中等粒度纳米金刚石用于磁头抛光的工艺

采用浮动块研磨抛光机,研究中等粒度纳米金刚石抛光液用于硬盘磁头抛光时其颗粒大小及其悬浮液的分散稳定性与磁头表面质量的关系,以及抛光各工序、运行参数与表面质量的关系.磁头表面质量采用原子力显微镜观测分析.通过对抛光过程运行参数的正交实验,对中等粒度纳米金刚石用于磁头抛光的工艺过程进行优化.实验结果表明:磁头表面粗糙度随着金刚石粒径的减小而减小,但二者并不呈线性关系;抛光液的分散稳定性比抛光液颗粒粒径更能影响表面划痕的深度;精研磨能有效去除表面划痕;而抛光能有效降低表面粗糙度,但其对划痕的消除不如精磨有效;各参数对表面粗糙度和划痕的影响程度不同,但是优化后参数取值相同.     

固结磨料确定性研磨表面生成建模与实验分析

基于CCOS技术原理,提出高效、高可控性的固结磨料确定性研磨工艺.通过线研磨实验发现采用中心供给研磨液方式相比于传统四周供液方式有利于提高加工效率及表面质量.分析了工艺参数对加工后表面硬度的影响,通过扫描电镜观察研磨后的表面形貌,分析固结磨料研磨的材料去除机制.通过不同参数线研磨实验验证了材料去除率与工具转速、载荷、时间呈线性关系,表明固结磨料研磨工艺的材料去除过程符合CCOS的卷积迭代原理.基于晶胞理论和磨粒粒径均匀的假设,建立了固结磨料研磨垫表面形貌的仿真模型.同时,模型考虑了磨粒浓度、磨粒粒度、研磨垫形状参数的影响.在固结磨料研磨垫形貌仿真数据的基础上,基于硬脆材料去除机理以及研磨垫与工件微观接触模型,考虑工件表面的力学性能,建立了一定参数条件下研磨垫与工件的接触间隙计算模型,进而建立了单点研磨去除斑模型.通过定点研磨实验验证了不同压力、转速、时长条件下单点研磨去除斑模型的准确性.将连续的研磨轨迹进行离散,考虑研磨垫形状、磨粒的尺寸和浓度、研磨工具的转速和承受的载荷、轨迹参数建立了总去除量与单点研磨去除量的卷积运算关系,提出固结磨料确定性研磨表面生成模型.开展不同参数下面研磨实验与表面仿真.结果表明,固结磨料确定性研磨表面生成模型能很好地预测不同参数下研磨去除的深度和研磨表面的残留误差,提高固结磨料研磨工艺的可控性.     

聚晶金刚石研磨机理研究

通过 PCD表面干研磨、湿研磨、钝湿研磨等对比试验 ,观察干研磨、湿研磨表面形貌 ,研究了 PCD材料研磨机理 .试验结果表明 ,干研磨去除率远大于湿研磨去除率 ,并可使 PCD表面达到镜面 ;湿研磨、钝湿研磨不能使其达到镜面 .干研磨时 ,材料的去除机理以热化学去除为主 ,基本不发生疲劳脆性去除 ;湿研磨时 ,材料去除机理以疲劳脆性去除为主 ,同时存在局部的热化学去除     

6H-SiC晶片集群磁流变研磨工艺优化

为了研究不同种类磨粒与羰基铁粉的粒径匹配性对加工效果的影响规律,并优化磁感应强度、研磨压力、研磨盘转速和工件转速等工艺参数,采用集群磁流变研磨方法对6H-SiC晶片进行了研磨试验。结果表明:当磨粒与羰基铁粉的粒径比约为1.5时加工效果较好;各工艺参数对6H-SiC加工的材料去除率的影响由大到小依次为磁感应强度、研磨盘转速、研磨压力、工件转速,对表面粗糙度的影响由大到小依次为磁感应强度、研磨压力、工件转速、研磨盘转速;磁感应强度可以改变羰基铁粉的吸附力,从而改变对磨粒的把持程度,成为影响加工效果最显著的因素。优化后的工艺参数组合为:工件转速60r·min-1;研磨盘逆向转速90r·min-1;研磨压力70kPa;磁感应强度0.012T。在此优化条件下能获得最大的材料去除率(0.498μm·min-1)和较低的表面粗糙度(86.3nm)。     

清洗研磨对改善铜板带材表面质量的作用

通过铜板带质量缺陷的数据统计,得出铜板带材普遍存在的质量缺陷主要是表面缺陷的结论,并在此基础上论述了清洗研磨对改善铜板带材表面质量的作用,以及保证清洗研磨效果的四个关键要素,即选好研磨辊刷、选好刷辊线径、选好磨粒目数和选好包括接触压力、研磨量及刷辊速度在内的研磨工艺.文章对现实铜板带材生产过程中,如何进一步改善表面质量具有借鉴价值.     

混合轴承陶瓷球的锥形研磨加工工艺

采用锥形研磨法加工热等静压氮化硅(HIPSN)陶瓷球,分析了研磨压力、研磨转速以及研磨剂添加周期等研磨工艺参数与研磨效率的关系,研究如何提高金刚石研磨剂的利用率,降低研磨加工成本·研究表明,为了提高研磨效率、降低研磨成本,合理、稳定的研磨工艺应确定为:单球研磨压力6～8N;研磨转速450～800r/min;研磨剂的一次添加时间是60min左右·按照总结出的研磨工艺进行HIPSN陶瓷球的研磨加工,成品陶瓷球的表面粗糙度在0 01～0 02μm,球形误差在0 09～0 18μm范围内,完全满足使用要求·     

磁力研磨的试验研究

本文介绍一种机械加工新工艺.利用永久磁铁及磁性磨料,对难加工材料不锈钢工件内表面进行研磨.用正交试验法试验了磨料粒度、工件转速、磁极间隙等参数对磁力研磨效果的影响.     

乙二醇对固结磨料研磨蓝宝石晶圆的影响

研磨液中的化学添加剂对于蓝宝石晶圆的高效超光滑表面加工至关重要.文中开展了固结磨料研磨蓝宝石晶圆的实验研究,探索了不同乙二醇含量的研磨液对材料去除速率和表面形貌的影响规律,采用微/纳米压痕技术和光电子能谱剖析了工件表层的物理化学性能.结果表明:当研磨液中含有5%的乙二醇时,工件表面变质层深度约为3.90 nm,远优于去离子水研磨液的工件变质层深度(1.04 nm);乙二醇含量的提高促进了表面变质层的生成,有利于蓝宝石工件研磨效率的提高和表面质量的改善.     

基于响应曲面法电火花线切割回转零件实验研究

以低速走丝电火花线切割加工回转铜钨合金(CuW70)试件为研究对象,采用Design-Expert软件设计Box-Behnken实验,利用响应曲面法分析得出不同速度参数对工件表面粗糙度及材料去除率的影响规律,并得出兼顾加工效率与表面质量的最优工艺参数组合.结果表明,速度参数对表面粗糙度影响的主次关系为工件转速>进给速度>走丝速度;对材料去除率影响的主次关系为进给速度>工件转速>走丝速度.多目标参数优化得出:当工件转速为46r/min,进给速度为1.0mm/min,走丝速度为45mm/s时,表面粗糙度达到0.882μm,材料去除率达到0.625mm³/min.     

TC4钛合金孔的磁粒研磨试验

采用内置磁极吸附磁性磨粒的方法,研究了工艺参数对高效去除TC4钛合金孔毛刺和切痕,降低表面粗糙度R_a,以及改善微观表面形貌的影响.首先,开展磁极与孔同轴研磨正交试验,通过极差和方差分析,获得磁极转速、磨料直径和磨料填充量对孔表面粗糙度R_a和微观形貌的影响程度,确定了较优的工艺参数组合;其次,开展磁极与孔偏心研磨试验,进行了三维力检测和数据分析.结果表明:对于10mm的TC4钛合金孔,使用6mm的径向磁极,偏心距1mm研磨30min后,孔的毛刺和切痕得以去除,表面形貌均匀平整,与同轴方案比较,表面粗糙度R_a下降13.7%,研磨效率提升25.0%.     

Markedness and its Interpretation in Language Use

Language markedness is a common phenomenon in languages, and is reflected from hearing, vision and sense, i.e. the variation in the three aspects such as phonology, morphology and semantics. This paper focuses on the interpretation of markedness in language use following the three perspectives, i.e. pragmatic interpretation, psychological interpretation and cognitive interpretation, with an aim to define the function of markedness.     

Features of Women's language

Language is a means of verbal communication. People use language to communicate with each other. In the society, no two speakers are exactly alike in the way of speaking. Some differences are due to age, gender, statue and personality. Above all, gender is one of the obvious reasons. The writer of this paper tries to describe the features of women＇s language from these perspectives： pronunciation, intonation, diction, subjects, grammar and discourse. From the discussion of the features of women＇s language, more attention should be paid to language use in social context. What＇s more, the linguistic phenomena in a speaking community can be understood more thoroughly.     

低渗透非均质砂岩油藏启动压力梯度研究

理论推导与室内实验相结合,建立了低渗透非均质砂岩油藏启动压力梯度确定方法。首先借助油藏流场与电场相似的原理,推导了非均质砂岩油藏启动压力梯度计算公式。其次基于稳定流实验方法,建立了非均质砂岩油藏启动压力梯度测试方法。结果表明:低渗透非均质砂岩油藏的启动压力梯度确定遵循两个等效原则。平面非均质油藏的启动压力梯度等于各级渗透率段的启动压力梯度关于长度的加权平均;纵向非均质油藏的启动压力梯度等于各渗透率层的启动压力梯度关于渗透率与渗流面积乘积的加权平均。研究成果可用于有效指导低渗透非均质砂岩油藏的合理井距确定,促进该类油藏的高效开发。     

On Tragic Consciousness In The Works By Ernest Hemingway

As an American modern novelist who were famous in the literary world, Hemingway was not a person who always followed the trend but a sharp observer. At the same time, he was a tragedy maestro, he paid great attention on existence, fate and end-result. The dramatis personae's tragedy of his works was an extreme limit by all means tragedy on the meaning of fearless challenge that failed. The beauty of tragedy was not produced on the destruction of life, but now this kind of value was in the impact activity. They performed for the reader about the tragedy on challenging for the limit and the death.     

Achieving Unusual States of Matter Under High Pressure

正The periodicity of the elements and the non-reactivity of the inner-shell electrons are two related principles of chemistry,rooted in the atomic shell structure.Within compounds,Group I elements,for example,invariably assume the+1 oxidation state,and their chemical properties differ completely from those of the p-block elements.These general rules govern our understanding of chemical structures and reactions.Using first principles calcula-     

Exchange-Correlation and Electronic Excitation Energies from Pairing Matrix Fluctuations

We have developed an adiabatic connection to formulate the ground-state exchange-correlation energy in terms of pairing matrix linear fluctuations.This formulation of the exchange-correlation energy opens a new channel for density functional approximations based on the many-body perturbation theory.We illustrate the potential of such approaches with an approximation based on the particle-particle Random Phase Approximation(pp-RPA).This re-     

Density Functional Theory for the Response of Periodic Systems to Electric Fields Based on the Vector Potential Approach

正The electronic and nuclear(structural/vibrational)response of 1D-3D nanoscale systems to electric fields gives rise to a host of optical,mechanical,spectral,etc.properties that are of high theoretical and applied interest.Due to the computational difficulty of treating such large systems it is convenient to model them as infinite and periodic(at least,in first approximation).The fundamental theoretical/computational problem in doing so is that     

On the Thermodynamic Limit for Responses to Static Electromagnetic Fields

For molecular systems,the quantum-mechanical treatment of their responses to static electromagnetic fields usually employs a scalar-potential treatment of the electric field and a vector-potential treatment of the magnetic field.Although the potential for each field separately is associated with the choice of an(unphysical)origin,the precise choice of the origin for the electrostatic field has little consequences for the results.This is different for the     

Call for Papers

<正>"The Journal of Shanghai Normal University:Mathematics"is published by Shanghai Normal University as regular issues of The Journal of Shanghai Normal University each year from 2014 in English.The editors-in-chief of the issues are professors Yuhao Cong and Maoan Han.The Journal of Shanghai Normal University was started in 1958 with     

Journal of Donghua University ( English Edition) Contents of Volume 31

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