文昌鱼碱性磷酸酶的分子量及氨基酸组成的初步研究

经凝胶过滤法测得文昌鱼(Bronchiostoma belcheheri Gray)碱性磷酸酶的分子量为138,000,用等电聚焦电泳法测得其等电点为4.79,用氨基酸自动分析仪测得该酶的氨基酸组成共20种和1117个氨基酸残基。     

分光光度法测定紫菜中的碘

用碱溶法使紫菜中的碘以I-形式转移到溶液中,然后在酸性条件下用过氧化氢氧化,四氯化碳萃取,经分光光度标准曲线法测得紫菜中的碘含量大约为126.69 μg,该方法可以用来提取和测得海草中的碘含量,回收率高,简便可靠.     

重组人促红细胞生成素的基本特性研究

重组EPO细胞灌注法培养的收获液,用Q SepharoseXL,C4反相疏水和Superdex75层析柱纯化表达的EPO.经SDS PAGE、PAGE和HPLC分析纯度达98%以上,总回收率为17%.经SDS PAGE分析其表观分子量为32～40kD.用IEF方法测得pI为3.75～4.15.网织红细胞计数法测得体内比活大于1.5×105IU,用ELISA测得体外活性为1.5×106～1.6×106IU.纯化的EPO的氨基酸组成和其它一些性质也进行了研究.     

Te—Bi—Se稀散元素化合物半导体制冷材料的合成及应用研究

用陶瓷工艺方法合成Ｔｅ－Ｂｉ－Ｓｅ化合物多晶陶瓷半导体材料,用法测得热导率为１０ｍＷ／ｃｍ．Ｋ,用四探针法测得材料电导率为９００－１０００Ω＾－１ｃｍ＾－１;热电法测得材料的温差电动热率达到１８８－２００μＶ／Ｋ,优质系数Ｚｐ,Ｚｎ达到３．５＊１０＾－３／Ｋ。     

氯离子浓度对含盐污水中有机污染物化学需氧量测定的影响研究

采用重铬酸钾法与高锰酸盐指数碱性法对水中化学需氧量(COD)进行了对比测定研究,考察了氯离子浓度对化学需氧量测定结果的影响。分析结果表明,对于低含氯水样(氯离子浓度小于1 000 mg/L),用重铬酸钾法测得的COD值(CODCr)和用高锰酸盐指数碱性法测得的COD值(CODOH)存在线性关系;而高含氯水样的CODCr和CODOH之间无线性相关性。高浓度氯离子对CODCr值的测定影响显著,其影响规律可以用二次多项式表示。     

椭偏光法研究离子注入层(二) 椭偏光法研究硅中离子注入层的损伤分布、增强腐蚀效应和热退火过程

本文包括三个方面:(一)比较了用剥层椭偏光法和背散射法测得的注P~ 硅中的损伤分布.实验结果表明,当注入剂量为5×10~(14)/厘米~2、10~(15)/厘米~2及10~(10)/厘米~2时,注入区形成了不同厚度的非晶层,且由椭偏光法测得的非晶层厚度及分布区域与由背散射沟道分析法测得的符合很好;在注入剂量为2×10~(14)/厘米~2的较低剂量时,未形成非晶层,从椭偏光法测得的损伤峰位置亦与背散射法所得结果一致.(二)用椭偏光法研究了注As~ 硅表面层的离子注入增强腐蚀效应.文中提出了一种较精确地测量注入层腐蚀厚度的方法,并测得注As~ (剂量为10~(15)/厘米~2)的硅注入层在温度为43℃到45℃的23%稀释HF酸中增强腐蚀速率为6.5埃/分到22埃/分.(三)用椭偏光法研究了注入10~(15)/厘米~2As~ 的硅在500℃下的热退火过程.实验证实了离子注入引起的非晶层在热退火时发生固相外延.用剥层椭偏光法测量经过热退火后的注入区,发现△和ψ值都较正常硅的低,ψ最低可达9.2°,其原因还有待进一步研究.     

a-Si:H薄膜固相晶化法制备大晶粒多晶硅薄膜

用等离子体化学气相沉积（PCVD）法制备：a－Si：N薄膜材料（衬底温度20O℃～350℃），用固相晶化法（SPC）获得多晶硅薄膜（退火温度500℃～650℃）,用X射线衍射法测得平均晶粒尺寸依赖于退火温度和沉积条件，随着沉积温度的降低需要较高的退火温度,用SEM观测形貌测得平均晶粒大小为1,0～1,5μm     

石榴石磁泡膜饱和磁化强度的两种测量方法

用振动样品磁强计（ＶＳＭ）测量了石榴石磁泡膜饱和磁化强度Ｍ，并与用磁光法测量的结果进行了比较，发现用两种方法测得的Ｍ随温度的升高而下降的趋势存在着明显的差别，用ＶＳＭ测得的下降趋势缓慢，用磁光法测得的下降趋势迅速，这就引出一个问题，与磁光法测量Ｍ有关的理论可能存着不足。     

对581G型光电比色计测定钢中锰的一点看法

在高等学校分析化学实验教材(华中师院等三院校编)第实验40,用581G型光电比色计测定钢中锰。其锰的含量为6.10％,属于含量较高的分析。按光度法的理论要求,所得的A应比较大,不能包含在理论上要求的测量范围,应采用高级光光度法才能得到较准确的结果。但用581G型比色计测得其吸光度仅能达到0.190,按测得的A值不能满足光度     

限制性核酸内切酶Bsp63I的部分性质研究及与其同工酶的比较

纯化至电脉均一纯的限制性核酸内切酶Bsp63I经SephadexG-200测得相对分子质量约为113800,SDS－聚丙烯酰凝胶电泳测得其亚基相对分子质量约为56800,用DNS法测得该酶N－末端氨基酸为丙氨酸,表明该酶由2个相同的亚基组成,还对Bsp63I和它的同工酶PstI和Bsp78I之性质进行了比较。     

Markedness and its Interpretation in Language Use

Language markedness is a common phenomenon in languages, and is reflected from hearing, vision and sense, i.e. the variation in the three aspects such as phonology, morphology and semantics. This paper focuses on the interpretation of markedness in language use following the three perspectives, i.e. pragmatic interpretation, psychological interpretation and cognitive interpretation, with an aim to define the function of markedness.     

Features of Women's language

Language is a means of verbal communication. People use language to communicate with each other. In the society, no two speakers are exactly alike in the way of speaking. Some differences are due to age, gender, statue and personality. Above all, gender is one of the obvious reasons. The writer of this paper tries to describe the features of women＇s language from these perspectives： pronunciation, intonation, diction, subjects, grammar and discourse. From the discussion of the features of women＇s language, more attention should be paid to language use in social context. What＇s more, the linguistic phenomena in a speaking community can be understood more thoroughly.     

低渗透非均质砂岩油藏启动压力梯度研究

理论推导与室内实验相结合,建立了低渗透非均质砂岩油藏启动压力梯度确定方法。首先借助油藏流场与电场相似的原理,推导了非均质砂岩油藏启动压力梯度计算公式。其次基于稳定流实验方法,建立了非均质砂岩油藏启动压力梯度测试方法。结果表明:低渗透非均质砂岩油藏的启动压力梯度确定遵循两个等效原则。平面非均质油藏的启动压力梯度等于各级渗透率段的启动压力梯度关于长度的加权平均;纵向非均质油藏的启动压力梯度等于各渗透率层的启动压力梯度关于渗透率与渗流面积乘积的加权平均。研究成果可用于有效指导低渗透非均质砂岩油藏的合理井距确定,促进该类油藏的高效开发。     

On Tragic Consciousness In The Works By Ernest Hemingway

As an American modern novelist who were famous in the literary world, Hemingway was not a person who always followed the trend but a sharp observer. At the same time, he was a tragedy maestro, he paid great attention on existence, fate and end-result. The dramatis personae's tragedy of his works was an extreme limit by all means tragedy on the meaning of fearless challenge that failed. The beauty of tragedy was not produced on the destruction of life, but now this kind of value was in the impact activity. They performed for the reader about the tragedy on challenging for the limit and the death.     

Achieving Unusual States of Matter Under High Pressure

正The periodicity of the elements and the non-reactivity of the inner-shell electrons are two related principles of chemistry,rooted in the atomic shell structure.Within compounds,Group I elements,for example,invariably assume the+1 oxidation state,and their chemical properties differ completely from those of the p-block elements.These general rules govern our understanding of chemical structures and reactions.Using first principles calcula-     

Exchange-Correlation and Electronic Excitation Energies from Pairing Matrix Fluctuations

We have developed an adiabatic connection to formulate the ground-state exchange-correlation energy in terms of pairing matrix linear fluctuations.This formulation of the exchange-correlation energy opens a new channel for density functional approximations based on the many-body perturbation theory.We illustrate the potential of such approaches with an approximation based on the particle-particle Random Phase Approximation(pp-RPA).This re-     

Density Functional Theory for the Response of Periodic Systems to Electric Fields Based on the Vector Potential Approach

正The electronic and nuclear(structural/vibrational)response of 1D-3D nanoscale systems to electric fields gives rise to a host of optical,mechanical,spectral,etc.properties that are of high theoretical and applied interest.Due to the computational difficulty of treating such large systems it is convenient to model them as infinite and periodic(at least,in first approximation).The fundamental theoretical/computational problem in doing so is that     

On the Thermodynamic Limit for Responses to Static Electromagnetic Fields

For molecular systems,the quantum-mechanical treatment of their responses to static electromagnetic fields usually employs a scalar-potential treatment of the electric field and a vector-potential treatment of the magnetic field.Although the potential for each field separately is associated with the choice of an(unphysical)origin,the precise choice of the origin for the electrostatic field has little consequences for the results.This is different for the     

Call for Papers

<正>"The Journal of Shanghai Normal University:Mathematics"is published by Shanghai Normal University as regular issues of The Journal of Shanghai Normal University each year from 2014 in English.The editors-in-chief of the issues are professors Yuhao Cong and Maoan Han.The Journal of Shanghai Normal University was started in 1958 with     

Journal of Donghua University ( English Edition) Contents of Volume 31

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