浓相气固两相流质量浓度摩擦电法测量研究

研究了一种气固两相流质量浓度在线实时检测的测量方法———摩擦电法 .推导了固体颗粒与管壁摩擦产生的电流与气固两相流固相质量浓度、气体平均流速以及固相颗粒大小间的关系 .以煤粉为研究对象进行实验研究 ,煤粉质量浓度在 1 7～ 45g/m3 、气体速度在 3～ 7m/s范围内 ,测量段产生的电流和气体流速、颗粒质量流量关系为 Im =4.92× 1 0 -11 u1.77W ,实验数据与理论计算基本符合 ,误差分析表明其测量误差为 2 0 % ,从而也验证了摩擦电法的可行性 .     

液态金属钠在环管热进口段的湍流传热研究

本文对液态金属钠在环管热进口段部分的湍流传热做了实验研究.实验的主要特性参数如下:环形通道之直径比 d_2/d_1=1.54;热流密度 q=50W/cm~2;雷诺数Re=2×10~4～1.5×10~5;伯克利数 Pe=122～1078.分析表明,实验值与理论值吻合良好.最后,分别给出稳定段和热进口段的努谢尔特数以及热进口段长度的计算式.     

二氧化锡修饰碳糊电极检测过氧化氢的研究

利用二氧化锡修饰碳糊电极开展过氧化氢的检测.采用循环伏安法和电流-时间曲线法对H2O2进行测定.研究磷酸缓冲溶液的pH、二氧化锡修饰含量等因素对该修饰电极测定H2O2的影响.在优化实验条件(pH=5.7,SnO2与石墨的质量比为1∶5)下,H2O2检测线性范围在1.0×10-5～2.19×10-3 mol.L-1内,还原峰电流与H2O2浓度呈良好线性关系.检测限为2.5×10-6mol.L-1(S/N=3).该传感器具有制备简易、成本低廉、响应快、灵敏度高、稳定性好等特点,具有较好的应用前景.     

管内沸腾临界热负荷的实验研究

文中簡述了管內沸騰临界热負荷的研究現狀,介紹了作者采用的試驗裝置和方法,列出除气蒸餾水向上流过垂直不銹鋼管时的沸騰临界热負荷的試驗数据,提出經驗关系式,分析主要因素的影响,并与其他作者的数据进行比較。試驗在以下参数范圍內进行: 实驗段出口压力:1.2～1.5工程大气压实驗段出口欠热度:5～35℃流速:0.25～8米/秒热負荷:1.0×10~6～8.5×10~6大卡/米~2的实驗段材料:1X18 H9T不銹鋼管管径:(內径×厚度)4×1;6×1;9×1.5毫米管長:105毫米管长/管内径=l/d内:26.2,17.5,11.7(都大于10)在上述条件下整理成經驗关系式: gKP=0.65×10~6(1+w)~(09)(1+Δt_H)~(0.23) (1) 实驗点与經驗关系式最大偏差小于±18％,其中93％点最大偏差≤±10％。     

n-C_(10)H_(22)和n-C_(12)H_(26)的热压力系数及内压

本文测定了n-C_(10)H_(22)和n-C_(12)H_(26)在20—55℃的热压力系数。这些系数可用修正的van der Waals模型来描述式中A和B是液体的特性常数。对于n-C_(10)H_(22):A=339.40×10~(-6)m~3mol~(-1),B=29822×10~(-12)m~6mol~(-2)。对于n-C_(12)H_(26):A=403.06×10~(-6)m~3mol~(-1),B=41818×10~(-12)m~6mol~(-2)。与一般小分子液体和少于八个碳的正构烷不同,它们的B/A~2不再等于0.2610,而是随着碳链的增长而逐渐减小。     

仲壬基苯氧基乙酸基本常数的测定

利用两相滴定法在(25±0 5)℃下测定了仲壬基苯氧基乙酸(CA-100)在水中的溶解度S,离解常数Ka,以及庚烷中的二聚常数K2和水-庚烷两相间的分配常数Kd.实验测得S=1 30×10-4mol/L,Ka=2 94×10-4,K2=3 29×102,Kd=4 15×102.     

离子对反相高效液相色谱法测定VB2,VB6,VB12,VC和叶酸

建立了用离子对反相高效液相色谱法同时测定VB2,VB6,VB12,VC和叶酸含量的方法.用HypersilC18色谱柱(ODS2,5 μm,4.6 mm×150 mm,),V(甲醇)V(0.5%醋酸溶液)=3070,其中每升流动相加入2.5 mmol的戊烷磺酸钠作为流动相.柱温30℃时于254 nm波长处以外标法测定.结果表明VB2,VB6,VB12,VC和叶酸的浓度与峰高成良好的线性关系.VB2的线性范围为2.0×10-7～8.0×10-6g/mL(r=0.999 8),VB6的线性范围为2.0×10-6～5.0×10-4g/mL(r=0.999 0),VB1 2的线性范围为2.0×10-7～8.0×10-4g/mL(r=0.999 9),叶酸的线性范围为2.0×10～5.0×10-5g/mL(r=0.998 7),VC的线性范围为5.0×10-7～8.0×10-5g/mL(r=0.999 1).VB2,VB6,VB12,VC和叶酸的检测限分别为6×10-9g/mL,6×10-8g/mL,7×10-9g/mL,1×10-9g/mL和6×10-8g/mL实验表明该法准确,快捷,操作简便,应用于蜂蜜和复合维生素片中维生素的测定,取得了很好的结果.     

PF胶杨木大片刨花板喷蒸真空热压的工艺优化

以饱和蒸汽压力、喷蒸时间、蒸汽保持时间和抽真空时间为变量因子 ,利用BY60 2× 4喷蒸试验压机 ,采用二次数学模型D =4近似饱和最优设计及复合型法 ,研究了水溶性A阶PF胶杨木大片刨花板的喷蒸真空热压工艺 ,求得回归方程 ,进行工艺优化。所得回归方程的预测偏差小 ,可用于预测刨花板性能。     

V型喷动流化床床层压力的研究

流化床床层压力及其分布是反映流化质量和床内物料运动状况的主要参数之一。本实验在于３１０×４０×２０００ｍｍ和８３×４０００ｍｍＶ型喷动流化床冷模装置上，以水泥生料粉为实验原料，对床层压力、缩口结构与流化质量关系进行了研究，分析了床层压降随喷射气流、流化气流的变化规律，并与普通流化床的类似特性作了比较，得出Ｖ型喷动流化床的适宜操作气速范围。流化浅床加上合理的缩口形状，可以实现层流边界层连续卸料的操作。     

保济丸中厚朴酚浓度的HPLC 法测定

HPLC法测定了不同产地保济丸中厚朴酚浓度.考察了样品制备方法、流动相系统、检测波长等因素对分析结果的影响.色谱柱为HypersilODS(4 6mm×150mm)不锈钢柱;以甲醇-水(V∶V=30∶70)为流动相;流速1mL/min,检测波长为294nm;进样量10μL.研究结果表明厚朴酚和其它组分可达基线分离,厚朴酚质量浓度在8×10-2～8×10-1mg/mL内线性关系良好(r=0 9979).保济丸中厚朴酚的回收率为99 46%,RSD为1 78%.     

Markedness and its Interpretation in Language Use

Language markedness is a common phenomenon in languages, and is reflected from hearing, vision and sense, i.e. the variation in the three aspects such as phonology, morphology and semantics. This paper focuses on the interpretation of markedness in language use following the three perspectives, i.e. pragmatic interpretation, psychological interpretation and cognitive interpretation, with an aim to define the function of markedness.     

Features of Women's language

Language is a means of verbal communication. People use language to communicate with each other. In the society, no two speakers are exactly alike in the way of speaking. Some differences are due to age, gender, statue and personality. Above all, gender is one of the obvious reasons. The writer of this paper tries to describe the features of women＇s language from these perspectives： pronunciation, intonation, diction, subjects, grammar and discourse. From the discussion of the features of women＇s language, more attention should be paid to language use in social context. What＇s more, the linguistic phenomena in a speaking community can be understood more thoroughly.     

An Analysis of Catherine＇s Character——Wuthering Heights

Wuthering Heights, Emily Bronte＇s only novel, was published in December of 1847 under the pseudonym Ellis Bell. The book did not gain immediate success, but it is now thought one of the finest novels in the English language. Catherine is the key character of this masterpiece, because everybody and everything center on her though she had a short life. We can understand this masterpiece better if we know Catherine well.     

Lower Paleozoic oil relationships within Williston Basin, Canada

The Williston Basin is a significant petroleum province, containing oil production zones that include the Middle Cambrian to Lower Ordovician, Upper Ordovician, Middle Devonian, Upper Devonian and Mississippian and within the Jurassic and Cretaceous. The oils of the Williston Basin exhibit a wide range of geochemical characteristics defined as "oil families", although the geochemical signature of the Cambrian Deadwood Formation and Lower Ordovician Winnipeg reservoired oils does not match any "oil family". Despite their close stratigraphic proximity, it is evident that the oils of the Lower Palaeozoic within the Williston Basin are distinct. This suggests the presence of a new "oil family" within the Williston Basin. Diagnostic geochemical signatures occur in the gasoline range chromatograms, within saturate fraction gas chromatograms and biomarker fingerprints. However, some of the established criteria and cross-plots that are currently used to segregate oils into distinct genetic families within the basin do not always meet with success, particularly when applied to the Lower Palaeozoic oils of the Deadwood and Winnipeg Formation.     

低渗透非均质砂岩油藏启动压力梯度研究

理论推导与室内实验相结合,建立了低渗透非均质砂岩油藏启动压力梯度确定方法。首先借助油藏流场与电场相似的原理,推导了非均质砂岩油藏启动压力梯度计算公式。其次基于稳定流实验方法,建立了非均质砂岩油藏启动压力梯度测试方法。结果表明:低渗透非均质砂岩油藏的启动压力梯度确定遵循两个等效原则。平面非均质油藏的启动压力梯度等于各级渗透率段的启动压力梯度关于长度的加权平均;纵向非均质油藏的启动压力梯度等于各渗透率层的启动压力梯度关于渗透率与渗流面积乘积的加权平均。研究成果可用于有效指导低渗透非均质砂岩油藏的合理井距确定,促进该类油藏的高效开发。     

On Tragic Consciousness In The Works By Ernest Hemingway

As an American modern novelist who were famous in the literary world, Hemingway was not a person who always followed the trend but a sharp observer. At the same time, he was a tragedy maestro, he paid great attention on existence, fate and end-result. The dramatis personae's tragedy of his works was an extreme limit by all means tragedy on the meaning of fearless challenge that failed. The beauty of tragedy was not produced on the destruction of life, but now this kind of value was in the impact activity. They performed for the reader about the tragedy on challenging for the limit and the death.     

Design and analysis of generic LBS application developing platform

Location based services is promising due to its novel working style and contents.A software platform is proposed to provide application programs of typical location based services and support new applications developing efficiently. The analysis shows that this scheme is easy implemented, low cost and adapt to all kinds of mobile nework system.     

Achieving Unusual States of Matter Under High Pressure

正The periodicity of the elements and the non-reactivity of the inner-shell electrons are two related principles of chemistry,rooted in the atomic shell structure.Within compounds,Group I elements,for example,invariably assume the+1 oxidation state,and their chemical properties differ completely from those of the p-block elements.These general rules govern our understanding of chemical structures and reactions.Using first principles calcula-     

Exchange-Correlation and Electronic Excitation Energies from Pairing Matrix Fluctuations

We have developed an adiabatic connection to formulate the ground-state exchange-correlation energy in terms of pairing matrix linear fluctuations.This formulation of the exchange-correlation energy opens a new channel for density functional approximations based on the many-body perturbation theory.We illustrate the potential of such approaches with an approximation based on the particle-particle Random Phase Approximation(pp-RPA).This re-     

Density Functional Theory for the Response of Periodic Systems to Electric Fields Based on the Vector Potential Approach

正The electronic and nuclear(structural/vibrational)response of 1D-3D nanoscale systems to electric fields gives rise to a host of optical,mechanical,spectral,etc.properties that are of high theoretical and applied interest.Due to the computational difficulty of treating such large systems it is convenient to model them as infinite and periodic(at least,in first approximation).The fundamental theoretical/computational problem in doing so is that