由沉积物中准同生构造的褶皱展平试验确定沉积剩磁固化深度

上新世湖心相页岩中准同生构造的褶皱展平试验揭示,这套沉积物中的剩磁固化于这些准同生构造形成之后,固化深度大于10-15cm。这一事实与模拟实验结论的之间矛盾表明,由于天然过程的进行速率慢得无法与实验室过程比拟,天然沉积物中沉积后碎屑剩磁的作用要比模拟实验的绪论强得多。将模拟实验得出的关于磁性颗粒重新排列条件的定量结论简单地外推到天然过程是不适当的。任何关于沉积物获得剩磁的模型都必须接受以天然过程为基础的检验,仅有实验室内的模拟试验是很不够的。     

菱铁矿热处理后的异常等温剩磁与逆向磁化

菱铁矿经过适当温度热处理后的异常等温剩磁曲线的全部形态与初始剩磁态的３个集合相对应。根据ＩＲＭ曲线存在负微商线段这一事实，提出有逆磁相存在，并用正常磁相和逆磁相的耦合来解释这种异常等温剩磁行为，这种逆向剩磁是在室温下获得的，在弱化时没有任何热过程和化学过程发生，在本质上已与观察到的逆向热剩磁和逆向化学剩磁不同。     

Magnetic properties of street dust and topsoil in Beijing and its environmental implications

Environmental magnetic measurements were carried out on the sanrhples of street dust and topsoil, which were collected along the roadway in the urban and suburb of Beijing, including magnetic susceptibility （X）, anhysteretic remanent magnetization （ARM）, isothermal remanent magnetization （IRM） of all samples and temperature-dependence of magnetic susceptibilities and magnetic hysteresis parameters of representative samples. Obvious differences exist between the samples of street dust and those of topsoil. Compared with topsoil samples, the concentration of magnetic particles and high-coercivity components in street dust samples are higher, and the magnetic grains are coarser. Both dust and topsoil samples are dominated by ferrimagnetic minerals, and iron particles are only detected in some dust samples. These results suggest that street dust samples reflect the characteris- tic of particles produced by industrial and traffic activities, and the magnetic property of topsoil sam- ples represents the characteristic of particles from both anthropogenic and natural sources. The distribution of magnetic parameters is influenced by the environment where the samples are collected, like industry, traffic density and other road conditions. Hard isothermal remanent magnetization （HIRM） may be used as an indicator of particles produced by traffic activity. Dust storm samples collected on 17 and 18 April, 2006 have different magnetic properties from street dust and natural particles, like loess and paleosol, which indicate that the dust storm might be mixed with anthropogenic particulates during transport and falling.     

垂直磁记录薄膜交换耦合作用及开关场分布的测量

采用Lakeshore7407型振动样品磁强计,以Co-Pt垂直磁记录薄膜为例,详细介绍了垂直薄膜等温剩磁(isothermalremanentmagnetization,IRM)曲线、直流退磁剩磁(directcurrentdemagnetizationremanence,DCD)曲线的测量方法和退磁因子的计算方法,并给出根据退磁场修正后的IRM和DCD曲线计算垂直磁记录薄膜曲线和开关场分布(SFD)的方法.最后详细讨论了薄膜的微观组织和易磁化轴取向分布对退磁场、交换耦合作用和SFD的影响.结果表明:退磁场的存在使得直接测量得到的晶粒间交换耦合作用偏小,开关场分布宽化;影响晶粒间交换耦合作用的内在原因是介质的微观组织和易磁化轴的取向分布.     

Paleoclimatic significance of mineral magnetic properties of loess sediments in northeastern Qinghai-Tibetan Plateau

Loess deposit in the northeastern Qinghai-Tibetan Plateau offers an excellent record of climate and environment changes in this region.We have conducted multiparameter mineral magnetic analyses of smaples of loess deposits from the Dongchuan,Lalakou and Panzishan sections.The methods used include magnetic susceptibility,fre-quency-dependent suceptibility,temperature-dependent susceptibility,isothermal remanent magnetization acquisibility.Maghemite and hematite is also present in the loess layers and paleosol horizons.The higher concentration of maghemite in paleosols suggests that the formation of maghemite occurred during in situ pedogenesis,which plays an important role in the enhancement of the magnetic susceptibitily.Similar to that in the Chinese Loess Plateau lying to the east of the Liupan Mountains,magnetic granulometry in the studied loess and paleosols is predominantly pseudo-single-domain(PSD). However,the mean grain-size of the ferrimagnetic minerals in loess is evidently coarser (larger PSD and multiomain-like) than in paleosols (mainly PSD).The magnetic susceptibility of loess and paleosols is positively correlated with the content of ultrafine magnet-ite/maghemite grains,and hence with the intensity of in situ pedogenesis.Therefore,the enhanced magnetic susceptibility in the studied loess-paleosol sequences can be interpreted as being due to climatically induced in situ pedogenesis.     

Magnetic records of Core MD77-181 in the Bay of Bengal and their paleoenvironmental implications

Located in the low latitude region of the northeastern Indian Ocean, the Bay of Bengal represents one of the largest marginal seas in the world. The Bengal Fan hosts erosional products mostly from Himalayas and is under the influence of the Indian monsoon system. The Bengal Fan has thus been one of the ideal places for studying the uplift of the Tibet Plateau and the history of the Indian monsoon[1―8]. The intensity of the Indian monsoon is controlled by secular variations in insola- ti…     

滇中昆阳群古地磁研究

对昆阳群中采集的２８３块样品用热退磁法做了磁清洗处理,经精度检验,进行了统计分析．根据获得的古地磁结果,探讨了昆阳群地层所代表的古地磁极性和古纬度,建立了该地区中、晚元古界古地磁视极移路径,并与华北地块及扬子地块该时期的视极移路径进行了对比,讨论了其构造运动及相互之间的关系,认为下昆阳亚群与长城系古纬度相近,古地磁极性及视极移路径可比,时代相当．     

Paleomagnetism of early Paleozoic volcanic rocks from the Beishan area,Gansu of northwest China: Preliminary insight into early Paleozoic kinemics of the Beishan terrane

We report rock magnetic and paleomagnetic results for Middle Silurian Gongpoquan and Middle Ordovician Huaniushan volcanic samples collected from the Mazongshan and Hongliuyuan areas of Gansu Province, northwest China. The resultsindicate that the main magnetic mineral of the Gongpoquan and Huaniushan volcanic rock is magnetite, and it may remain characteristic remanent magnetization acquired at the time of formation of the rocks. However, with the exception of samples from site go20, most of Middle Ordovician Huaniushan volcanic samples have a very weak nature remanent magnetization, and generally show an erratic demagnetization behavior, which does not allow isolation of characteristic remanent magnetizations from these samples. Comparison of paleomagnetic results obtained from the Beishan area of Gansu with Paleozoic apparent polar wander paths for Tarimand Siberia suggests that the Beishan tarrane, the southern part of the Beishanarea of Gansu beyond the Mingshui-Shipanjin-Xiaohuang- shan zone, and adjacent Tarim block and Siberia plate could not have been connected in their present configuration by the Middle Silurian time. On the other hand, we infer that the early Paleozoic Mingshui-Shipanjin-Xiaohuangshan oceanic basin may open from west to east during period from the Ordovician to Silurian, and the post-Middle Silurian closing of this oceanic basin may result from a progressed eastward scissor-like rotation.     

9Cr5MoV钢的磁性分析与深冷处理

采用SLX-80深冷处理系统对9Cr5MoV钢进行冷处理,采用综合物理测试系统的振动样品磁强计选件(PPMS-VSM)测试样品的室温磁性。钢在930℃淬火态、-80℃和-120℃冷处理态,样品中残余奥氏体含量分别为13.5%,11.7%和10.1%,深冷处理(-120℃)较冷处理(-80℃)能更有效地减少钢中残余奥氏体。950℃淬火态钢测得最大硬度值(65HRC),淬火后-120℃深冷处理可使钢的硬度值提高至66HRC。950℃淬火再140℃低温回火后,-120℃深冷处理可使钢的硬度提高约1HRC。     

Nd_4Fe_(77.5)B_(18.5)纳米合金的磁化和反磁行为

研究了Nd4Fe77.5A18.5纳米合金的高场磁化特性及磁化场高低对其反磁化行为的影响.结果表明，在磁化场μOHmc－7T时，此合金仍没完全饱和．当磁化场Hmc高于某一临界值Hmc时，材料才表现出明显的永磁性．材料的永磁性来源于各相晶粒间的交换耦合作用．     

华南地块中三叠统巴东组红层磁倾角浅化效应

对华南地块中三叠统巴东组红层样品进行系统的岩石磁学和古地磁学研究, 采用高场等温剩磁各向异性(hf-AIR)方法, 识别出巴东组红层的磁倾角浅化因子f = 0.63。岩石磁学研究结果显示, 巴东组红层的主要载磁矿物为赤铁矿和少量磁铁矿; 磁化率和高场等温剩磁各向异性组构均指示其具有典型沉积组构特征, 表明未遭受后期构造应力改造。高温特征剩磁分量为碎屑赤铁矿所携带, 具有单一负极性, 并在95%置信水平上通过褶皱检验, 与前人在同一剖面不同位置获得的以正极性为主的古地磁方向一致。该特征剩磁方向在地层校正后的平均方向为D_s = 222.1°, I_s = ?27.2° (α₉₅ = 8.7°), 对应古地磁极为48.1°N, 215.5°E (A₉₅ = 8.4°)。对包括本文数据在内的华南中三叠世红层高质量古地磁极数据(Q≥5)用f = 0.63 进行统一校正后, 获得平均古地磁极为48.5°N, 207.6°E (A₉₅ = 10.7°)。对比华北地块同样经hf-AIR方法浅化校正后的早三叠世古地磁极, 两者在其东部参考点上的古纬度完全一致, 验证了前人提出的华南华北中生代剪刀式旋转拼合模型。     

Magnetic granulometry of recent sediments from the Huguang Maar and its implication for provenience

To understand the origin and its climatic implications of the Huguang Maar sediments, we conducted laser grain size analysis and rock mangtic measurement for the recent deposits from the Huguang Maar and for the volcanic rocks of the caldera for comparison. The grain size distributions are dominated by clayey silts for both the bulk sediments and magnetic separates. Acquisition of isothermal remanent magnetization (IRM) and thermal demagnetization of IRM suggest (titano) magnetite as the dominating magnetic mineral in the sediments; high coercivity minerals are not detected. Therefore, the ratio of the susceptibility of anhysteretic remanent magnetization (k _ARM) to the weak field magnetic susceptibility (k), k _ARM/k can be used to estimate the grain size of magnetite. The sediments and volcanic rocks yield values of 13.7 and 11.8 for the k _ARM/_k, respectively, corresponding to grain size values of ～0.03 µm and ～0.05 µm. The magnetic granulometry of lake sediments is distinctive from one of the Chinese loess, in which published data suggest a value of 6.0 for k _ARM/_k, and grain size of ～0.1 µm, but is akin to the nearby volcanic rocks. Although a Loess Plateau source of the lake sediments cannot be fully ruled out, the catchment is most probably the main source. We explain the slightly finer magnetite grain size in sediments than in the volcanic rocks as being disintegrated of particles during erosion and transportation. We conclude that there is no evidence for aeolian input of the Loess Plateau dusts into the Huguang Maar, and the relationship between magnetic parameters of the lake sediments and winter monsoon intensity is probably more complicated than previously thought.     

Rock-magnetic investigation of Siberia loess and its implication

Multiple-rock magnetic investigations conducted on the loess-paleosol sequences at Kurtak in Southwestern Siberia reveal that the mass-normalized low-field magnetic susceptibility profiles reflect changes in lithology between relatively unweathered primary loess of glacial periods and the interglacial paleosols. Maxima in susceptibility values correspond with the least-weathered loess horizons, and minima with the humic horizons of soils. Frequency-dependent susceptibility of the loess-paleosol sequences at Kurtak is very low and practically uniform, indicating the dominance of non-SP ferrimagnetic minerals and negligible pedogenesis. The history of temperature-dependence of susceptibility (TDS) and stepwise acquisition of the isothermal remanent magnetization (SIRM) have confirmed that magnetite is predominant magnetic mineral, and only few maghemite and probably hematite are present within the studied section. Anisotropy of the magnetic susceptibility (AMS) can be used to monitor tilt and disturbance of the sedimentary layers, and also to provide information about the paleo-transport direction for Siberia loess.     

Mineral magnetism of quaternary red earth in Eastern China and Its paleoenvironmental significance

Mineral magnetic measurements have been made on Quaternary Red Earth profiles from Zhejiang Province, Eastern China. Three distinctive magnetic stratigraphic horizons have been identified on the basis of magnetic susceptibility, anhysteretic remanent magnetization, saturation isothermal remanent magnetization and magnetization parameters measurements. Magnetic measurements revealed that there were great variations in ferrimagnetic mineral concentration, mineralogy assemblages and grain size in Quaternary Red Earth profiles, suggesting that these variations reflect pedogenic processes fluctuation and environmental changes. The preliminary results indicate that mineral magnetic measurement of Quaternary Red Earth is useful for studying the Quaternary environmental changes recorded in paleosols.     

东鞍山含碳酸盐铁矿石悬浮磁化焙烧试验

介绍了一种半工业试验用悬浮焙烧设备,并考察了焙烧温度、还原气体CO及流化气体N₂用量对东鞍山含碳酸盐铁矿石预富集粗精矿悬浮焙烧效果的影响.试验结果表明,在焙烧温度540℃,还原气体CO用量4m³/h及流化气体N₂用量2m³/h的条件下,焙烧物料经磨矿-磁选后可获得铁品位66.1%,回收率91.2%的铁精矿.铁的化学物相、光学显微结构及穆斯堡尔谱分析表明,经悬浮焙烧后弱磁性的菱铁矿和赤铁矿转化为了强磁性的磁铁矿,部分结晶粒度较粗(>100μm)的赤铁矿仅颗粒表面转变为磁铁矿,但这种Fe₂O₃@Fe₃O₄核壳结构的新生磁铁矿由于磁性较强,在后续磁选过程中依然能够得到有效的回收,并不会影响分选效果.     

甘氨酸燃烧法制备纳米晶CoFe2O4铁氧体及烧结温度对其磁性能的影响

利用甘氨酸作为燃料和配合剂, 采用自蔓延燃烧法制备纳米晶钴铁氧体, 并通过X射线衍射、 扫描电子显微镜和振动样品磁强计表征样品的结构和磁性能. 结果表明, 平均晶粒尺寸对样品的磁性能影响较大, 晶粒尺寸随烧结温度的变化而变化, 并得到了矫顽力H_c和比饱和磁化强度σ_s随烧结温度的变化曲线.      

铝对FeN薄膜结构和磁学特性的影响

铝的添加使ＦｅＮ薄膜变成非晶，并在ＦｅＡｌＮ薄膜中形成某些柱状物，材料粒度变小，ＦｅＡｌＮ薄膜矫顽力也变小．多层膜的效果，阻断了微粒沿垂直于膜面方向的生长，从而进一步降低其矫顽力．同时铝的添加，也增加了样品饱和磁化强度的热稳定性．     

Partial anhysteretic remanent magnetization （pARM） synthetic single- and multi-domain magnetites and its paleoenvironmental significance

In order to isolate magnetic signals carried by single-domain （SD） ferrimagnetic （FM） minerals from multi-domain （MD） FM minerals, we developed a few parameters using partial anhysteretic remanent magnetization （pARM）. Because MD fraction contains only soft （easy to be demagnetized） coercivity spectrum, pARM（〉20 mT） was sensitive in eliminating MD contributions. Ratio of pARM（5 mT, 10 mT）/pARM（0, 5 mT） is useful in quantifying a relative abundance of mass ratio between SD and MD fractions. These new proxies can quickly characterize the details of grain size distribution of magnetic minerals in paleoclimatic and paleomagnetic studies.     

Partial anhysteretic remanent magnetization (pARM) of synthetic single-and multidomain magnetites and its paleoenvironmental significance

Mineral magnetism is an inexpensive, efficient and non-destructive tool to decode paleoclimatic signals re- corded in natural sediments. However, this approach has often been hampered by its inherent complexities because the bulk magnetic signals could be contributed from a magnetic assemblage including both ferromagnetic (FM) (e.g., magnetite and/or maghemite) and antiferromagnetic minerals (AFM) (e.g., hematite and/or goethite) covering a wide range of grain size distribution. Therefore, t…     

La掺杂双钙钛矿Ba2NiMoO6的磁性和铁电性能

通过固相烧结工艺制备Ba2-xLaxNiMoO6(x=0,0.1)陶瓷样品,采用多晶X射线衍射仪和扫描电子显微技术对样品的物相成分、晶体结构及其表面形貌进行表征与分析.实验样品的X射线衍射谱与理论模拟多晶样品的X射线标准谱比较,显示样品相已经形成.X射线衍射分析结果表明,Ba2NiMoO6晶体原胞(a=b=c=0.8045 nm)属于立方晶系,空间群为Pm3m,布拉格衍射峰(1,1,1),(3,1,1)分别为样品中Ni离子和Mo离子有序占据B位超晶格有序峰,实验显示La掺杂对样品的晶胞参数影响很小.对样品铁电性能的测试表明,A位的替代增强了Ba2NiMoO6的偶极运动,使剩余极化得到提高.通过振动样品磁强计(VSM)测量样品磁化强度与磁场强度的关系,表明样品在室温下呈现顺磁行为.