氯化钡生产工艺的研究

论述了氯化钡的两种主要生产工艺,对反应、除杂及分离、浓缩及结晶等工序作了深入的研究,并对影响产品收率、质量等有关的主要因素作了进一步的探讨,同时提供了浓缩结晶的新方法,另外也对生产过程中的劳动保护和环境保护提出了参考意见。     

学生自拟项目的计算机实验教学模式

计算机实验教学是提高学生计算机实践能力的关键环节。文中在传统项目教学法的基础上提出了以学生自拟项目作为主导的计算机实验教学模式,探讨了以该模式来培养创新人才的实验教学方法,并在实验课程考核评价体系中引入了自评的评价方式,最后分析总结了该实验教学模式的优点。     

Sb(Ⅲ)和Sb(Ⅴ)在蒙脱土表面的吸附与解吸

采取批实验方法研究不同pH值条件下,Sb(Ⅲ)和Sb(Ⅴ)在蒙脱土表面的吸附与解吸行为,以及离子强度对吸附行为的影响。结果表明,pH值对Sb(Ⅲ)和Sb(Ⅴ)在蒙脱土表面的吸附行为影响显著,pH值在3～10时,随介质pH值的升高,Sb(Ⅲ)和Sb(Ⅴ)的吸附均减弱;离子强度对吸附影响不显著,Sb(Ⅴ)的解吸量随吸附介质pH值的增加而增加。     

棉机织物在风场中的自由动态弯曲性测试及影响因素分析

采用一种新的动态弯曲测试方法并制作测试装置,将矩形自制纯棉机织物试样置于规定的稳定风场中,一端固定,另一端自由下垂,在气流的作用下来回自由弯曲摆动;提出动态弯曲角指标,每隔1/24s对织物试样在来回弯曲运动中的动态弯曲角进行测试,得到该指标随时间的变化曲线和一段时间内的平均值,以此对棉机织物试样的动态弯曲变形行为进行分析和评价.通过试验分析,探讨气流、纱线线密度、织物密度及组织结构对织物动态弯曲变形性能的影响.研究发现,织物试样在一定的气流环境中呈现一种有内在规律性的动态弯曲变形行为,这种行为是织物本身和外界气流等多因素下的综合效果.     

选煤厂主厂房网架结构屋盖的抗震性能研究

以某在役选煤厂主厂房屋盖的固定铰支座网架结构为研究对象,采用3D3S分析软件分析了组合荷载对网架结构抗震性能的影响.结果表明:两区网架结构动力特性相似,各网架结构的自振频率密集,结构的低阶整体振型以竖向振型为主,结构整体性强,局部振动不明显;在7度多遇地震作用下,结构的组合荷载作用的内力和位移响应属于同一量级,结构安全稳定性符合规范要求.     

TG-DTG和FTIR法研究碳酸镁水合物的热分解

以水氯镁石(MgCl2.6H2O)为镁源、Na2CO3为沉淀剂,利用沉淀法分别在30℃和90℃下制备得到碳酸镁水合物:三水碳酸镁和碱式碳酸镁。采用TG-DTG和热重跟踪法对此碳酸镁水合物的热分解进行分析。采用FTIR和SEM对热重跟踪实验中试样的组成和形态进行分析。结果表明:三水碳酸镁和碱式碳酸镁分别分5个和2个阶段进行分解,且二者脱水和脱二氧化碳的温度区间几乎相同;对于中间相的组成,FTIR分析结果与TG数据的计算结果一致;SEM图形象地呈现出了二者在轻烧过程中的形态变化。这将为盐湖水氯镁石制备高纯镁砂过程中轻烧工艺的确定提供一定的理论依据。     

热等离子裂解甲烷制备纳米碳纤维

以N2、H2混合气体为工作气,常压条件下裂解甲烷制得纳米碳纤维。考察了原料气流量、工作气气氛和催化剂类型对CNFs生长的影响,并用SEM和TEM表征产物的形貌和结构。结果表明:原料气甲烷流量的增加可引起产物的形貌多样性增加;由于N2比Ar热值高,高温持续时间长,有利于元素态金属原子参与完成碳结构的石墨化进程,所得纳米碳纤维较Ar气氛产物碳层连续、互相平行,纤维管内外表面平直、光滑、无沉积。以Fe2O3为催化剂,纤维管直径分布范围小,杂质或无定形碳很少;以Co2O3为催化剂,产物近似多壁碳纳米管结构,但纯度较低;以Ni2O3为催化剂的管状产物是长度不到1μm的短截管,结晶度较差。     

Cell-specific ATP7A transport sustains copper-dependent tyrosinase activity in melanosomes

Copper is a cofactor for many cellular enzymes and transporters. It can be loaded onto secreted and endomembrane cuproproteins by translocation from the cytosol into membrane-bound organelles by ATP7A or ATP7B transporters, the genes for which are mutated in the copper imbalance syndromes Menkes disease and Wilson disease, respectively. Endomembrane cuproproteins are thought to incorporate copper stably on transit through the trans-Golgi network, in which ATP7A accumulates by dynamic cycling through early endocytic compartments. Here we show that the pigment-cell-specific cuproenzyme tyrosinase acquires copper only transiently and inefficiently within the trans-Golgi network of mouse melanocytes. To catalyse melanin synthesis, tyrosinase is subsequently reloaded with copper within specialized organelles called melanosomes. Copper is supplied to melanosomes by ATP7A, a cohort of which localizes to melanosomes in a biogenesis of lysosome-related organelles complex-1 (BLOC-1)-dependent manner. These results indicate that cell-type-specific localization of a metal transporter is required to sustain metallation of an endomembrane cuproenzyme, providing a mechanism for exquisite spatial control of metalloenzyme activity. Moreover, because BLOC-1 subunits are mutated in subtypes of the genetic disease Hermansky-Pudlak syndrome, these results also show that defects in copper transporter localization contribute to hypopigmentation, and hence perhaps other systemic defects, in Hermansky-Pudlak syndrome.     

A two-tiered mechanism for stabilization and immobilization of E-cadherin

Epithelial tissues maintain a robust architecture which is important for their barrier function, but they are also remodelled through the reorganization of cell-cell contacts. Tissue stability requires intercellular adhesion mediated by E-cadherin, in particular its trans-association in homophilic complexes supported by actin filaments through beta- and alpha-catenin. How alpha-catenin dynamic interactions between E-cadherin/beta-catenin and cortical actin control both stability and remodelling of adhesion is unclear. Here we focus on Drosophila homophilic E-cadherin complexes rather than total E-cadherin, including diffusing 'free' E-cadherin, because these complexes are a better proxy for adhesion. We find that E-cadherin complexes partition in very stable microdomains (that is, bona fide adhesive foci which are more stable than remodelling contacts). Furthermore, we find that stability and mobility of these microdomains depend on two actin populations: small, stable actin patches concentrate at homophilic E-cadherin clusters, whereas a rapidly turning over, contractile network constrains their lateral movement by a tethering mechanism. alpha-Catenin controls epithelial architecture mainly through regulation of the mobility of homophilic clusters and it is largely dispensable for their stability. Uncoupling stability and mobility of E-cadherin complexes suggests that stable epithelia may remodel through the regulated mobility of very stable adhesive foci.     

项目引导型模式在电工电子实验教学中的应用

电工电子实验是电类人才教育的基础,直接影响着电类创新型人才的培养,而长期以来电工电子实验的教学模式因循守旧,已经不符合时代的需要。文中着力研究项目引导型实验教学模式在电工电子教学改革中的应用,通过改革内容、教学方法和评价体系三个方面的探索,证明了此模式对于提高学生的自主学习积极性、动手能力以及创新能力有着积极的效果。此项研究为电工电子实验教学改革以及创新型人才培养提供了一种有效途径,具有一定的现实意义。