THE TRANSFER BEHAVIOUR OF SOME CATIONS AT WATER／NITROBENZENE INTERFACE BY SEMIDIFFERENTIAL CYCLIC VOLTAMMETRY

The transfer of Sr~(2+) and Ba~(2+) ion, facilitated by 18-Crown-6 present in the aqueous phase, and of succinylcholine ion at w/nb interface were investigated by semi-differential cyclic voltammetry. A good polarographic curve of succinylcholine ion dissolved in water was obtained in the system of 0.01 mol/l LiCl (w)——0.01 mol/l TBATPB (nb). The peak current is directly proportional to the concentration of SC~(2+) ion. It can be used for the determination of SC and the detection limit is 1.05×10~(-5) mol/l.The apparent D~w and D~(nb) have been estimated. The transfer of Sr~(2+) and of Ba~(2+) at the interface are facilitated by 18-Crown-6 present in the aqueous phase and the peak current is directly proportional to the concentration of 18-Crown-6 in water. This method can be used for the determination of the complexing agent and for the stability constant of the complex formed in the aqueous phase.All the experimental results are in keeping with the theoretical.     

浅谈普通话的可感性特点

作为审美对象,普通话和其它美的形象一样,是具有特殊规定性的形式和内容的统一体,从形式上看,普通话的可感形象体现在它的语音美及节奏美。     

HPA/MXOY杂多酸在合成异戊酯上的应用研究

本文研究了HPA/MXOY固体杂多酸催化剂的制备及负载,并以异戊醇合成异戊酯为探针,用硅盐、锆盐、活性炭等物质为载体,进行了催化效果的研究及表征。实验结果得出:HPA/ZrO型杂多酸催化剂效果最佳,酯收率可达82%。     

关于计量经济学学习的几点思考

计量经济学是一门独特的学科,它的学科基础十分广泛,学习的方法与思维有别于其他的学科,并且实际的操作性很强,从宏观的角度把握了它的一些特点,有利于从总体上理解并学好计量经济学。     

PRELIMINARY STUDY ON RETRO-REFLECTIVE COATED PAPER BASED ON MICROGLASS BEADS

INTRODUCTIONThe micro-glass bead[1-2] is a new kind of silicate material, with good properties of chemical stability, mechanical strength as well as electro-resistance. When its diameter is below 0.08mm and the reflective index is in the range of 1.9~2.1, retro-reflective characteristics can be achieved. When a beam of ray from any direction irradiates the surface of the micro-glass beads, it can be converged at the special reflective layer consisted of focuses of micro-glass beads, owing …     

Molecular dynamics study on the structure I helium hydrate

A 368- water molecule structure I gas hydrate, encased by the number of helium (He) molecules ranging from two to twenty-two, are calculated by molecular dynamical simulations. The potential TIP4P (transferable intermolecular potentical with four sites) is used for water interactions and Lennard-Jones for He-He and He-water interactions. He molecules do not affect the water lattice and can stabilize the hydrate when their concentration is small. A trough signature of He encased is found at 80～90 meV in the phonon density of states. He molecules prefer to be more off-center in 51262 cages. Heavier isotope He are energetically favorable to be filled in cages.     

A ROBUST DECOMPOSITION OF LINEAR PROGRAMMING USING A GOAL-PARTITIONING METHOD

The Dantzig/Wolfe linear programming decomposition algorithm has had important economicinterpretations as well as a widespread impact on solving large scale linear programming problem.Inthis paper we consider a similar underlying structure,where however there is only one couplinginequality or equation.With this simplification,we demonstrate how to achieve an equitable partitionof the overall coupling resource to individual subproblem constraints through a simple iterationprocedure which appears to be very efficient.     

算子子空间的D_σ~(n)(r)性质的一个充分条件

给出了一个确定算子子空间具有性质D_σ~(n)(r)的方法。     

芝麻素类型木脂素的合成研究Ⅳ2－苯基呋喃3，4－二羧酸二甲脂与格氏试剂反应的研究

研究了２－苯基呋喃－３，４－二羧酸二甲酯（２）与格氏试剂苯基溴化镁等（３）反应，生成酮基酸酯２－苯基－４－苯甲酰基呋喃－３－羧酸甲酯（１）的条件和方法。     

基于截断正态概率模型的改进目标跟踪算法

在应用NIFPAT算法对机动目标跟踪时存在计算量大和要求网络训练两个弱点。分析了截断正态概率模型和NIFPAT算法后 ,把截断正态概率模型与NIFPAT算法思想相结合 ,提出了基于截断正态概率模型的改进目标跟踪算法。该算法根据目标机动情况自动调整系统方差 ,在附加较小计算量的情况下 ,能取得较好的跟踪效果。仿真实验表明 ,该算法能有效地提高对机动目标的跟踪精度。