高效液相色谱法分析聚甘油乳酸酯的组成

建立了HPLC-ELSD法测定聚甘油乳酸酯组成的方法.采用Agilent DZORBAX NH2色谱柱（4．6 mm×250 mm）,确定了最佳色谱条件：流动相为乙腈和水（体积比为90∶10）,蒸发光散射检测器（ELSD）,流速为1．2 mL/min,柱温40℃,进样量4μL .结果表明,在0．1～0．5 mg/mL范围内线性关系良好,相关系数为0．9986,在信噪比（S/N）为3时,检出限为0．020 mg/mL .回收率为98％～102％,相对标准偏差（RSD）为1．2％～1．4％.     

萝卜播期和栽培密度对产量及性状的影响

以“泸优一号”白萝卜为试材,研究不同时期播种和不同种植群体对萝卜产量和开花的影响。结果表明:播期推迟,植株生长势减弱,肉质根产量下降;开花量减少,结实率下降。高产栽培的适宜播期为 8月下旬至 9月上旬,最佳种植规格50 cm×33 cm,每穴 2苗。萝卜不同栽培密度下的根长与横径之比、株高与开展度之比可作为根形和株型划分的依据。     

Ferroelectricity of nanocrystalline BaTiO<Subscript>3</Subscript> ceramics by first principle calculation

The vibrational modes of BaTiO₃ in different crystalline phases have been investigated by means of density functional theory pseudo potential method. The evidence of tetragonal to orthorhombic and orthorhombic to rhombohedral phase transitions present for 8 nm BaTiO₃ ceramics further demonstrates that the similar successive transitions in 8 nm BaTiO₃ ceramics from rhombohedral to orthorhombic, tetragonal and cubic transitions are as those in coarse BaTiO₃ ceramics.     

基于聚类非参数检验的动态停车需求分布特征

为了探索动态停车需求的分布特征,提出聚类非参数检验分析方法.该方法按照个体-组-类的顺序对多时段随机变量进行聚合,在各聚合阶段运用相应的非参数检验方法校核结果,在确保拟合精度的同时,采用相应的模型描述动态随机变量的分布特征.结合该方法的运用,从问题确定、数据调查、数据处理与分析以及分布特征的归纳总结等环节详细阐述了动态...     

Measurement of the Mie-Grüneisen equation of state for polyimide

An equation of state(EOS) is a thermodynamic equation describing the state of matter under a given set of physical conditions,and the Mie-Grüneisen EOS is a widely used EOS for solid materials.Polyimide is a typical complex high-molecular polymer of imide monomers which is widely used in the manufacture of parts for aerospace technology and for fabricating the inertial fusion energy shells(IFE).When a spacecraft collides with a meteoroids(or orbital debris) or the IFE shells are radiated by high power laser,the polyimide used in the equipment is in high pressure state.In order to study the safety of the spacecraft and IFE shells,the EOS of polyimide should be determined.In our research,the three key parameters of the Mie-Grüneisen EOS based on the shock adiabat for polyimide have been determined with two-stage light-gas gun experiments,i.e.the bulk speed of sound of polyimide is determined as 2.62±0.22 km/s,the linear Hugoniot slope coefficient is determined as 1.25±0.063,and the Grüneisen parameter at initial state is determined as 1.53±0.135.The Mie-Grüneisen EOS for polyimide is finally obtained,and the parameter values are proved reliable via the comparison of Grüneisen parameter value calculated from two different theoretical models using the experimental data.     

Mapping of genetic modifiers of <Emphasis Type="Italic">Plcd1</Emphasis> in scant hair mice (<Emphasis Type="Italic">snthr</Emphasis><Superscript><Emphasis Type="Italic">1Bao</Emphasis></Superscript>)

The scant hair mutant mouse (locus symbol: snthr ^1Bao ) is a recessive mutation that originated in an ethylnitrosourea chemical carcinogenesis study using the DBA/2J inbred strain. The gene responsible for the mutation was previously determined to be phospholipase C, delta 1 (Plcd1; mutant allele symbol Plcd1 ^snthr1Bao ). To map the modifiers of Plcd1, an intercross (DBA/2J-snthr ^1Bao /snthr ^1Bao × C57BL/6J+/+) was conducted. The F2 mutant progeny exhibited a variety of alopecia phenotypes; all F2 mutants (n=507) were classified into 3 groups (mild, moderate, and severe alopecia) and genotyped based on 96 microsatellites. A major QTL was identified on mouse chromosome (mChr) 15 at 12 cM with an LOD score greater than 7 (P < 0.0001). Three minor QTLs were detected on mChr 2, 5, and 7 at 40, 84 and 48 cM, respectively. The QTLs on mChr 7 and 15 were associated with minor alopecia while the QTLs on mChr 2 and 5 were associated with moderate to severe alopecia. No antagonistic or synergistic effects among or between the 4 QTLs were found. Integrating the functions of the 4 potential regulatory QTLs and mutant Plcd1 ^snthr1Bao , we found that these QTLs might contribute to variations of scant hair severity by altering the Ca²⁺ signal pathways in mouse skin.     

New testing methodology for the quantification of rock crushability: Compressive crushing value (CCV)

Crushing is a size reduction process that plays a key role in both mineral processing and crushing-screening plant design. Investigations on rock crushability have become an important issue in mining operations and the manufacture of industrial crusher equipment. The main objective of this research is to quantify the crushability of hard rocks based on their mineralogical and mechanical properties. For this purpose, the mineralogical, physical, and mechanical properties of various hard rocks were determined. A new compressive crushing value (CCV) testing methodology was proposed. The results obtained from CCV tests were compared with those from mineralogical inspections, rock strength as well as mechanical aggregate tests. Strong correlations were found between CCV and several rock and aggregate properties such as uniaxial compressive strength (UCS), the brittleness index (S₂₀), and aggregate impact value (AIV). Furthermore, the relationship between the mineralogical properties of the rocks and their CCVs were established. It is concluded that the proposed testing methodology is simple and highly repeatable and could be utilized as a pre-design tool in the design stage of the crushing process for rock quarries.     

英汉文化价值观对比

本文就英汉文化价值观在集体主义与个人主义、权力分配差距、人与自然的关系、时间取向、思维方式等差异最为悬殊的方面进行了对比。     

基于改进灰色关联投影法的无人机避让优先运行策略

针对未来混合空域中多种航空器共同执行任务而可能出现飞行避让安全问题,提出了一种基于组合赋权改进灰色关联投影法的无人机避让优先运行策略。首先,从空域管理、航空法规、风险评估等角度分析影响避让过程的因素,构建无人机避让评价指标体系;其次,利用层次分析法和粗糙熵法进行主客观赋权,由合作博弈方法构建离差和最小目标优化函数将主客观权重融合确定最终权重,克服主观赋权随意性和客观赋权过分依赖数据的弊端;随后,利用优劣解距离法(TOPSIS)与灰色关联投影法的融合算法对无人机避让对象进行综合评价,从而获取无人机优先避让运行策略;最后,将融合算法与TOPSIS算法进行对比。结果表明,较于TOPSIS法,所提融合算法获取策略与空域运行实践相符且灵敏度提高了17.08%。因此,新算法避免了单一算法的数据丢失现象,提高了获取策略的准确性,可为混合空域的无人机运行策略获取提供新思路。