水杨醛缩苯磺酰腙的合成与结构表征

在乙醇溶剂中合成了水杨醛缩苯磺酰腙,用元素分析、红外光谱对其进行了表征。并用X-射线单晶衍射方法对其进行了晶体结构解析,结果表明,该化合物为单斜晶系,晶胞为P21/c,晶胞参数：a=1.04490（13）nm,b=1.15656（17）nm,c=1.08579（15）nm,V=1.3121（3）nm^3,Z=4,Mr=276.31,Dc=1.399 g/cm^3,T=298（2）K,F（000）=576,（μMo Kα）=0.252 cm-1,R=0.0434,ωR=0.1100,化合物通过分子间氢键形成了一维链状结构。     

Long-day photoperiod induced unhealthy development of chloroplasts in the photoperiod-sensitive genie male-sterile rice

By measurement of photochemical activities of chloroplasts and observation on supramolecular archi tecture of thylakoids in chloroplasts, it was found that compared with the effects of short-day photoperiod, long-day pho toperiod could induce normal development of chloroplasts in seedlings of NK58S (photoperiod-sensitive genie male-sterile rice) and NK58 (original line) which do not enter the photoperiod sensitive phase and in seedlings of NK58 just enter the photoperiod-sensitive phase. However, it could induce unhealthy development of chloroplasts in seedlings of NK58S which also just enter the photoperiod sensitive phase. This special effect of long-day photoperiod on the development of chloroplasts in NK58S is probably one of main reasons why long-day photoperiod induces rale-sterility in NK58S and normal fertility in NK58.     

高效液相色谱法和薄层—紫外法测定淫羊藿中淫羊藿甙质量分数的研究

应用HPLC法测定淫羊藿中淫羊藿甙的质量分数,测得结果显示提取淫羊藿甙的质量分数与提取液关系密切,以50％乙醇提取的质量分数为最高,对同一淫羊藿药材进行质量分数测定,HPLC法操作简单,省时,分离效果好,准确度和再现性也明显优于药典的TLC－UV法。当提取方法相同时,两种方法测得的淫羊藿甙质量分数基本一致。因此,使用HPLC法也可按照药典的质量分数限度进行药材有效成分的检测工作。     

Influence and determinative factors of ion-to-atom arrival ratio in unbalanced magnetron sputtering systems

Low pressure sputtering with a controlled ratio of ion flux to deposited atom flux at the condensing surface is one of the main directions of development of magnetron sputtering methods. Unbalanced magnetron sputtering, by producing dense secondary plasma around the substrate, provides a high ion current density. The closed-field unbalanced magnetron sputtering system (CFUBMS) has been established as a versatile technique for high-rate deposition high-quality metal, alloy, and ceramic thin films. The'key factor in the CFUBMS system is the ability to transport high ion currents to the substrate, which can enhance the formation of full dense coatings at relatively low value homologous temperature. The investigation shows that the energy of ions incidenced at the substrate and the ratio of the flux of these ions to the flux of condensing atoms are the fundamental parameters in determining the structure and properties of films produced by ion-assisted deposition processes. Increasing ion bombardment during deposition combined with increasing mobility of the condensing atoms favors the formation of a dense microstructure and a smooth surface.     

也谈《花间集序》的主旨

《花间集序》中所批评的对象是在宫体诗的艳情色彩影响下,北里娼妓口中所唱出的,产生于坊曲里巷乐工妓女之手的歌辞。"言之不文"是说其没有文采,"秀而不实"是指处于词体初期阶段,还未成熟。花间集序的主旨是通过对歌辞的历史发展过程之勾勒和描述来为花间词寻找存在的理由和价值,认为花间词要继承的是歌辞文采上的精美,音乐上的和律,功能上的娱乐性;要创新的是用相对文雅的文人词来对鄙俗的市井之词进行"雅化",这种雅化是相对的,是进士文化和市井文化结合的产物,是从单纯的"娱宾"到"娱宾"、"遣兴"并存的转变。     

双掺杂钙钛矿型复合氧化物La0.7Sr0.3Co1—xMxO3的电性能研究

以开发新型激光器阴极材料和固体氧化物燃料电池阴极材料为目的,合成一系列钙钛矿型复合氧化物La0.7Sr0.3Co1-xMxO3(M:过渡族金属元素）,并对Co位掺杂过渡族元素后样品的高温电阻率和热电动势进行研究,发现Co位掺杂不同元素显著影响材料的电导率和导电类型,并对其相应的物理机制进行探讨。     

基于非负矩阵分解最小二乘的多视角行人分类算法

针对不同视角的行人样本具有较大的类内差异性,造成多视角行人识别错误率较高的问题,提出一种基于非负矩阵分解最小二乘的多视角行人分类算法.采用非负矩阵分解的方法对多视角的行人样本图像进行子空间分解,提取基向量;引入协同表示的方法并在最小二乘约束下,对子空间进行稀疏表示获得稀疏分解系数;利用近邻子空间方法对分解系数进行分类.基于自行构建的多视角行人数据库进行对比实验,结果表明该算法的准确性和有效性优于其他方法.     

聚氨酯-橡胶组合挂胶负重轮有限元分析

提出了聚氨酯-橡胶组合挂胶负重轮设计方案,采用有限元方法建立了组合挂胶负重轮有限元模型,分析比较了聚氨酯与橡胶不同厚度比例情况下负重轮轮缘的应力、温升.分析结果表明,胎面聚氨酯挂胶厚度为胎体总挂胶厚度的20%～30%时得到的组合挂胶负重轮的设计方案最好.     

体育教学中的德育渗透

本文通过体育教学特点的分析,以及对学校体育教学中德育内容的探讨,提出在体育教学中进行体育渗透的途径与方法,为同行在体育教学中开展德育渗透理清思路,提供借鉴,只有不断的探寻渗透的方法,才能最大限度地发挥德育渗透的力度,促进学生健康的成长。     

用经济型数控系统改造普通车床的设计

用经济型数控系统改造车床的设计方案论证、数控系统的造型、进给系统设计计算在文中作了详细论述