氯化石蜡-70的催化合成

本文介绍以PC-05为催化剂的催化合成氯化石蜡-70的新方法.着重讨论催化氯化反应机理,催化反应速度和各因素对氯化过程的影响规律,并探讨催化法的优化条件.反应条件:氯化温度50～60℃,反应时间70～90分钟,氯气流速18～20〔克/公斤·分〕,催化剂浓度0.03～0.05%(重量).研究工作表明,催化氯化法具有反应速度快,生产周期短,产品质量好和工艺先进等优点.     

向家坝水电站混凝土浇筑VR与智能进度模拟系统设计

针对向家坝水电站大坝混凝土浇筑施工工程量大、工期长、设备多、关系复杂等特点以及提高施工管理与决策科学性和效率的现实需求出发,以虚拟现实和人工智能领域的知识工程为理论基础,开发了向家坝水电站混凝土浇筑VR与智能进度模拟系统,并应用于工程实践.介绍了该系统的需求分析与实现思路、整体结构设计、系统功能设计以及系统实现的主要技术方案等研究成果,以期为相关工作提供参考和借鉴.工程实践应用表明,本系统具有形象性、智能化、综合化等优势,对于保证向家坝水电站大坝混凝土浇筑施工具有重要的实践价值.     

一种微弧氧化逆变电源控制系统

为满足微弧氧化工艺要求,设计出一种两级逆变式微弧氧化电源,介绍了该电源的控制系统.它以高性能DSP作为控制核心,通过调节输出两组4路PWM (脉宽调制)信号分别驱动前级功率逆变电路和后级斩波逆变电路.功率逆变电路采用有限双极性的控制方式以实现电压的调节,通过控制斩波逆变电路可以得到所需的各种电压波形.同时,该电源控制系统还具有过流、过欠压、过热、参数超限等故障诊断与保护功能.试验结果表明,该控制系统可以实现精密、稳定的电源控制,提高电源的适应能力.     

Cupric ion release and cytotoxicity for Yuangong Cu-IUDs and the release behavior of indomethacin for medicated 220 Cu-IUD

These years Yuangong copper-bearing intrauterine devices （Cu-IUDs） have been used because of less side effects in use. The corrosion of copper is essential to the success of contraception, and the release behavior of indomethacin from medicated Cu-IUD is related to its therapeutic effect. In this study, analytical methods were established to investigate the release behavior of cupric ion of three kinds of Yuangong Cu-IUDs and indomethacin of medicated Yuangong 220 Cu-IUD. Cu-IUDs were incubated in simulated uterine solution （SUS）. The concentrations of cupric ion and indomethacin were analyzed by flame atomic absorption spectrometer （FAAS） for 60 days and UV/vis -3310 spectrophotometer for 60 days, respectively. The morphology of copper after corrosion was characterized by SEM. In addition, we detected cytotoxicity by MTT of L929 mouse fibroblasts cells caused by extracts of the three Yuangong Cu-IUDs. The release behavior of cupric ion for three kinds of Yuangong Cu-IUDs was biphasic, which consisted of the initial burst release and then slow and constant release. In vitro release experiment confirmed a biphasic release of indomethacin from Yuangong 220. The copper wire of Yuangong Cu-IUDs showed uneven corrosion. The RGR value of Yuangong 365 Cu-IUD was smaller than that of medicated Yuangong 220 Cu-IUD and RGR value of medicated Yuangong 220 Cu-IUD was smaller than that of Yuangong 300 Cu-IUD. The cupric ion release and indomethacin release showed biphasic. Indomethacin increased the cupric ion release rate and might diminish the adverse effects caused by burst release of cupric ion. The toxicity grade of these three Yuangong Cu-IUDs was 4. We should canvass the adverse events of Cu-lUDs based on practical experiments, and try our best to reduce the toxicity of Cu-lUDs.     

一种基于区分服务的IEEE 802.11 QoS信道访问控制机制

研究表明,无线移动自组织网络具有带宽有限,信道质量不稳定,节点移动造成网络拓扑结构变化等诸多特性,这些特性严重损害了网络性能,以致在传统无线移动网络中支持具有严格QoS要求的多媒体应用面临严峻的挑战.本文提出了一种基于区分服务的信道接入控制机制,以更好地支持实时通信流.该机制对传统的IEEE 802.11DCF机制进行...     

扇叶铁线蕨总黄酮和总酚含量及其抗氧化能力分析

测定了扇叶铁线蕨(Adiantum flabellulatum L.)的总黄酮和总酚含量及其对DPPH(DPPH˙)自由基、ABTS自由基(ABTS˙)的清除力和Fe的还原力.结果表明:1)扇叶铁线蕨总黄酮质量分数在6%~8%之间,总酚质量分数在7%~14%之间,地下部分总黄酮和总酚含量高于地上部分,不同产地的扇叶铁线蕨总黄酮和总酚含量存在一定差异;2)扇叶铁线蕨提取物具有一定的Fe还原能力,以及清除DPPH自由基和ABTS自由基的能力;且ABTS自由基清除能力和Fe还原能力随总黄酮和总酚浓度的增加而增强.     

Preparation of the selenomethionine derivative of tabtoxin resistance protein

In order to obtain phase information for the X-ray diffraction of tabtoxin resistance protein (TTR) crystal using the MAD phasing method, a selenomethionine (Se-Met) derivative of TTR was overexpressed in E. coli strain M15, with pQE-30 plasmid, through IPTG induction in M9 medium containing Se-Met. The product was purified to an estimated homogeneity of greater than 95% according to SDS-PAGE, by a Ni-NTA metal affinity followed by a Mono Q anion exchange column chromatography. The successful substitution of Se-Met for methionine (Met) was confirmed by MALDI-TOF and ESI-Quadrupole Mass Spectrometry analysis. The derivative crystal was obtained using similar conditions as those for the native.     

《现代汉语词典》第5版家具类词计量研究

现代汉语家具类词颇具特色。在语音形式上,家具类词语以单音节和双音节居多,三音节相对较少,四音节很罕见。在词义架构上,单义词占优势,多义词只占少数一部分,词义架构简单。从词的内部语素构成来看,家具类词语中合成词占有绝对的优势。单纯词中以单音节单纯词为主。合成词中不存在重叠式合成词。复合式合成词中,偏正型占有主要地位,联合型次之。附加式合成词中,以"词根+词缀"型为主。《现汉》在家具类词语的诠释中较之《汉语大词典》和《现代汉语规范词典》还存在一些有待改善的地方,尤其在遵循统一性方面还有许多问题可以讨论。     

利用RBF神经网络实现聚合反应的内模控制

文中研究基于径向基(RBF)神经网络算法的内模控制策略在苯乙烯本体聚合反应相对分子质量分布控制领域的应用。利用神经网络对非线性系统的逼近能力，把内模控制推广到聚合反应过程质量指标控制这一非线性系统中。针对建模过程中存在的稳态误差，在训练数据中增加了部分静态数据，有效的提高了模型的验证精度，大大改善了由神经网络构成的内模控制器的控制精度，消除了系统余差。仿真结果证明，基于神经网络算法的内模控制策略达到了较好的控制质量。     

一种聚丙烯酰胺凝胶的快速染色方法——热考染法

在蛋白的染色方法中,目前以考马斯亮蓝染色最为常用.以樟子松的针叶为材料,以加热的考马斯亮蓝R-350染液和未经加热的考马斯亮蓝R-350染液以及未经加热的考马斯亮蓝R-250染液进行染色法方法的比较,从而证明热考染法具有蛋白点清晰、背景及对比度良好、安全、操作便捷等较优的染色特点.