鸟翼凤蝶这种长距离迁徙蝴蝶作为研究对象, 设计了简化模型, 应用氢气泡流动显示的方法研究该蝴蝶翼面绕流结构, 包括前缘涡、翼尖涡、翼身相交处的分离泡和马蹄形尾迹等流动结构, 并进一步讨论了各绕流结构随迎角的变化规律. 特别是在本实验条件下观测到的倒八字形前缘涡结构, 是一种新的流动现象.     

长三角16市近10年利用FDI实证分析:1998-2007

经济全球化、市场化在国家与地区之间营造了高度的竞争环境,以跨国公司为载体的资本流动成为全球化时代经济发展的重要元素;吸引外资、扩大对外开放已经成为促进地区经济发展的重要手段.长江三角洲地区自1998年以来逐渐成为外商投资的热点地区,2007年所吸收的FDI占全国的比重达到45%.基于近10年的数据分析表明,上海、苏州等利用了较多FDI的城市近10年其FDI的业绩指数在不断的下降,趋向于平均水平,而杭州、宁波、南通、嘉兴等4个城市其FDI业绩指数不断增加;从区块看,江苏省内的长三角各城市及上海,FDI业绩指数在不断的下降,而浙江省内的城市则普遍都有较人的上升;空间分布上由原来主要沿沪宁铁路沿线分布逐渐演化成沪宁铁路和沿海分布并重的局面.     

Cupric ion release and cytotoxicity for Yuangong Cu-IUDs and the release behavior of indomethacin for medicated 220 Cu-IUD

These years Yuangong copper-bearing intrauterine devices （Cu-IUDs） have been used because of less side effects in use. The corrosion of copper is essential to the success of contraception, and the release behavior of indomethacin from medicated Cu-IUD is related to its therapeutic effect. In this study, analytical methods were established to investigate the release behavior of cupric ion of three kinds of Yuangong Cu-IUDs and indomethacin of medicated Yuangong 220 Cu-IUD. Cu-IUDs were incubated in simulated uterine solution （SUS）. The concentrations of cupric ion and indomethacin were analyzed by flame atomic absorption spectrometer （FAAS） for 60 days and UV/vis -3310 spectrophotometer for 60 days, respectively. The morphology of copper after corrosion was characterized by SEM. In addition, we detected cytotoxicity by MTT of L929 mouse fibroblasts cells caused by extracts of the three Yuangong Cu-IUDs. The release behavior of cupric ion for three kinds of Yuangong Cu-IUDs was biphasic, which consisted of the initial burst release and then slow and constant release. In vitro release experiment confirmed a biphasic release of indomethacin from Yuangong 220. The copper wire of Yuangong Cu-IUDs showed uneven corrosion. The RGR value of Yuangong 365 Cu-IUD was smaller than that of medicated Yuangong 220 Cu-IUD and RGR value of medicated Yuangong 220 Cu-IUD was smaller than that of Yuangong 300 Cu-IUD. The cupric ion release and indomethacin release showed biphasic. Indomethacin increased the cupric ion release rate and might diminish the adverse effects caused by burst release of cupric ion. The toxicity grade of these three Yuangong Cu-IUDs was 4. We should canvass the adverse events of Cu-lUDs based on practical experiments, and try our best to reduce the toxicity of Cu-lUDs.     

Subtyping of type A influenza by sequencing the variable regions of HA gene specifically amplified with RT-PCR

The outbreak of a novel influenza A （H1N1） virus across the globe poses a threat to human health. It is of paramount importance to develop a rapid, reliable and inexpensive diagnostic procedure. Based on the bioinformatic information from public database, primers specific for influenza A virus surface protein haemagglutinin （HA） of several subtypes （including H1, H2, H3, H5, H7 and H9） were designed. Primer-specific PCR products were subiected to sequencing for accurately distinguishing H1 and H3 subtypes from others. This sequencing-based detection method will not only be applied to rapid detection and simultaneous subtype identification of new influenza A virus H1N1, but also provide the strategies to monitor other new types of influenza virus with explosive potential.