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1.
用溅射技术制作γ-Fe2O3磁性薄膜,并通过透射电子显微镜观察磁性薄膜的电子显微像和选区电子衍射环,进行了γ-Fe2O3晶体结构分析,讨论了多晶薄膜的生长条件。  相似文献   

2.
本文报导了不同制备条件下四氧化三铁薄膜的结构和磁性。实验的关键制备是水蒸气和氩气的分压之比,其变化范围从1.0到3.0。透射电子显微镜研究表明了在不同的溅射条件下都可以得到结构均匀的薄膜。扫描隧道显微镜的观察清楚地显示了薄膜的表面的三维形貌。  相似文献   

3.
通过改变溅射功率,使用直流磁控溅射设备,在玻璃衬底上制备了系列Ti O2薄膜。分别用扫描电子显微镜、X射线衍射仪和椭偏光谱仪测试了Ti O2薄膜的形貌、结构及厚度。使用紫外-可见分光光度计测试了Ti O2薄膜的光学性能。使用Ti O2薄膜降解罗丹明B溶液测试了其光催化活性。研究结果表明:溅射功率增大,薄膜的透射谱及吸收谱在紫外出现明显的"红移"现象,光学带隙从3.51 e V减小到3.40 e V。适当提高溅射功率有利于提高Ti O2薄膜的光催化活性,当溅射功率为213 W时,薄膜的光催化性能最好。  相似文献   

4.
磁控溅射法制备PET基纳米TiO2抗菌薄膜的研究   总被引:5,自引:0,他引:5  
利用磁控反应溅射法在PET基底上制备了纳米TiO2抗菌薄膜。利用扫描电子显微镜(SEM)对制得的溅射膜的微观形貌进行了表征,发现采用磁控溅射法在很短的时间内即可在基底上得到一层致密均匀的由纳米粒子组成的薄膜。采用光—氧抗菌实验方法,研究了溅射薄膜的抗菌性能。实验结果表明溅射后的薄膜比未溅射样品具有明显的抗菌性能。  相似文献   

5.
常见的小型等离子溅射仪是配合中小型扫描电子显微镜制样必备的仪器。针对其辉光放电,对实验人员产生隐性紫外线伤害的问题,本文介绍了基于TiO2-SiO2薄膜的紫外反射膜的设计过程。通过优化获得了380nm~400nm近紫外波段具有高反射的溅射仪防护罩紫外隔离膜的参数,得出了最优化的膜层组合,为低成本地制备性能稳定、高可见光透射、高紫外线隔离的新型溅射仪防护罩紫外隔离膜提供了参考。  相似文献   

6.
利用磁控反应溅射法在PET基底上制备了纳米TiO2 抗菌薄膜。利用扫描电子显微镜(SEM)对制得的溅射膜的微观形貌进行了表征 ,发现采用磁控溅射法在很短的时间内即可在基底上得到一层致密均匀的由纳米粒子组成的薄膜。采用光 -氧抗菌实验方法 ,研究了溅射薄膜的抗菌性能。实验结果表明溅射后的薄膜比未溅射样品具有明显的抗菌性能  相似文献   

7.
利用磁控溅射法在BaF2(111)单晶衬底上生长了PhTe薄膜,通过原子力显微镜(AFM)、X射线衍射(XRD)、傅里叶红外透射谱(FTIR)表征了溅射PbTe/BaF2(111)薄膜的微结构和光学特性.测量结果显示:溅射生长的PbTe/BaF2(111)薄膜表面由规则金字塔形岛和三角形坑组成的纳米颗粒构成,且薄膜沿〈111〉取向择优生长,其晶粒大小与表面纳米颗粒大小接近.室温下傅里叶红外透射谱及其理论模拟表明溅射生长的PbTe薄膜光学吸收带隙(Eg=0.351eV)出现蓝移,与PbTe纳米晶粒的尺寸效应有关.  相似文献   

8.
常温下,利用射频(RF)反应磁控溅射方法在K9双面抛光玻璃基底上沉积氧化钛薄膜.采用光栅光谱仪对薄膜样品的透射谱进行测试,通过椭圆偏振光谱仪测试并拟合得到薄膜的厚度、折射率和消光系数等光学参数,借助掠入射角X-射线衍射对薄膜的结晶状态进行了测试.实验结果表明:不同溅射功率下沉积的样品呈非晶态,在40~100W范围内,溅射功率越大,薄膜的沉积速率越大,但溅射功率对折射率和消光系数影响不大.  相似文献   

9.
本采用室温转化法、分别用乙二胺与氨水做模板合成硒化银量子点,对合成的硒化银样品进行了X-射线衍射分析,并在透射电子显微镜下研究了模板对合成硒化银形态的影响.  相似文献   

10.
采用基于磁控等离子体团簇束流源的低能团簇束流沉积制备不同形态的Pb纳米颗粒薄膜。通过透射电子显微镜TEM对颗粒的尺寸、数密度进行表征分析,建立磁控等离子体团簇源及低能团簇束流沉积过程的可调参数——溅射气流、缓冲气流、溅射电压电流、沉积时间等与颗粒尺寸、数密度的对应关系,并通过对参数的调整优化获得Pb纳米颗粒薄膜中颗粒尺寸和数密度的独立调控。  相似文献   

11.
Language markedness is a common phenomenon in languages, and is reflected from hearing, vision and sense, i.e. the variation in the three aspects such as phonology, morphology and semantics. This paper focuses on the interpretation of markedness in language use following the three perspectives, i.e. pragmatic interpretation, psychological interpretation and cognitive interpretation, with an aim to define the function of markedness.  相似文献   

12.
The Williston Basin is a significant petroleum province, containing oil production zones that include the Middle Cambrian to Lower Ordovician, Upper Ordovician, Middle Devonian, Upper Devonian and Mississippian and within the Jurassic and Cretaceous. The oils of the Williston Basin exhibit a wide range of geochemical characteristics defined as "oil families", although the geochemical signature of the Cambrian Deadwood Formation and Lower Ordovician Winnipeg reservoired oils does not match any "oil family". Despite their close stratigraphic proximity, it is evident that the oils of the Lower Palaeozoic within the Williston Basin are distinct. This suggests the presence of a new "oil family" within the Williston Basin. Diagnostic geochemical signatures occur in the gasoline range chromatograms, within saturate fraction gas chromatograms and biomarker fingerprints. However, some of the established criteria and cross-plots that are currently used to segregate oils into distinct genetic families within the basin do not always meet with success, particularly when applied to the Lower Palaeozoic oils of the Deadwood and Winnipeg Formation.  相似文献   

13.
王慧 《科技信息》2008,(10):240-240
Wuthering Heights, Emily Bronte's only novel, was published in December of 1847 under the pseudonym Ellis Bell. The book did not gain immediate success, but it is now thought one of the finest novels in the English language. Catherine is the key character of this masterpiece, because everybody and everything center on her though she had a short life. We can understand this masterpiece better if we know Catherine well.  相似文献   

14.
The discovery of the prolific Ordovician Red River reservoirs in 1995 in southeastern Saskatchewan was the catalyst for extensive exploration activity which resulted in the discovery of more than 15 new Red River pools. The best yields of Red River production to date have been from dolomite reservoirs. Understanding the processes of dolomitization is, therefore, crucial for the prediction of the connectivity, spatial distribution and heterogeneity of dolomite reservoirs.The Red River reservoirs in the Midale area consist of 3~4 thin dolomitized zones, with a total thickness of about 20 m, which occur at the top of the Yeoman Formation. Two types of replacement dolomite were recognized in the Red River reservoir: dolomitized burrow infills and dolomitized host matrix. The spatial distribution of dolomite suggests that burrowing organisms played an important role in facilitating the fluid flow in the backfilled sediments. This resulted in penecontemporaneous dolomitization of burrow infills by normal seawater. The dolomite in the host matrix is interpreted as having occurred at shallow burial by evaporitic seawater during precipitation of Lake Almar anhydrite that immediately overlies the Yeoman Formation. However, the low δ18O values of dolomited burrow infills (-5.9‰~ -7.8‰, PDB) and matrix dolomites (-6.6‰~ -8.1‰, avg. -7.4‰ PDB) compared to the estimated values for the late Ordovician marine dolomite could be attributed to modification and alteration of dolomite at higher temperatures during deeper burial, which could also be responsible for its 87Sr/86Sr ratios (0.7084~0.7088) that are higher than suggested for the late Ordovician seawaters (0.7078~0.7080). The trace amounts of saddle dolomite cement in the Red River carbonates are probably related to "cannibalization" of earlier replacement dolomite during the chemical compaction.  相似文献   

15.
何延凌 《科技信息》2008,(4):258-258
Language is a means of verbal communication. People use language to communicate with each other. In the society, no two speakers are exactly alike in the way of speaking. Some differences are due to age, gender, statue and personality. Above all, gender is one of the obvious reasons. The writer of this paper tries to describe the features of women's language from these perspectives: pronunciation, intonation, diction, subjects, grammar and discourse. From the discussion of the features of women's language, more attention should be paid to language use in social context. What's more, the linguistic phenomena in a speaking community can be understood more thoroughly.  相似文献   

16.
Location based services is promising due to its novel working style and contents.A software platform is proposed to provide application programs of typical location based services and support new applications developing efficiently. The analysis shows that this scheme is easy implemented, low cost and adapt to all kinds of mobile nework system.  相似文献   

17.
以AC-13级配为基础,将橡胶颗粒代替部分集料掺入混合料中,以低温弯曲试验为评价方法对不同橡胶颗粒掺量下沥青混合料的低温抗裂性进行研究,并引入应变能密度值对混合料的低温抗裂性进行综合评价.试验结果表明:橡胶颗粒沥青混合料试件的破坏微应变均超过2 300,满足冬寒区的技术指标;无论是否掺加橡胶颗粒,随着温度的下降,沥青混合料破坏时的最大弯拉强度增大,弯拉应变降低,劲度模量增大;弯曲应变能密度在胶粒掺量为1%左右时具有较大的弯曲应变能密度值,此时橡胶颗粒沥青混合料具有较好的低温抗裂性.  相似文献   

18.
AcomputergeneratorforrandomlylayeredstructuresYUJia shun1,2,HEZhen hua2(1.TheInstituteofGeologicalandNuclearSciences,NewZealand;2.StateKeyLaboratoryofOilandGasReservoirGeologyandExploitation,ChengduUniversityofTechnology,China)Abstract:Analgorithmisintrod…  相似文献   

19.
理论推导与室内实验相结合,建立了低渗透非均质砂岩油藏启动压力梯度确定方法。首先借助油藏流场与电场相似的原理,推导了非均质砂岩油藏启动压力梯度计算公式。其次基于稳定流实验方法,建立了非均质砂岩油藏启动压力梯度测试方法。结果表明:低渗透非均质砂岩油藏的启动压力梯度确定遵循两个等效原则。平面非均质油藏的启动压力梯度等于各级渗透率段的启动压力梯度关于长度的加权平均;纵向非均质油藏的启动压力梯度等于各渗透率层的启动压力梯度关于渗透率与渗流面积乘积的加权平均。研究成果可用于有效指导低渗透非均质砂岩油藏的合理井距确定,促进该类油藏的高效开发。  相似文献   

20.
Quality traits in wheat (Triticum aestirum L.) were studied by quantitative trait locus (QTL) analysis in a recombinant inbred line (RIL) population, a set of 131 lines derived from Chuan 35050 × Shannong 483 cross (ChSh). Grains from RILs were assayed for 21 quality traits related to protein and starch. A total of 35 putative QTLs for 19 traits with a single QTL explaining 7.99-40.52% of phenotypic variations were detected on 10 chromosomes, 1D, 2A, 2D, 3B, 3D, 5A, 6A, 6B, 6D, and 7B. The additive effects of 30 QTLs were positive, contributed by Chuan 35050, the remaining 5 QTLs were negative with the additive effect contributed by Shannong 483. For protein traits, 15 QTLs were obtained and most of them were located on chromosomes 1 D, 3B and 6D, while 20 QTLs for starch traits were detected and most of them were located on chromosomes 3D, 6B and 7B. Only 7 QTLs for protein and starch traits were co-located in three regions on chromosomes 1D, 2A and 2D. These protein and starch trait QTLs showed a distinct distribution pattern in certain regions and chromosomes. Twenty-two QTLs were clustered in 6 regions of 5 chromosomes. Two QTL clusters for protein traits were located on chromosomes 1D and 3B, respectively, three clusters for starch traits on chromosomes 3D, 6B and 7B, and one cluster including protein and starch traits on chromosome 1D.  相似文献   

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