氢化物发生-原子荧光法测定烟叶中的铅

建立了一种测定烟叶中微量铅的方法--氢化物发生-原子荧光光谱法.研究了光电管负高压、灯电流、屏蔽气和载气流量、载流的选择、酸度等对实验的影响.在选定的工作参数下,检出限为0.08 μg/L.用标准物质桃叶(GBW08501)对该法进行了验证,验证结果与推荐值一致,相对标准偏差为0.34%.该方法简便、快速、灵敏,对于实际样品的测定得到了满意的结果.     

快速多极边界元法在薄板结构中的应用

基于Taylor级数多极展开研究了边界元快速多极算法(FM—BEM)，并将它应用于薄板结构。算例分析表明FM—BEM的计算时间和存储空间明显少于常规边界元迭代解法。随着问题规模的增大，这种优势将更加突出。     

Effects of Ca on the distribution, structure and morphology of aluminum species in polyaluminum chloride

The flocculation efficiency of polyaluminum chloride (PAC) is closely related to the distribution and structure of its AI species, and Al13 is the optimal species in PAC for flocculation. A series of PAC containing Ca was prepared by adding Ca before and after the basifying reaction. The effects of Ca on the Al species were studied by ^27Al nuclear magnetic resonance (NMR) and atomic force microscope (AFM) techniques. The experimental results show that the introduction of Ca increases the content of Alm and Al13 in PAC and decreases their chemical shifts in NMR spectra due to the electric repulsion between the positive Ca species and AI species and the formation of AI-O-Ca complexes.With the rise of Ca/AI molar ratio, the AI species in PAC tend to scatter. It is observed that the formerly branch-aggregated clusters are tending to form granule-aggregated ones whose diameter gets smaller and smaller, and the floccule aggregates are formed at a higher Ca/Al molar ratio. The introduction of Ca to PAC, which increases the Al13 content, is certainly to enhance the flocculation efficiency of PAC in water treatment.     

Preparation and properties of antimony thin film anode materials

Metallic antimony thin films were deposited by magnetron sputtering and electrodeposition. Electrochemical properties of the thin film as anode materials for lithium-ion batteries were investigated and compared with those of antimony powder. It was found that both magnetron sputtering and electrodeposition are easily controllable processes to deposit antimony films with flat charge/discharge potential plateaus. The electrochemical performances of antimony thin films, especially those prepared with magnetron sputtering, are better than those of antimony powder. The reversible capacities of the magnetron sputtered antimony thin film are above 400 mA h g^-1 in the first 15 cycles.     

Deep-water Earliest Oligocene Glacial Maximum （EOGM） in South Atlantic

The most prominent cooling event of the Earth surface during Cenozoic in the long-term transition from a non-glaciated planet, or “green-house world”, to a polar, glaciated planet, or “ice-house world”, is the Earliest Oligocene Glacial Maximum (EOGM) above the Eocene/Oligocene boundary at about 33.7 Ma. Planktonic and benthic foraminiferal oxygen and carbon isotopes, carbonate content, and coarse fraction, along with high-resolution color reflectance and magnetic susceptibility records during 35-30 Ma, from deep-water Sites 1262 and 1265, Ocean Drilling Program (ODP) Leg 208 in South Atlantic, reveal the global cooling event occurring in both surface and deep oceans. The results show that the earliest Oligocene δ^18O values during 33.5-33.1 Ma represent the magnitude of continental ice sheets on east Antarctica and indicate the large decrease in both surface and deep water temperatures of worldwideoceans. The δ^13C records show the large excursion during the period of EOGM event and indicate some types of shift in global carbon reservoir, probably demonstrating the sudden increase in organic carbon burial rates and the changes in the distribution and timing of production. At the same time, lithologic composition, carbonate content, color reflectance, and coarse fraction brought about significant changes close to the Eocene/Oligocene boundary, reflecting the abrupt deepening in the carbonate compensation depth (CCD). Changes in carbonate content were revealed from the color reflectance identify periodicities associated with eccentricity of the Earth‘s orbit (100 and 400 ka), further indicating orbitally forced global climate variations in the Early Oligocene.     

Discovery of a Miaohe-type Biota from the Neoproterozoic Doushantuo Formation in Jiangkou County, Guizhou Province, China

A megascopic algal fossil assemblage was first discovered by Ma Guogan and Chen Meng‘e in the black shales of the Neoproterozoic Doushantuo Formation in Miaohe Town, Zigui County, Hubei Province in 1978. Formal naming of the Miaohe Biota was proposed by Cheng Meng‘e and Xiao Zongzheng in 199112j, and eleven morphological genera have been previously described. including megascopic algae and putative metazoans .Ding et al. greatly expanded the scope of the Miaohe Biota to 9 phyla consisting of 140 genera, including microphytoplanctons, megascopic algae, metazoans, spongesand trace fossils. Xiao et al. further restudied this fossil assemblage, concluding that only about 18 distinct taxa could be recognized and that many Miaohe taxa are poorly defined or svnonvmous.     

产业集群环境下的知识创新体系研究

经济全球化的今天 ,激烈的市场竞争要求企业通过有效的知识创新来提高对环境的响应能力 ,增强其竞争力 ,产业集群有利于提高集群内产业组织的知识创新能力。本文首先阐述了产业集群对知识创新的促进作用 ,进而提出了产业集群的创新体系 ,从创新要素、创新过程两个角度分析创新活动的完成 ,最后对我国产业集群环境下的知识创新的发展提出了几点思考     

建筑创作活动中的创新能力剖析

建筑创作活动具有艺术与工程的双重属性 ,本文从建筑创作活动的特点出发 ,综合广义的创造力研究成果 ,从建筑创作的思维特点、建筑师的个性特征、建筑创作过程、建筑创作成果、建筑创作的源泉等方面来剖析建筑创作能力的特征和内涵     

海啸

海啸是一种具有强大破坏力的海浪。当海底地壳发生断裂、移位、塌陷、山崩、火山爆发、大面积滑坡等活动时，都会伴随着海底地震的出现。地震的发生使震区的海洋水体出现振荡波。当振荡波接近大陆海岸时，与越来越浅的海底磨擦，使波速降低、波长缩短，而周期不变。由振荡波所卷起的海浪．在海岸一带其波高可达数十米(有时会超过百米)，     

如何设计企业财务收支审批制度

通过介绍财务收支审批制度设计的原则、财务收支审批制度设计的内容,叙述了如何设计企业财务收支审批制度。