The hybridization between peptide nucleic acid containing azobenzene and DNA labeled nanoparticle on chip surfaces studied by atomic force microscopy

Peptide nucleic acid containing azobenzene （N-PNA） was covalently bound on chip surfaces. Complementary DNA probes labeled by gold nanoparticles hybridizated with PNA on chip surfaces, The hybridization was successfully detected with AFM by the microscopy mothed. The influences of the position and the cis-trans isomerization of azobenzene unit on hybridization were investigated with AFM.     

化工生产人工误操作危险与可操作性分析研究

研究了危险化学品生产装置开、停车过程中人工误操作危险与可操作性分析系统,可为防范人工误操作提供新的分析方法,为防范事故提供技术依据。以吉林石化硝基苯初馏塔开车过程中由于人工误操作引发的爆炸事故为例进行了分析。     

Preparation and Structural Analysis of Lanthanide Complexes with α-Hydroxyl-phenyl-acetic Acid and 1,10-Phenanthroline as Ligands

A series of ternary lanthanide complexes Ln(C6H5CHOHCOO)3(phen) (H2O) (Ln= La, Ce, Pr, Nd,Sin, Eu) were synthesized with α-hydroxyl-phenyl-acetic acid and 1, 10-phenanthroline (phen) as ligands. The structure and of complexes were characterized by elemental analysis, IR, 1H-NMR, UV and TGA, and the co-ordinate mode of both ligands was discussed. It was shown that the co-ordinate mode of 1, 10-phenanthroline was chelated,while α-hydroxyl-phenyl-acetate ion was monodentate or bridging. The mechanism of thermal by thermogravimetry was indicated that the degree of co-ordinate ability of ligand was: α-hydroxyl-phenyl-acetate ion＞1, 10-phenanthroline (phen).     

鸡油菌挥发油化学成分分析

用同时蒸馏-萃取方法提取鸡油菌挥发油(得率为1.27%),并用气相色谱-质谱联用仪对鸡油菌挥发油的化学成分进行分析,分离并鉴定出了32个组分,占总峰面积的86.79%,并用峰面积归一化法测定了各成分的质量分数.挥发油主要成分是1-辛烯-3-醇(33.42%)、2-辛烯-1-醇(17.25%)、棕榈酸(9.19%)、(E)-9-十八碳烯酸(4.82%)、亚油酸(4.56%)、3-辛醇(2.75%)、3-羟基-2-丁酮(2.24%)、己醛(2.03%)、2-环戊烯-1,4-二酮(1.52%)和3-辛酮(1.39%).     

奇异杂交边界点方法求解泊松方程

用奇异杂交边界点法同双重互易法相结合来求解泊松方程,将泊松方程的解分为通解和特解两部分,通解使用奇异杂交边界点方法求解,特解则利用局部径向基函数近似.该方法输入数据只是求解域上离散的点,不需要额外的方程来计算域内物理量,后处理十分简便.数值算例表明,奇异杂交边界点法在求解泊松方程时具有较高的精度和数值稳定性.     

基于I/Q正交双路的USB、LSB和DSB的一种识别算法

针对传统的单路P参数识别算法中必须保留载波残余频偏的缺点,提出了一种基于I/Q正交双路的识别算法.该算法直接将信号搬到基带,无需保留载波残余频偏,消除了残余频偏对较低频段信号识别和解调的不利影响.给出了上边带调制信号、下边带调制信号和双边带调制信号在不同信噪比(SNR)下的P参数值,并给出了其在不同SNR下的正确识别率.仿真结果表明,在SNR不小于0的情况下,平均正确识别率在95%以上.     

基于套迭代技术的弹性梁动力H向应分析的多重网格方法

提出了一种基于套迭代技术的求解弹性梁动力响应的多重网格方法。这种方法充分利用了初始网格下的结果,然后由多重网格嵌套迭代过程实现对弹性梁动力响应问题的求解。这种方法将网格离散过程和数值求解过程很好地相结合,与其他方法相比较,具有计算精度高,运算时间短等特点。     

Optimal carrier-smoothed-code algorithm for dual-frequency GPS data

Carrier-smoothed-code (CSC) algorithm is an effective pseudorange multipath mitigation technique, which can alleviate the computational burden and reduce the communication bandwidth needed for the transmission of GPS observations. This paper presents an improved Hatch filter and address the optimal CSC algorithm for dual-frequency GPS data based on the optimal parameter estimation theory. The smoothed observations have the same information content as that of the raw dual-frequency GPS data from which they are derived. Consequently, the optimal CSC algorithm is equivalent to the uncombined algorithm. Theoretical analyses show that the data precision of the optimal CSC algorithm is better than that of Hatch filter and its improved version.     

Petrology and mineral chemistry of new ureilites found in Grove Mountains, Antarctica

Petrography and mineral chemistry of two new ureilites, GRV021512 and GRV022931, from the Grove Mountains, Antarctica, are reported in this paper. GRV 021512 exhibits a typical ureilite texture, and consists of 48.3% olivine, 9.4% pigeonite and 38.1% carbonaceous interstitial material and/or reduction product. GRV 022931 has a cataclastic porphyritic texture, and consists of 19.1% olivine and 14.1% pigeonite embedded in 66.3% carbonaceous interstitial material and/or reduction product. The coarse-grained olivine and pigeonite in both meteorites have homogeneous cores, and they are FeO-rich within the range of the ferroan subgroup (subgroup I) of olivine-pigeonite ureilites. All olivine grains of the meteorites show reduction zones along boundaries and cracks. Abundant diamond coexists with graphite as graphite-rich patches and veins in the carbonaceous interstitial material. Petrogenesis of both meteorites and origin of diamond are discussed.     

拒绝服务攻击防范技术研究

拒绝服务攻击对网络构成了巨大的安全威胁.由于网络协议本身并不安全,所以处理拒绝服务攻击是非常困难的.从分析拒绝服务攻击的起因入手,揭示拒绝服务攻击的机制和过程,并对拒绝服务攻击进行归类,总结了防范拒绝服务攻击的措施.