Synthesis of Ta C and Ta_2C from tantalum and graphite in the laser-heated diamond anvil cell

The pressure dependence of the onset of the formation of Ta C and Ta2 C from the elements has been investigated by in situ X-ray diffraction and pyrometry.Ta C has been synthesized by the reaction of Ta and graphite at pressures between 8.6 and 14.3 GPa and at temperatures up to 2,300 K using a laser-heated diamond anvil cell. The products were characterized by X-ray diffraction. Ta and graphite begin to react around 1,100 K at ambient pressure conditions, and the reaction temperature increases with increasing pressure. A linear extrapolation of these data is consistent with recent observations of the formation of Ta C at 90 GPa and 3,600 K. We show that diffusion of carbon into tantalum significantly changes the lattice parameter of up to 2 % in the pressure range of up to19 GPa. In some experiments, Ta2 C was formed concomitantly. The experimentally determined bulk modulus of Ta2 C is B0;exp：= 286（5） GPa. Other tantalum carbide phases were not observed.     

基于中期基准面旋回变化的沉积微相精细研究——以松辽盆地扶余油田泉四段为例

 从区域沉积背景出发,以岩心和测井资料分析为基础,对松辽盆地扶余油田泉四段的岩石类型、粒度分布、沉积构造、泥岩颜色及地球化学特征等各类沉积相标志进行分析,确定其为三角洲沉积,包含三角洲平原和前缘亚相。其中,平原亚相可识别出分支河道、决口扇、天然堤、废弃河道、湖泊沼泽微相;前缘亚相可细分为水下分支河道、河口坝、远沙坝、水下天然堤和支流间湾等微相。依据沉积微相与地层格架的成因关系,在中期基准面旋回的控制下应用取心关键井建立了沉积微相的定量识别图板,对非取心井进行沉积微相的定量识别与划分,并在此基础上绘制了沉积微相的平面及剖面图,总结了微相类型的平面和纵向展布规律及其与含油性的关系,指出分支河道砂体发育规模、连续性、储集性、含油性最好,其次为河口坝砂体,为研究区下一步的开发方案提供地质依据。     

标量FDTD法分析渐变折射率光波导模场分布

用标量时域有限差分法（Finite-differece Time-domain Method,FDTD法）分析了渐变折射率平面光波导中基模的模场分布情况，采用平面光波、球面光波、高斯光波等5种不同形态的光波激励同一波导，借助计算机进行数值求解，得到的光场分布图在光场传播达到稳定后完全相同，说明波导的模式与光波形态无关，只与波导结构和光波波长有关，结果表明该方法直观、精确、快速，并与解析法分析的结果一致。     

空调用多翼离心风机叶轮的性能预估

采用二维粘性数值模拟方法对三个不同参数的空调用多翼离心风机叶轮进行了数值计算，分析了空调用多翼离心叶轮的内部流场，预估比较了三个叶轮的风量静压性能．预估结论与试验结果相符，说明了在空调用多翼离心风机设计中可以采用数值模拟技术对叶轮性能进行预估，以减少实物模型试验，缩短产品开发周期，降低产品开发成本。     

基于单调链的平面型腔行切加工轨迹生成算法

针对平面型腔行切加工刀具轨迹生成中如何合理而最大程度地减少在加工刀具轨迹中产生的跳刀动作的次数，提出了一种基于单调链技术的行切刀具轨迹生成算法，从而使对给定平面型腔而产生的行切刀具轨迹最大程度地减少了跳刀动作的次数，而且针对给定的复杂平面型腔，该算法可以预先分析出可能产生的最大跳刀次数，这一算法已在实际开发的CAM系统中成功实现。     

EB病毒及化学致癌物DNP对人胚鼻咽粘膜裸鼠移植的诱癌研究

用EBV,DNP及PMA分别或协同对人胚鼻咽粘膜裸鼠移植物进行诱癌研究,探讨上述因素在人实验性鼻咽癌发生中的作用。免疫荧光法检查证实,经B95-8上清液体外及体内转染的人胚鼻咽粘膜上皮表达EBNA。实验结果显示,实验各组均可见各种增生性改变,对照组仅见一般增生性病变。各诱癌组均可见癌前病变,组间无显著性差异。共出现癌8例(1)EBV组:原位癌1例。 (2)EBV+PMA组:早期浸润癌1例。(3)EBV+DNP组:原位癌及浸润癌各1例。(4)EBV+DNP+PMA组:浸润癌1例。 (5)DNP组:原位癌1例。(6)DNP+PMA组:原位癌及浸润癌各1例。结果提示EBV可能在人鼻咽上皮实验性癌变过程中起病因作用。本研究成功诱发了三例浸润癌,均系DAP与其它因素(PMA、EBV)协同作用,提示人鼻咽癌的发生可能与多种致癌因素的相互作用有关。     

管内流动换热过程的性能综合分析

基于管内流动换热方程,在最小初投资的条件下导出经济合理的管长、管径比与换热参数的关系式.同时对管内流动换热过程进行火用分析,得出火用损失率最小的最佳运行参数(Reopt),以及由换热准则关系式得出的最佳换热参数(Stopt),最后得到使管内流动换热过程的结构、流动与换热性能综合优化的管长管径比.     

膜厚综合法确定磷化液

根据正交实验各组磷化膜的性能指标,采用膜厚综合评定法确定出了一种常温磷化液的介质组成及相应的工艺参数,并检测分析了磷化膜的均匀性、耐蚀性、膜重等.     

Symmetrical directional cloning: An efficient method to prepare hairpin RNA interference constructs

RNA interference (RNAi) is a loss-of-function approach by which double-stranded RNA (dsRNA) initiates degradation of homologous mRNAs in a sequence specific manner. The dsRNA molecules can be produced in vitro or in vivo, and can be introduced to cells in a number of ways. Here we report a more efficient method for the cloning of inverted repeat DNA fragments into expression vectors that can be transcribed into effective dsRNA molecules in vivo or in vitro. This method, named Symmetrical Directional Cloning (SDC), takes the advantage of compatible non-palindromic restriction enezyme sites, which allow one to directionally clone a single PCR product in both the sense and antisense orientations together into a vector. SDC allows for the directional cloning of inverted repeats using a single PCR product; it requires only one cut site on each side of the loop. Hence this method is more cost effective and less time-consuming. At least 21 commercially available restriction endonucleases can be used as cloning sites for the SDC method. The efficacy of dsRNA expression vectors prepared by SDC has been demonstrated by targeting a negative regulator of the signaling pathway mediating the response of cells to phytohormone, gibberellins (GA), in the aleurone cells.     

弯掠翼叶轮内流二次涡系的计算机数值仿真

采用非交错网格下的曲率时间尺度K-ε湍流模型和纳维斯托克斯方程线求解，对宇宙航空用弯掠叶轮和基准叶轮叶道内部三维粘性速度场进行了数值仿真，分析了叶轮流道内部通道涡等复杂二次涡系结构的流谱特性及其对气动性能特别是旋转失速的作用机理．研究表明：弯掠叶轮流道内通道涡、刮擦涡有效卷吸翼顶边界层低能流体，抑制了翼顶部的流动分离和旋转失速，有利于失速裕度的扩大．数值仿真结果为弯掠叶轮的计算机辅助设计提供了改进指导信息．