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891.
柱前衍生反相高效液相色谱法同时测定植物络合素(PCn)等巯基化合物 总被引:2,自引:0,他引:2
介绍一种荧光试剂monobromobimane柱前衍生,反相高效液相色谱一荧光检测测定标准样品和植物组织中植物络合素(PCn)等巯基化合物的方法.结果表明,采用乙腈和0.1%三氟乙酸组成的二元梯度洗脱程序,标准混合液中PCn等5种巯基化合物15min内得到很好的分离.以谷胱甘肽为代表考察方法的精密度,在1.25~160ng/μL浓度范围内与峰高有较好的线性关系,相关系数r^2=0.9999.谷胱甘肽的回收率平均为97.64%,40d内的变异系数平均为2.21%.方法具有快速、灵敏、稳定性好、易于实施、同时测定PCn等多种巯基化合物等优点.通过该方法的应用,首次揭示Cd超积累植物东南景天对CA的超量积累和解毒与PCn无关. 相似文献
892.
XURen-zuo HANYi-fan HUANGCan YAOJun-feng 《武汉大学学报:自然科学英文版》2005,10(1):9-12
Based on the fact that the software development cost is an important factor to control the whole project, we discuss the relationship between the software development cost and software reliability according to the empirical data collected from the development process. By evolutionary modeling we get an empirical model of the relationship between cost and software reliability, and validate the estimate results with the empirical data. 相似文献
893.
Carbon isotopic record of foraminifers in surface sediments from the South China Sea and its significance 总被引:3,自引:0,他引:3
CHENGXinrong WANGPinxian HUANGBaoqi LIUChuanlian JIANZhimin ZHAOQuanhong LIJianru TIANJun XUJian 《科学通报(英文版)》2005,50(2):162-166
Since the 1990s, the papers and data involved withthe South China Sea (SCS) have been emerging in largenumbers in the world as people pay more attention to thepaleoceanography of the SCS. There have been more than100 cores mentioned in papers containing p… 相似文献
894.
黄敏 《西南科技大学学报》2005,20(2):10-12,22
Internet大面积遭受蠕虫攻击的事件时有发生,针对这种问题,引入Honeypot技术,结合入侵检测系统(IDS)、数据挖掘提出了一种解决办法:将Honeypot置于DMZ中,利用其欺骗地址空间技术覆盖服务器中没有用到的IP地址,捕获蠕虫;IDS监控流入网络的数据包,对入侵作出反映;系统日志异地保存。该系统能有效抵御目前已经出现的蠕虫攻击,同时对新出现的目前未知的蠕虫攻击也有很好的防御效果。 相似文献
895.
HUANG Dan SUN Hongmei LIU Taiqi XU Fan SHEN Qi 《科学通报(英文版)》2005,50(17):1843-1845
Cp2Yb·2THF reacts with CpNa in 1:1 molar ratio in THF at 40℃ for 2 h, and the in situ generated anionic divalent complex NaYbCp3(THF)n reacts further with an excess of CpH at 40℃ for 48h, after work-up, affording the trivalent anionic ytterbium complex[Na(THF)2(μ2-η^5-Cp) (η^5, η^5,η^1-Cp3Yb)(THF)]n:(1) by oxidation reaction of Cp2Yb with CpH. Crystal structure determination reveals that complex 1 has one-dimension polymeric chains of distinct Na(THF)2(μ2-η^5-Cp) (η^5, η^5,η^1-Cp3Yb)(THF) units, which were formed by the coordination of the bridging Cp ligand with Cp3Yb'THF and Na(THF)2 in η^5,η^5 mode via self-assembly. 相似文献
896.
HUANG Zhiqun XU Zhihong BOYD Sue WILLIAMS David 《科学通报(英文版)》2005,50(22):2581-2586
Decomposition of stumps in successive rotation of Chinese fir (Cunninghamia lanceolata (Lamb.) Hook.) plantations was studied using a chronosequenee approach. The results showed that decomposition rate constant of Chinese fir stump was 0.02695 as calculated from Olson's model. The N content of stump increased during the first two-year decomposition. When the dead stump C/N ratio was 463.2 ± 27.3, the stumps started to release N. The pattern of P release was similar to that for N. However, K content of stumps showed a consistent declining trend over time during the whole decomposition. ^13C nuclear magnetic resonance spectroscopy with cross polarization and magic-angle spinning (^13C CPMAS-NMR) was used to analyse organic carbon (C) components in decomposing stumps. The ^13C CPMAS-NMR spectra of stumps displayed that stump was dominated by cellulose and hemieellulose. The spectra also showed the accumulation of intensity in alkyl C, aromatic C, and earboxyl C spectral regions, which was expected as the labile cellulose and hemieellulose components in O-alkyl C spectral region were selectively decomposed first. 相似文献
897.
LUO Ercang HUANG Yun DAI Wei ZHANG Yong WU Zhanghua 《科学通报(英文版)》2005,50(22):2662-2664
The working principle of an efficient travelling- wave thermoacoustic refrigerator operating in room-temperature range has been analyzed and an experimental set-up has been built. The experiment showed that suppressing DC-flow streaming was very critical to efficient operation, and an elastic membrane was used to solve the problem successfully. At the most efficient operating point, the novel thermoacoustic refrigerator achieved a cooling capacity of about 80 W at -20℃, with a much higher efficiency than previously developed standing-wave thermoacoustic refrigerator. 相似文献
898.
机动目标空间合群仿真 总被引:1,自引:0,他引:1
为了解决空间合群和战场中的事件检测问题,提出了一种新的机动目标的空间群生成算法.该算法通过一级融合获得的信息来定义特征相似度,即归属相似度、位置相似度和速度相似度,并将这些相似度再次融合以求得合群结果.由于测量空间的不确定性被映射到了模糊相似度空间,因此通过模糊匹配机制可解决测量空间的不确定性问题.仿真结果表明,所提算法能实时完成多个级别的空间合群融合,其计算复杂度也比较低,而且在空间合群的态势评估中获得了比较好的结果. 相似文献
899.
900.
QI Xianghui SUN Liang LUO Zhaofei WU Jiequn MENG Xiaolei TANG Yue WEI Yutuo HUANG Ribo 《科学通报(英文版)》2006,51(24):2977-2985
1,3-propanediol (1,3-PD) is an important material for chemical industry,and there has been always much interest in the production of 1,3-PD using all possible routes. The genes encoding glyc-erol dehydratase (GDHt) from Citrobacter freundii,Klebsiella pneumoniae and metagenome were cloned and expressed in E. coli. All glycerol dehy-dratases but the one from metagenome could be detected to show enzyme activities. In order to im-prove the enzymatic properties of GDHts,the genes encoding α and β-γ subunits were cloned,and the enzyme characteristics were evolved by rational de-sign based on their 3D structures which were con-structed by homology modeling. Six heteroenzymes were obtained by swapping the α subunit genes of these three different-source-derived GDHts. The pH,thermal stability and Vmax of some heteroenzymes were dramatically improved by 2―5 times compared with the wild one (GDHtKP). The GDHt cloned from metagenome,originally proved to be with no enzyme activity,was converted into active enzyme by swap-ping its subunits with other different GDHts. In addi-tion,the effect of subtle 3D structural changes on the properties of the enzyme was also observed. 相似文献