柱前衍生氨基酸的色谱分析

对氨基酸的反相高效液相色谱的双荧光检测了作了介绍。采用邻苯二甲醛／巯基乙醇与９－芴基氯甲酸酯柱前衍生物,同时采用两台串联的荧光检测器对伯氨基酸和仲氨基酸进行分析;利用高半胱氨酸、高丝氨酸、正缬氨酸（ＮＶＡＬ）,硫代脯氨酸（ＴＰＲＯ）四种内标消降了系统误差。同时,由样品各组分保留时间重现性的相对误差及标准氨基酸衍生物的回收率实验来确定该方法的准确性。结果表明：此检测氨基酸方法灵敏度高,检出高且重现性     

Helmholtz Solving and Performance Optimization in Global/Regional Assimilation and Prediction System

Despite efficient parallelism in the solution of physical parameterization in the Global/Regional Assimilation and Prediction System(GRAPES), the Helmholtz equation in the dynamic core, with the increase of resolution, can hardly achieve sufficient parallelism in the solving process due to a large amount of communication and irregular access. In this paper, optimizing the Helmholtz equation solution for better performance and higher efficiency has been an urgent task. An optimization scheme for the parallel solution of the Helmholtz equation is proposed in this paper. Specifically, the geometrical multigrid optimization strategy is designed by taking advantage of the data anisotropy of grid points near the pole and the isotropy of those near memory equator in the Helmholtz equation,and the Incomplete LU(ILU) decomposition preconditioner is adopted to speed up the convergence of the improved Generalized Conjugate Residual(GCR), which effectively reduces the number of iterations and the computation time.The overall solving performance of the Helmholtz equation is improved by thread-level parallelism, vectorization, and reuse of data in the cache. The experimental results show that the proposed optimization scheme can effectively eliminate the bottleneck of the Helmholtz equation as regards the solving speed. Considering the test results on a 10-node two-way server, the solution of the Helmholtz equation, compared with the original serial version, is accelerated by 100, with one-third of iterations reduced.     

NTG对侧耳的诱变效应

采用正交试验设计以菌落直径为指标研究了NTG对侧耳8405的诱变效应.实验结果表明:当NTG的最终浓度为300μg/mL,处理前孢子先培养14h,于24℃黑暗条件下处理40min时,突变率和正变率高,变异幅度大.     

电力调度系统的数据处理与数据统计算法分析

本文对电力调度和用电管理的自动化系统，提出了电力负荷的数学模型和数据处理方法，论述了运用一元回归法进行正态分布检验的数据统计方法．     

地膜棉花土壤生态的研究

地膜栽培棉花能改善土壤的理化性状和微量生物性状,使土壤增温保墒,容重降低,孔隙度增大;加强土壤微生物活动,使总菌数增加,尤其是细菌数量的增加最为明显;有利于土壤养分的释放及腐殖的形成和积累;覆膜棉花的生长发育加快,从土壤吸收养分的数量大大地增加,产量显著地提高。     

圆薄板中心受迫非线性振动

本文通过引入载荷函数,用变分法推导出圆薄板中心受迫振动的大振幅变分方程,继之给出非线性振动方程。由于考虑了时间作用,采用摄动变分法求解,给出了稳态解;在一次近似中,得到了一个有效的求解板的基频近似值的方法。     

Catalytic oxidation of phenol in wastewater-A new application of the amorphous Fe78Si9B13 alloy

The amorphous Fe78Si9B13 alloy was used as a heterogeneous Fenton catalyst in the process of phenol degradation.The influences of main operating parameters such as reaction temperature,catalyst amount,hydrogen peroxide dosage and initial pH of solution on phenol degradation rate were investigated.The maximum mineralization of phenol was achieved at 60°C,6 g/L Fe78Si9B13, 0.31 mol/L hydrogen peroxide,with an initial pH of 2.5.More than 99%of phenol was completely removed under the optimum conditions within 10 min for a solution containing 1000 mg/L of phenol.Batch experiments for solutions containing phenol con- centrations ranging from 50 to 2000 mg/L were investigated under the above conditions and the same excellent degradation rate was obtained.The Fe78Si9B13 showed better catalytic activity than iron powder and Fe 2+ .Addition of n-butannol(hydroxyl radical scavenger)decreased the degradation rate of phenol,which demonstrates that hydroxyl radicals were mainly responsible for the removal of phenol.We demonstrated that phenol may be degraded by hydroxyl radicals decomposed by hydrogen peroxide on the surface of Fe78Si9B13 and illustrated the reaction mechanism for this process.This amorphous alloy exhibited high stability in recycling experiments and showed excellent reuse performance even after continuous operations of 8 cycles.     

氧化铁的制备及其电化学性能研究

以三氯化铁和氢氧化钠为原料,按照不同的比例混合进行反应,得到铁的无机多聚离子,并采用水热反应合成了α-Fe_2O_3．运用XRD、SEM和IR等测试手段对其进行结构表征,并研究了合成的氧化铁材料作为锂离子电池负极材料的电化学充放电性能．     

基于Strahler积分的DEM精度评价模型

提出了一种新的基于规则格网DEM的Strahler积分算法,并在此基础上提出了DEM的Strahler积分精度评价模型.该模型利用Strahler积分值表达规则格网DEM的整体误差,同时在一定程度上体现了DEM误差的空间分布,避免了常用DEM中误差模型的不唯一性以及等高线套合难以定量化的缺点.