A study of interparticulate strain in a hot-extruded SiC_p/2014 Al composite

We report a correlative study of strain distribution and grain structure in the Al matrix of a hot-extruded SiC particulate-reinforced Al composite(SiC_p/2014 Al). Finite element method(FEM) simulation and microstructure characterization indicate that the grain structure of the Al matrix is affected by the interparticulate strain distribution in the matrix during the process. Both electron-backscattered diffraction(EBSD) and selected-area electron diffraction(SAED) indicated localized misorientation in the Al matrix after hot extrusion. Scanning transmission electron microscopy(STEM) revealed fine and recrystallized grains adjacent to the Si C particulate and elongated grains between the particulates. This result is explained in terms of recrystallization under an interparticulate strain distribution during the hot extrusion process.     

大尺寸多层喷射沉积6066Al/SiCp/Gr 复合材料管坯的制备

采用多层喷射沉积技术与双喷嘴雾化系统制备了外径为650mm，内径为300mm，长为800mm的大尺寸6066Al/SiC     

热处理对SiCp/Al 2124复合材料显微组织与耐蚀性的影响

为提高SiC颗粒增强铝基复合材料Al2124的耐蚀性,采用X射线衍射、扫描电镜和电化学测试等手段,研究了3种热处理工艺（T1,T4和T6）对复合材料中第二相化合物的析出状况以及该材料在NaCl水溶液中的腐蚀行为的影响。结果表明,在T1状态下,铝合金基体内及SiCp/铝合金界面上析出大量以CuAl     

Microstructure and mechanical properties of a hot-extruded Al-based composite reinforced with core-shell-structured Ti/Al3Ti

An Al-based composite reinforced with core-shell-structured Ti/Al3Ti was fabricated through a powder metallurgy route followed by hot extrusion and was found to exhibit promising mechanical properties. The ultimate tensile strength and elongation of the composite sintered at 620°C for 5 h and extruded at a mass ratio of 12.75:1 reached 304 MPa and 14%, respectively, and its compressive deformation reached 60%. The promising mechanical properties are due to the core-shell-structured reinforcement, which is mainly composed of Al3Ti and Ti and is bonded strongly with the Al matrix, and to the reduced crack sensitivity of Al3Ti. The refined grains after hot extrusion also contribute to the mechanical properties of this composite. The mechanical properties might be further improved through regulating the rela-tive thickness of Al-Ti intermetallics and Ti metal layers by adjusting the sintering time and the subsequent extrusion process.     

准脆性SiC_p/Al复合材料SHPB实验中入射波整形技术

针对陶瓷体积分数为50%的准脆性SiCp/Al复合材料恒应变率动态压缩实验,研究了入射波整形原则和理想入射波设计方法.结果表明:采用原始透射波和修正后反射波叠加设计的新入射波,通过控制整形器尺寸和子弹初速获得了理想的入射波,实现对准脆性复合材料的恒应变率加载;以测试材料力学特性为基础设计的整形器,可调整入射波形使之与透射波具有相同形状.针对准脆性SiCp/Al复合材料,SHPB实验中应变率只取决于入射波的幅值,而与整形后的入射波加载率关系不大,入射波中平台段实现试样的恒应变率变形;入射波形设计成梯形波,使之与SiCp/Al复合材料的透射波波形相似,实现了对复合材料的恒应变率加载.     

SiCp/Al切削表面层力学物理性能研究

通过切削试验研究,从宏观和微观的角度探讨了SiCp/Al材料本身微观组织结构,切削力,切削温度等因素对已加工表面层硬度和表面残余应力的影响.试验结果表明已加工表面层硬度和残余应力是各种因素叠加作用的结果,最高硬度值出现在次表层,切削温度升高使表面具有拉应力和加工软化的倾向增大,表面层塑性变形增大使表面残余压应力和加工硬化的倾向增大.     

双连续相SiC/Al复合材料压渗工艺初探

为了充分发挥陶瓷和金属的各自优势 ,同时避免它们的各自劣势 ,文章采用鲜有报道的多孔陶瓷骨架压渗工艺制备双连续相金属 /陶瓷复合材料。首先采用有机泡沫浸渍法制备 Si C多孔陶瓷骨架 ,然后将纯金属 A l压渗到骨架中 ,为了改善压渗效果 ,还对助渗剂进行研究。结果表明 ,纯金属 A l可以压渗进入陶瓷骨架中 ,使用助渗剂可得到更好的效果。该材料应用前须进一步改善压渗工艺 ,并选择合适的压渗合金     

封装SiCp/Cu复合材料组织性能研究

采用粉末冶金法制备SiC体积分数分别为20%、35%、50%的SiCp/Cu复合材料,并采用扫描电镜、热膨胀仪、热分析仪、洛氏硬度计等对其显微组织、热物理性能和力学性能进行表征。结果表明,随着SiCP含量升高,偏聚现象趋于明显,SiCp/Cu复合材料热导率减小,分别为167、145、130W/m·K,SiCp/Cu复合材料热膨胀系数分别为10.2×10-6、8.6×10-6、9.6×10-6 K-1,呈先减小后增大趋势;在SiCp/Cu复合材料中,当SiC体积分数小于35%时,其硬度值变化取决于SiCp含量,当SiC体积分数大于35%时,其硬度值取决于致密度。     

激光诱导氧化辅助铣削SiCp/Al复合材料试验研究

为了提高碳化硅颗粒增强铝基复合材料(SiCp/Al)的切削加工性,本文提出了一种激光诱导氧化辅助铣削的复合加工方法。在激光参数为平均功率10 W,扫略速度为2 mm/s,扫略间距为10 μm的条件下,能够获得疏松多孔氧化层,从而提高加工效率和加工质量。本文主要研究该材料在激光辐照下的氧化机理,以及铣削过程中铣削参数对切削力和表面完整性的影响规律。在铣削深度为0.1 mm,每齿进给量为0.005 mm/z时,加工质量最佳。     

SiC/Al电子封装材料的制备工艺研究

对用无压浸渗法制备高体积分数的SiC／Al复合材料的浸渗过程进行了分析。结果表明：温度在900～1100℃之间变化时，随着温度的升高浸渗深度增加；充分的浸渗时间可提高界面的润湿性，促使铝合金液顺利浸渗；Mg量为10%时浸渗能顺利进行；N2作为保护气氛，不但可以防止氧化，而且可以促进铝合金液对SiC颗粒的浸渗。     

TiC/TiN/Al2O3复合陶瓷的研究进展

文章综述了TiC/TiN/Al2O3复合陶瓷的研究进展,介绍了复合陶瓷的制备工艺、组织与性能,探讨了材料成分对组织和力学性能的影响,总结了复合陶瓷的增韧机制及在刀具上的应用情况,指出纳米复合陶瓷是进一步改善强韧性的主要发展方向,为氧化铝陶瓷的广泛应用丰富了科学内涵.     

纳米ZTM／Al2O3复相陶瓷材料抗热震损伤性能

简要分析了表述复相陶瓷材料的抗热震损伤的一些机理。并且利用典型的湿化学法制备了两种ZTM／Al2O3复相陶瓷材料;晶间型和纳米／纳米型;分别对高温和低温深冷条件下,两种不同结构材料的抗热震损伤性能进行了研究。结果表明:对ZTM／Al2O3复相陶瓷材料,高温热冲击下,纳米／纳米型材料的残余强度的衰减变化大于晶间型材料;晶间型材料的抗热冲击性能优于纳米／纳米型材料。低温深冷条件下,晶间型材料由于ZrO2马氏体相变的失效和残余微量玻璃相的脆化,表现出与普通耐火材料相似的残余强度衰变趋势,而纳米／纳米型材料却呈现与高温热冲击条件下相似的变化趋势。     

Microstructure and mechanical properties of a hot-extruded Al-based composite reinforced with core-shell-structured Ti/Al3Ti

An Al-based composite reinforced with core-shell-structured Ti/Al₃Ti was fabricated through a powder metallurgy route followed by hot extrusion and was found to exhibit promising mechanical properties. The ultimate tensile strength and elongation of the composite sintered at 620℃ for 5h and extruded at a mass ratio of 12.75:1 reached 304 MPa and 14%, respectively, and its compressive deformation reached 60%. The promising mechanical properties are due to the core-shell-structured reinforcement, which is mainly composed of Al₃Ti and Ti and is bonded strongly with the Al matrix, and to the reduced crack sensitivity of Al₃Ti. The refined grains after hot extrusion also contribute to the mechanical properties of this composite. The mechanical properties might be further improved through regulating the relative thickness of Al-Ti intermetallics and Ti metal layers by adjusting the sintering time and the subsequent extrusion process.     

SiCf／Al模型复合材料界面微区残余应力

实验测定界面附近残余应力的分布有利于深入研究金属基复合材料变形和断裂行为的微观机制,对制备综合性能良好的复合材料具有指导作用。采用束斑直径为30μm的微小X射线束,测定了单根SiC连续纤维及连续SiC纤维束增强纯Al模型复合材料中SiC纤维附近基体中的周向和径向残余应力分布,并将测量结果与有限元模拟结果进行了比较。     

Al/Pb-WC-ZrO2复合电极材料的电化学性能研究

 研究了电镀液中固体微粒质量浓度及工艺条件对Al/Pb-WC-ZrO₂复合电极材料的表面化学组成及稳态析氧极化曲线的影响规律,对上述工艺条件进行了优化,优化后的工艺条件如下:WC:50 g/L,ZrO₂:40g/L,温度:20℃,电流密度:1.5 A/dm²,电沉积时间:2 h.所获得Al/Pb-WC-ZrO₂复合电极材料的析氧动力学参数为:a=771 mV,b=140 mV,i⁰=3.11×10^-6A·cm^-2,并且电极的析氧过电位为η=1 009 mV,复合镀层中WC和ZrO₂质量分数分别为10.02%和3.55%.     

CuO/Al反应自生复合材料的机械性能研究

采用液态搅拌法制备了反应自生 Al2 O3增强金属基复合材料并研究了它的机械性能 .采用 X衍射和扫描电镜分析了相组成和断口形貌 .与基体合金比较 ,复合材料的强硬性得到较大提高 ,其中 10 % Cu O复合材料的抗拉强度提高了 5 2 .3% ,硬度提高近一倍 .复合材料中的拉伸断裂特征为韧性断裂 ,铸造缺陷渣气孔是主要的裂纹源     

添加金属铝粉的锆刚玉莫来石材料显微结构与性能

通过扫描电镜、x射线衍射分析和体积密度、抗弯强度、烧结线收缩率以及抗热震性能的测定 ,主要探讨了金属铝粉的添加对反应烧结锆刚玉莫来石材料性能和显微结构的影响。     

添加金属铝粉的锆刚玉莫来石材料显微结构与性能

通过扫描电镜、x射线衍射分析和体积密度、抗弯强度、烧结线收缩率以及抗热震性能的测定,主要探讨了金属铝粉的添加对反应烧结锆刚玉莫来石材料性能和显微结构的影响.     

Diffusion welding of SiCp/2014Al composites using Ni as interlayer

SiCp/2014Al composites were bonded with the vacuum diffusion welding technique using Ni as the interlayer metal. Ni and Al were interdiffused and there were intermetallic compounds formed in the inter transition layer, which was composed of Ni₃Al//NiAl//NiAl₃. The relation between the diffusion distance and the element concentration was calculated according to Fick’s second law. The relations of the diffusion concentration and the diffusion welding technique parameters were calculated.