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101.
Selective functionalization of mesoporous silica nanospheres (MSNs) is crucial for nanoengineering of MSNs.
Herein, we have combined “surface-protected etching strategy” and “cationic surfactant assisted etching
strategy” to prepare functionalized MSNs with externally attached amino groups. The externally attached NH2
groups endow the catalysts with excellent catalytic performance for nitroaldol reaction between nitromethane
and benzaldehyde. In addition, those NH2-MSNs can also be used to support gold nanoparticles, which display
very good catalytic performance for reduction of 4-nitrophenol. It can be envisioned that the synthesis protocol
developed in this work could also be extended to nanoengineered MSNs, which provides opportunities for nanoreactors
design. 相似文献
102.
The pedigrees of three sequenced rice cultivars were analyzed to show that a majority of the genetic composition of 'Nipponbare' originates from japonica cultivars while the minority originates from indica cultivars. In contrast, '93-11' is derived mainly from indica cultivars with a smaller contribution from japonica cultivars. All ancestors of 'Guang lu ai 4' appeared to be indica lines. A set of molecular markers (46 InDels and 53 SSRs) polymorphic between 'Nipponbare' and '93-11' were examined in 46 typical indica and 47 typical japonica cultivars selected from 443 accessions according to Cheng's index. All cultivars were divided into indica and japonica groups without overlapping when clustered by Cheng's index, InDels and SSRs. Much higher InDel and SSR diversity between groups than within groups implies that the marker polymorphisms between 'Nipponbare' and '93-11' represent a large proportion of inter-subspecific diversity. About 85% of indica cultivars and more than 90% of japonica cultivars were confirmed to have the same PCR banding patterns as '93-11' and 'Nipponbare', respectively. Some polymorphic loci between 'Nipponbare' and '93-11' cannot be validated in other indica and japonica cultivars, either as subspecies-specific but not predominant alleles, or alleles not specific between the two groups. It was concluded that molecular markers developed from sequence polymorphism between 'Nipponbare' and '93-11' often represent inter-subspecific diversity, although some exceptions were sensitive to either particular marker loci or particular cultivars. 相似文献
103.
变数据窗阻抗算法的频域分析方法研究 总被引:1,自引:1,他引:0
分析典型变数据窗阻抗算法的估计原理和特点 ,提出了一种适用于不同阻抗估计算法的新型频率响应计算方法 ,为不同算法的频域特性分析和比较提供了共同的基础 .该方法也可用于对算法抑制非周期分量的性能进行分析研究 相似文献
104.
卡拉帕克斯约书亚E.基廷 《科学大观园》2013,(4):30-31
美国国家航空航天局发布消息说,1977年发射的"旅行者1号"探测器已抵达太阳系边缘,这意味着"人类第一个星际使者"有望不久后首次脱离太阳系,进入星际空间。那让我们天马行空地想象一下,假如"人类星际使者"遭遇外星人怎么办?或者,更糟糕的情况,如果将并不友善的外星人引到地球,向人类发起袭击又该怎么办?人类在抵御外星人入侵时,是否已掌握合适的 相似文献
105.
Imran Sadiq Shahzad Naseem Saira Riaz S. Sajjad Hussain Muhammad Naeem Ashiq Mazhar Rana 《自然科学进展(英文版)》2018,28(4):478-482
Rare earth Dy~(3+)and divalent Mn~(2+)elements substituting W-type hexagonal ferrites Ba_(1-x)Dy_xZn_2Fe_(16-y)Mn_yO_(27)(x=0,0.02,0.06,0.1 and y=0,0.1,0.3,0.5)were prepared by sol-gel method.The thermo-gravimetric analysis(TGA)and differential scanning calorimetry(DSC)was carried out to find the temperature at which single phase can be obtained.XRD patterns indicate the presence of the single phase for all the synthesized samples with the absence of any extra peak due to unreacted material and secondary phases.The occurrence of absorption bands at low wave numbers(563 and 446 cm~(-1)),can be assigned to the stretching vibration of metal and oxygen ions in FTIR spectra,which also confirms the single hexagonal phase for prepared material.The grains are of platelet like structure,which enhances the microwave absorption properties of hexagonal ferrites.The synthesized material exhibits the minimum reflection loss of-20.9 dB at 11.8 GHz frequency,which reflects the applications of this material in super high frequency devices.The microwave conductivity of the material increases with frequency. 相似文献
106.
通过WAXS,SAXS和拉伸试验对聚丙烯-聚异丁烯共混物进行了表征,讨论了结晶条件和共混物的组成对其形态和拉伸行为的影响,与室温淬火试样相比,等温结晶试样具有较高的结晶度、较厚的晶片、较高的拉伸模量及强度、较差的韧性,PIB的存在导致iPP结晶度降低,力学性能变差。 相似文献
107.
The change in seismicity of the Garm region in Tajikistan after an irradiation of its crust with high energy electromagnetic pulses (EP) and after the Semipalatinsk nuclear explosions (NE) is considered. It’s shown that the influence of EP, as well as NE, causes a statistically significant increase in the seismic activity and speed up the seismic energy release. Two areas of anomalous increase in seismic energy after irradiation and explosions adjoined to active faults were identified within the region. Both have a complex configuration in the form of two “petals” located in different sides of those faults. In both cases, one of the “petals” appears after EP, and the second after NE. It is shown that each of these “butterflies” constitutes as a whole anomalous area in which there are high tectonic stresses. The impact of NE has also been studied before beginning and after completion of these experiments. In both cases, those anomalous areas were not observed. Moreover after those experiments were completed, on distances of 50~70 km from the EP source no high stresses areas were observed at all. Consequently, the irradiation of the crust caused their relaxation on the area of about 3 500 km2. However,judging by the appreciable rise in seismicity caused by NE on the southwestern and southeastern margins, stresses had been increasing on periphery of the irradiated area. 相似文献
108.
Cheryl E.Praeger 《科学通报》1994,39(2):187-187
设G为群,π_e(G)为G中元的阶之集.在文献中作者证明了G(?)A_n当且仅当(1)π_e(G)=π_e(A_n),(2)|G|=|A_n|.对某些交错群,如A_5,A_7,A_8可以仅用上述条件(1)加以刻划.在文献中作者证明了对所有的对称群S_n,n≥2,可用上述条件(1)和(2)加以刻划.然而,对群S_i,i=2,3,…,6均不能由条件(1)单独确定. 相似文献
109.
阿不都克热木.热木克 《科技咨询导报》2009,(35):121-121
采用问卷调查法、文献资料法、访谈法.逻辑分析法对当前新疆高校开设足球选项课教学的现状进行分析,提出了应转变足球教学的指导思想改革现有的足球教学模式、建足球健身教学体系、丰富教学内容和教学形式、完善教学考核评价制度等对策与建议,以尽快解决当前高校足球教学中的问题,使之在素质教育中发挥更大的作用。 相似文献
110.
人们改善环氧树脂基复合材料的脆性通常只改善环氧树脂基体和增强纤维间的界面,提高环氧树脂韧性的另一种常用方法是添加初始相容性良好的热塑性树脂如聚醚酰亚胺,在某一转化率(取决于体系的组成和反应温度)时体系发生相转变,体系最终的形态由相转变速率和环氧树脂反应速度所控制。本文作者研究了两种增强纤维(玻璃纤维和碳纤维)对不同环氧树脂/聚醚酰亚爱体系形态形成的影响,结果发现体系中纤维的存在不会影响基体相分离过程,但会改变体系的最终形态;形态的变化与纤维的品种关系不大;基体中不同组分的粘度是影响复合材料形态形成的关键因素。 相似文献