往复冲击式低温粉碎技术制备中药超细粉体

分析了现有的各种具有代表性中药超细粉碎技术中存在的问题,并提出改进思路.在此基础上,结合低温冷脆性原理,开发了新型的中药粉碎技术--"往复冲击式低温粉碎技术",试验得到了该技术主要操作参数--破碎时间、球罐往复频率、球罐往复行程、球罐内钢球填充率、球料比以及钢球直径等--对粉碎效果的影响规律.试验结果表明:经过12分钟粉碎,对于难粉碎的木本类植物根茎,粒径小于5微米的颗粒质量分数可迭70%;对于较难粉碎的草本类植物根茎,粒径小于5微米的颗粒质量分数可达98%;对于易粉碎的花、叶类植物,粒径小于2微米的颗粒质量分数可达97%,且各种中药极限粒径均达到0.1微米以下.     

往复冲击式低温粉碎技术制备中药超细粉体

分析了现有的各种具有代表性中药超细粉碎技术中存在的问题,并提出改进思路。在此基础上,结合低温冷脆性原理,开发了新型的中药粉碎技术——“往复冲击式低温粉碎技术”,试验得到了该技术主要操作参数——破碎时间、球罐往复频率、球罐往复行程、球罐内钢球填充率、球料比以及钢球直径等——对粉碎效果的影响规律。试验结果表明：经过12分钟粉碎,对于难粉碎的木本类植物根茎,粒径小于5微米的颗粒质量分数可达70%；对于较难粉碎的草本类植物根茎,粒径小于5微米的颗粒质量分数可达98%；对于易粉碎的花、叶类植物,粒径小于2微米的颗粒质量分数可迭97%,且各种中药极限粒径均达到0．1微米以下。     

1.5T MR弥散加权成像评价肝纤维化的临床应用

评价3.0TMR弥散加权成像在肝纤维化诊断中的临床意义。选取2012年1月至2015年7月收治的45例肝纤维化患者为观察组,同时取同期健康体检者30名作为对照组,对所有研究对象行DWI检查,并对检查结果进行分析比较,以评价DWI在肝纤维化诊断与评估中的临床意义。肝纤维化组ADC值为(1.18~2.01)×10-3mm2/s,平均为(1.59±0.23)×10-3mm2/s;正常对照组ADC值为(1.75~2.25)×10-3mm2/s,平均为(2.05±0.23)×10-3mm2/s,组间比较存在显著性差异(P0.05)。F1、F2、F3、F4的平均ADC值分别为(1.78±0.31)×10-3mm2/s、(1.58±0.25)×10-3mm2/s、(1.40±0.19)×10-3mm2/s、(1.23±0.14)×10-3mm2/s,随着肝纤维化分级的增高,平均ADC值不断下降,组间比较存在显著性差异(P0.05)。DWI在肝纤维化的诊断和评估中具有较高的应用价值,可做为一种高效准确的影像学检查方法在临床加以推广应用。     

10-bit 100-Ms/s视频模拟前端IP核的设计

设计了一个10 bit,100 Ms/s视频模拟前端IP核,并用台积电(TSMC)0.18μm 1.8/3.3 V互补金属氧化物半导体(CMOS)纯数字工艺进行了仿真.电路中模拟部分采用3.3 V电源电压,仿真结果显示当输入信号为18 MHz,信号幅度为满幅(单端1 V,差分2 V)时,输出信号信号-噪声-失真比(SNDR)为60 dB.整个电路的功耗为73 mA,版图面积为2 mm×2.5 mm.     

10 GHz低相噪扩频时钟发生器的设计与实现

基于55nm CMOS工艺设计并制造了一款小数分频锁相环低相噪10GHz扩频时钟发生器(SSCG).该SSCG采用带有开关电容阵列的压控振荡器实现宽频和低增益,利用3阶MASHΔΣ调制技术对电路噪声整形降低带内噪声,使用三角波调制改变分频系数使扩频时钟达到5 000×10~(-6).测试结果表明:时钟发生器的中心工作频率为10GHz,扩频模式下峰值降落达到16.46dB;在1 MHz频偏处的相位噪声为-106.93dBc/Hz.芯片面积为0.7mm×0.7mm,采用1.2V的电源供电,核心电路功耗为17.4mW.     

一种失调电压补偿电容比例型带隙基准源设计

设计了一种全新的电容比例型带隙基准源,用电容比例取代了通常的电阻比例,有效地减小了电路设计误差以及电路的功耗,理论失调电压可获补偿.电路采用Cadence Spectre软件仿真,Charter 0.35μm CMOS工艺库实现.仿真结果表明,该电路具有极低的电路功耗(8μW),其直流电源抑制比PSRR达到50 dB,温度系数为3×10-5V/℃.     

H2O2-荧光素化学发光体系测定没食子酸

基于在碱性条件下,没食子酸对H2O2-荧光素体系化学发光反应具有明显的增敏作用,建立了流动注射化学发光测定没食子酸的分析方法,并探讨了可能的发光机理.在优化的实验条件下,没食子酸在4.0×10-7～1.0×10-4 g/mL范围内与发光强度呈现良好的线性关系,检出限为5.83×10-7 g/mL,11次平行测定6.0×10-6 g/mL没食子酸的相对标准偏差为1.50%,该方法应用于健民咽喉片以及中药五倍子的测定,结果令人满意.     

毛细管电泳-安培检测法同时测定白藜芦醇及虎杖甙

采用毛细管电泳-电化学检测技术(CE-ECD)对白藜芦醇及虎杖甙进行分离检测.采用柱端喷壁式安培检测方式,在最佳分离条件下,2待测物在12 m in以内完全分离.白藜芦醇和虎杖甙分别在1.2×10-6~1.0×10-4mol/L与6.0×10-7~5.0×10-5mol/L浓度范围内与峰电流成良好的线性关系,检测下限分别为1.6×10-7和2.3×10-7mol/L.将该体系用于中药虎杖、中成药护肝宁片及市售红葡萄酒的分析和回收实验,测定结果令人满意.     

表面活性剂对瓦斯水合物生成诱导时间影响

为了揭示表面活性剂在瓦斯水合物生成过程的促进作用规律,利用可视化水合物实验设备,研究了5组表面活性剂溶液体系(T40,1.0×10-3 mol·L-1;T80,1.0×10-3 mol·L-1;T40/T80,1.0×10-3 mol·L-1;SDS,10.0×10-3 mol·L-1;SDBS,2.0×10-3 mol·L-1)中瓦斯水合物的生成过程,运用直接观测法测定了水合物生长的广义诱导时间,结合建立的水合物诱导时间模型对实验数据进行了计算和分析.结果表明:表面活性剂的加入降低了溶液的表面张力,促进了烷烃类气体溶解,加快了晶核形成过程,缩短了水合物生成的诱导时间.该成果对运用水合物技术储运瓦斯具有一定理论价值.     

嵌入式高速低功耗ROM设计研究

提出了一种改进的单相钟控的并联型ROM电路 ,该结构缩小了位线的电压摆幅 ,使电路速度提高 ,功耗降低 ,周边接口规整 ,连接方便 ,特别适合作为嵌入式ROM集成于片上系统 (SOC)中 .用 0 6 μmCMOS标准工艺设计了 1k× 2 8bitROM ,并嵌入微处理器芯片设计中 .模拟和流片结果表明 ,该ROM的读取时间小于等于 12ns ,功耗约为 0 82mW /MHz ,面积为 (0 6 4× 0 6 3)mm2 .     

Markedness and its Interpretation in Language Use

Language markedness is a common phenomenon in languages, and is reflected from hearing, vision and sense, i.e. the variation in the three aspects such as phonology, morphology and semantics. This paper focuses on the interpretation of markedness in language use following the three perspectives, i.e. pragmatic interpretation, psychological interpretation and cognitive interpretation, with an aim to define the function of markedness.     

低渗透非均质砂岩油藏启动压力梯度研究

理论推导与室内实验相结合,建立了低渗透非均质砂岩油藏启动压力梯度确定方法。首先借助油藏流场与电场相似的原理,推导了非均质砂岩油藏启动压力梯度计算公式。其次基于稳定流实验方法,建立了非均质砂岩油藏启动压力梯度测试方法。结果表明:低渗透非均质砂岩油藏的启动压力梯度确定遵循两个等效原则。平面非均质油藏的启动压力梯度等于各级渗透率段的启动压力梯度关于长度的加权平均;纵向非均质油藏的启动压力梯度等于各渗透率层的启动压力梯度关于渗透率与渗流面积乘积的加权平均。研究成果可用于有效指导低渗透非均质砂岩油藏的合理井距确定,促进该类油藏的高效开发。     

On Tragic Consciousness In The Works By Ernest Hemingway

As an American modern novelist who were famous in the literary world, Hemingway was not a person who always followed the trend but a sharp observer. At the same time, he was a tragedy maestro, he paid great attention on existence, fate and end-result. The dramatis personae's tragedy of his works was an extreme limit by all means tragedy on the meaning of fearless challenge that failed. The beauty of tragedy was not produced on the destruction of life, but now this kind of value was in the impact activity. They performed for the reader about the tragedy on challenging for the limit and the death.     

Achieving Unusual States of Matter Under High Pressure

正The periodicity of the elements and the non-reactivity of the inner-shell electrons are two related principles of chemistry,rooted in the atomic shell structure.Within compounds,Group I elements,for example,invariably assume the+1 oxidation state,and their chemical properties differ completely from those of the p-block elements.These general rules govern our understanding of chemical structures and reactions.Using first principles calcula-     

Exchange-Correlation and Electronic Excitation Energies from Pairing Matrix Fluctuations

We have developed an adiabatic connection to formulate the ground-state exchange-correlation energy in terms of pairing matrix linear fluctuations.This formulation of the exchange-correlation energy opens a new channel for density functional approximations based on the many-body perturbation theory.We illustrate the potential of such approaches with an approximation based on the particle-particle Random Phase Approximation(pp-RPA).This re-     

Density Functional Theory for the Response of Periodic Systems to Electric Fields Based on the Vector Potential Approach

正The electronic and nuclear(structural/vibrational)response of 1D-3D nanoscale systems to electric fields gives rise to a host of optical,mechanical,spectral,etc.properties that are of high theoretical and applied interest.Due to the computational difficulty of treating such large systems it is convenient to model them as infinite and periodic(at least,in first approximation).The fundamental theoretical/computational problem in doing so is that     

On the Thermodynamic Limit for Responses to Static Electromagnetic Fields

For molecular systems,the quantum-mechanical treatment of their responses to static electromagnetic fields usually employs a scalar-potential treatment of the electric field and a vector-potential treatment of the magnetic field.Although the potential for each field separately is associated with the choice of an(unphysical)origin,the precise choice of the origin for the electrostatic field has little consequences for the results.This is different for the     

An affordable accurate evaluation of the binding conformations predicted by molecular docking studies in bio-system

Franck-Condon factors bridge the gap between theoretical modeling and experimental observations for molecular electronic spectroscopy and electron transfer.Under the displaced harmonic oscillator approximation,multidimensional Franck-Condon factors are decomposed into a product of many one-dimensional(1D)Franck-Condon(FC)factors,and each 1D-FC factor is associated with one Huang-Rhys factor that determines the leading contribution of     

Call for Papers

<正>"The Journal of Shanghai Normal University:Mathematics"is published by Shanghai Normal University as regular issues of The Journal of Shanghai Normal University each year from 2014 in English.The editors-in-chief of the issues are professors Yuhao Cong and Maoan Han.The Journal of Shanghai Normal University was started in 1958 with     

Journal of Donghua University ( English Edition) Contents of Volume 31

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