水解法制备高吸水腈纶正交实验

对腈纶纤维的水解工艺进行研究．正交实验结果表明，实验范围内，水解时间是影响腈纶纤维吸水率的关键因素，随着时间的延长，吸水率增加；水解温度80℃时吸水率较高；NaOH浓度对水解腈纶的吸水率也产生较大的影响．温度、时间和NaOH浓度都会对纤维白度产生影响．     

利用SPOT5数据制作正射影像图并辅助更新土地利用现状图的方法

对利用SPOT5卫星数据制作正射影像图的方法进行了研究，并以扬中市为例，对使用正射影像图辅助更新土地利用基础图件的可行性进行了探讨。研究发现此方法易于掌握，辅助更新效果显著。     

Land vehicle positioning using GPS and dead reckoning

To ensure reliable land vehicle positioning, the Global Positioning System (GPS) is one of the best techniques commonly used in present-day positioning systems. However, GPS signals are not available if line of sight with the satellites is lost. In this respect, the addition of the Dead Reckoning (DR) method to complement the GPS unit would enhance the reliability of land vehicle positioning system. For implementing the DR method, the magnetic sensor and accelerometer are used for obtaining heading and velocity or distance information. Calibration of two sensors' dynamic model and DR algorithm are also introduced in this paper. The test result utilizing the GPS and DR methods is analyzed in this paper. It utilize spositioning information from GPS receiver when GPSsignal is available, otherwise DR is started to compensate GPS outage with the GPS output as the original point. The results showed that the error in east and north produced by the DR algorithm for a short time interval can be limitedwithin an acceptable range.     

In-vehicle GPS/DR navigation system development and test results in Singapore

This paper introduces the in-car navigation system prototype development and test results under the context of Singapore. In the system, integrated GPS/DR is used for continuous vehicle positioning. A digital road network map database is built for the whole Singapore. The database is designed to support map matching, route determination, and route guidance functions. The prototype system demonstrates GPS positioning of the vehicle in real-time, tracking the vehicle onto a digital map with fix updates every one or two seconds.With the map matched vehicle location on the map, voice and/or text guidance is provide to the driver. The vehicle position can also be transferred to control centre through communication data link for the purpose of fleet management.     

A carbon- and oxygen-isotope record of recent environ- mental change from Qinghai Lake, NE Tibetan Plateau

An understanding of natural climatic variability is essential for evaluating anthropogenic impacts on recent and future climate[1—3]. Due to the lack of lengthy instrumental records, such an understanding must be gained from natural archives of climate change. Palaeolimnological indicators of past lake levels may provide a sensitive record of changes in effective precipitation in closed basins. This approach is particularly relevant on the Tibetan Plateau, where instrumental records are very…     

Ni2MnGa铁磁形状记忆材料

铁磁形状记忆合金 (FSMA)是在一定温度范围马氏体相稳定同时又具铁磁性的一类特殊的形状记忆合金。Ni2MnGa铁磁形状记忆合金近年来成为呈现磁场驱动大应变的新型驱动材料 ,这些应变来自磁场诱发马氏体孪晶的重排 ,而不是磁场对奥氏体至马氏体相变的作用。孪晶变体的重排在宏观上呈现为正或切应变 ,一非化学计量比Ni2 MnGa单晶于室温加 0 .4T磁场能产生6 %的应变 ,Ni Mn Ga单晶在高至 15 0Hz的交变磁场仍可得到 2 .5 %的应变。本文阐述了与这种磁控形状记忆效应相关的孪晶界迁动的磁学和晶体学理论。马氏体相的大磁晶各向异性能使磁化沿c轴方向有利 ,穿过孪晶界c轴刚好转动 90度 ,同时 ,这个孪晶界也构成了约 90度的畴界。在各向异性的情况下 ,孪晶界的迁动仅有相邻孪晶变体的Zeeman能差驱动 ,μ0 ΔMis·Hi。磁场和外应力对应变的影响通过对一简单的自由能表达式取极小值来表示 ,自由能表达式包括Zeeman能、磁晶各向异性能和外应力以及在某些情况下需考虑的内部弹性能 ,模型的所有参数可通过应力 应变曲线和磁化曲线测量得到。铁磁形状记忆合金的磁场诱发应变可类比传统热弹性形状记忆效应 ,与更为人们所熟知的磁致伸缩现象不同。     

含苯并三氮唑的三脚架化合物及其配合物研究

合成了两个新的三脚架结构化合物；1，1，1-三（1-苯并三氮唑基甲氧甲）丙烷（A）和三[2，1-苯并三氮唑基甲氧基）乙基]胺（B），获得了它们和一些过渡金属离子形成的配合物，并用元素分析，红外光谱，摩尔电导和热分析等手段对其进行了表征。     

一类新的液晶性芳香羧酸化合物的合成

合成了一系列新的液晶性芳香羧酸化合物，化合物的结构通过元素分析、红外光谱、核磁共振波谱和质谱等方法确证。化合物5的液晶行为用示差扫描量热法(DSC)和偏光显微镜(POM)表征。发现化合物5加热至各自的熔点以上都能形成液晶态，在液晶态可以观察到向列相的丝状织构和纹影织构，随分子中末端烷氧基碳原子数增加，化合物5的熔点(Tm)和液晶态的清亮点(Ti)呈规律性变化，液晶态温度范围变宽。     

近红外光谱技术鉴别海面溢油

近红外光谱技术分析速度快、效率高、成本低、重现性好,典型的无损分析;主要用于样品类别鉴定和纯度检验.近红外光谱技术结合模式识别方法,在纯品油种类的鉴别中已得到成功应用[1,2],本实验室也初步建立了纯品油近红外谱图数据库[3],但该法在实际海面溢油样品的鉴别中应用仍甚少.     

丁烯二酸二异辛酯生产工艺的改进

通过系列的实验，研究了催化剂，反应温度和操作压力对酯化过程的影响，找出了适宜的反应条件，改进了丁烯二酯二异辛酯酯化过程的生产工艺，并扩大生产。