电致发热SiC多孔陶瓷Al2O3/SiO2复相绝缘涂层制备

以异丙醇铝为前驱物,水为溶剂,硝酸为胶溶剂,用分散法制得性能稳定的透明氧化铝溶胶,将多孔陶瓷置于氧化铝溶胶中反复浸渍,经低温和高温热处理后使其表面形成致密的Al2O3和SiO2陶瓷涂层。通过EDS能谱分析得到Al2O3的含量约54%,SiO2含量约46%,电阻较涂覆前显著增加,得出用溶胶-凝胶法涂覆陶瓷体表面后,再经热处理是一种切实可行的制备绝缘陶瓷涂层的方法。     

铷频标光强稳定性影响因素的研究

从理论和试验两方面分析了影响铷频标光谱灯光强稳定性的若干因素,通过铷光谱灯参数优化、采用电致变色薄膜,提出了稳定铷光谱灯光强的技术措施和可行性方案,旨在为提高铷频标的长期稳定度提供可以借鉴的方法。     

用于北斗三号卫星导航系统的星载铷原子钟特性

本文介绍用于北斗三号卫星导航系统的星载铷原子钟主要设计特点和性能指标.铷原子钟频率稳定度主要取决于原子跃迁信号信噪比、电路噪声和原子体系的物理环境效应.为提高原子信号信噪比,物理系统采用了微波场方向因子高于0.9的开槽管微波腔和Xe气启辉的铷光谱灯,并采用了光学滤光和同位素滤光双重滤光方案.电路系统采用了低相噪微波链路,交互调制噪声对铷原子钟稳定度的影响被控制在4.9×10^-13/τ^1/2水平.通过工作参数优化,将物理环境效应对天频率稳定度的影响降低到3×10^-15以下.研制了高精度和甚高精度两型号星载铷原子钟.高精度铷原子钟典型指标为短稳1.5×10^-12/τ^1/2,万秒稳1.3×10^?14,天稳9.4×10^-15;甚高精度铷原子钟典型指标为短稳6.1×10^-13/τ^1/2,万秒稳7.1×10^-15,天稳3.9×10^-15.本文还分析了铷原子钟最新研究进展,预期铷原子钟的性能还可以进一步提升.     

纳米复合彩色薄膜的制备

以正硅酸乙酯、乙醇、生物染色剂为主要原料 ,通过溶胶 -凝胶法制备了掺有有机染料的SiO2 溶胶 ,利用提拉法在普通玻璃上成功镀制了均匀透明、色泽丰富的彩色涂层 ,该涂层颜色在高温下会彻底分解消失 ,实现了玻璃的可回收利用 .运用光谱分析、扫描探针显微镜研究了薄膜的结构 ,以及工艺参数对薄膜在可见光区光谱性能的影响 .     

溶胶-凝胶法Al2O3涂层碳纤维的制备与表征

该文研究了溶胶-凝胶法在碳纤维表面制备氧化铝(Al2O3)涂层时勃姆石溶胶浓度、涂层厚度和材料的层间剪切强度的关系，发现Al2O3涂层的厚度与勃姆石溶胶浓度基本呈线性关系，并且随着溶胶浓度的提高，涂层厚度增加，试样的层间剪切强度表现为先增加后下降的趋势。在勃姆石溶胶的浓度为0．27mol／L左右时，所得Al2O3涂层的厚度约为30nm，环氧基复合材料的层间剪切强度达到最大值。X射线光电子能谱和扫描电子显微镜分析表明，在碳纤维表面形成的Al2O3薄膜均匀、完整。     

防水玻璃表面涂层新工艺的初步探索

对正硅酸乙酯(TOFS)作溶胶涂层制备防水透光玻璃材料的新工艺进行初步的试验。该涂层工艺的特点在于改变涂液的配方和浸涂制膜条件,使玻璃表面的防水性和透光度增强,并借助SEM、UV等方法测量涂层的结构、厚度与其透光度及水的接触角等性质,对照试验表明:所得涂层玻璃具有明显的防水性和透光度,进一步完善后具有一定的实用价值。     

纳米氧化铝对金属基陶瓷涂层性能的影响

在金属基陶瓷涂层的制备过程中,添加了适量的纳米氧化铝,使涂层的综合性能得到了改善。对涂层的表面形貌、界面结合情况和摩擦磨损性能进行了研究和分析。实验结果表明:添加了纳米氧化铝的涂层试样表面更加光滑平整,涂层与基体结合更加紧密,当纳米氧化铝的最佳添加量为陶瓷骨料总质量的2%时,制备出来的陶瓷涂层综合性能达到最佳。     

纳米TiO2溶胶制备及其对PBO纤维抗紫外光老化的影响

制备了特定配比的TiO2溶胶,并把TiO2溶胶应用到PBO纤维表面形成抗老化TiO2涂层;使用紫外灯连续照射PBO纤维,从宏观力学性能和微观结构两个角度研究TiO2涂层对缓解PBO纤维紫外老化速度的作用。     

溶胶-凝胶法制备氧化铝薄膜的研究

采用溶胶 -凝胶法在普通玻璃载片上制备了Al2 O3 薄膜 .通过XRD ,DSC -TGA以及椭圆偏振测厚仪等测量手段研究了勃姆石溶胶的制备条件 ,氧化铝薄膜的光学参数以及勃姆石凝胶在热处理过程中的物理变化 .结果表明 :异丙醇铝的浓度、水解温度和胶溶剂的加入量直接影响了勃母石溶胶的稳定性 .45 0℃热处理所得薄膜单层厚度为 31.3nm ,折射率为 1.72 ,表面均匀 ,透光性好     

锡林浩特石灰窑花岗岩型铷多金属矿床中铷矿石选矿实验研究

铷金属是非常重要的稀有金属之一,不仅在军事工业和科学技术领域,而且在民用领域有着广泛的用途.随着我国国民经济高速增长,对铷矿产品需求不断加大.我国最近在内蒙古锡林浩特石灰窑地区发现一大型花岗岩型铷多金属矿床,其初步探明的铷总金属量超过8.7×10~5t,Rb_2O平均品位0.163%.矿石中铷主要赋存于云母类矿物和微斜长石中.由于长石中的铷很难提取,为高效回收该铷矿资源,本研究采用富集云母类矿物的方式进行了铷回收实验研究.结果表明,矿石在浮选探索实验中,随着混合胺用量或水玻璃的增加,铷粗精矿的回收率逐渐提高,当混合胺超过150 g/t或者水玻璃超过1 200 g/t后,回收率增幅较小,确定混合胺用量以150 g/t或水玻璃用量以1 200 g/t为宜,最终可取得Rb_2O品位1.59%,回收率约为62.92%的铷精矿.实验指标较好,可实现铷的高效回收.     

铷D2线高分辨光电流谱研究

应用空心阴极放电管观测铷D₂线的光电流谱,发现谱线中部有凹陷出现。对凹陷出现的原因进行了分析和研究。利用此现象,将半导体激光器(0.7800μm)频率锁定于谱线凹陷的中央。     

四元含锂铷氯化物水盐体系298.2 K介稳相平衡研究

采用等温蒸发法研究了四元含锂铷氯化物体系Li+,Na+,Rb+//Cl--H2O 298.2K下的相平衡关系,测定了平衡液相的溶解度、密度和折光率.基于实验数据,绘制了该四元体系的立体图、干基图、密度-组成图和折光率-组成图.该四元体系298.2K下的介稳相图由1个共饱和点,3条单变量曲线和3个结晶区(RbCl、NaCl、LiCl·H2O)组成.将研究的结果同LiCl+KCl+RbCl+H2O体系进行了对比和分析,总结Na+和K+对三元体系Li+,Rb+//Cl--H2O的影响.应用折光率计算的经验公式对实验测定的折光率进行了验证,其最大绝对误差小于-0.0090,从而证明了实验数据的可靠性.     

数字调频及数字伺服在铷频标中的应用

介绍了铷原子频标的基本原理及现状 ,提出了采用数字锁相调频电路代替原变容二极管调相电路实现对量子系统激励信号频率调制的方案 ,以及采用数字伺服电路代替原模拟纠偏电路的措施 ,可消除电子线路上的不完善给铷原子频标带来的温度系数和不稳定性     

Markedness and its Interpretation in Language Use

Language markedness is a common phenomenon in languages, and is reflected from hearing, vision and sense, i.e. the variation in the three aspects such as phonology, morphology and semantics. This paper focuses on the interpretation of markedness in language use following the three perspectives, i.e. pragmatic interpretation, psychological interpretation and cognitive interpretation, with an aim to define the function of markedness.     

Features of Women's language

Language is a means of verbal communication. People use language to communicate with each other. In the society, no two speakers are exactly alike in the way of speaking. Some differences are due to age, gender, statue and personality. Above all, gender is one of the obvious reasons. The writer of this paper tries to describe the features of women＇s language from these perspectives： pronunciation, intonation, diction, subjects, grammar and discourse. From the discussion of the features of women＇s language, more attention should be paid to language use in social context. What＇s more, the linguistic phenomena in a speaking community can be understood more thoroughly.     

An Analysis of Catherine＇s Character——Wuthering Heights

Wuthering Heights, Emily Bronte＇s only novel, was published in December of 1847 under the pseudonym Ellis Bell. The book did not gain immediate success, but it is now thought one of the finest novels in the English language. Catherine is the key character of this masterpiece, because everybody and everything center on her though she had a short life. We can understand this masterpiece better if we know Catherine well.     

Lower Paleozoic oil relationships within Williston Basin, Canada

The Williston Basin is a significant petroleum province, containing oil production zones that include the Middle Cambrian to Lower Ordovician, Upper Ordovician, Middle Devonian, Upper Devonian and Mississippian and within the Jurassic and Cretaceous. The oils of the Williston Basin exhibit a wide range of geochemical characteristics defined as "oil families", although the geochemical signature of the Cambrian Deadwood Formation and Lower Ordovician Winnipeg reservoired oils does not match any "oil family". Despite their close stratigraphic proximity, it is evident that the oils of the Lower Palaeozoic within the Williston Basin are distinct. This suggests the presence of a new "oil family" within the Williston Basin. Diagnostic geochemical signatures occur in the gasoline range chromatograms, within saturate fraction gas chromatograms and biomarker fingerprints. However, some of the established criteria and cross-plots that are currently used to segregate oils into distinct genetic families within the basin do not always meet with success, particularly when applied to the Lower Palaeozoic oils of the Deadwood and Winnipeg Formation.     

低渗透非均质砂岩油藏启动压力梯度研究

理论推导与室内实验相结合,建立了低渗透非均质砂岩油藏启动压力梯度确定方法。首先借助油藏流场与电场相似的原理,推导了非均质砂岩油藏启动压力梯度计算公式。其次基于稳定流实验方法,建立了非均质砂岩油藏启动压力梯度测试方法。结果表明:低渗透非均质砂岩油藏的启动压力梯度确定遵循两个等效原则。平面非均质油藏的启动压力梯度等于各级渗透率段的启动压力梯度关于长度的加权平均;纵向非均质油藏的启动压力梯度等于各渗透率层的启动压力梯度关于渗透率与渗流面积乘积的加权平均。研究成果可用于有效指导低渗透非均质砂岩油藏的合理井距确定,促进该类油藏的高效开发。     

On Tragic Consciousness In The Works By Ernest Hemingway

As an American modern novelist who were famous in the literary world, Hemingway was not a person who always followed the trend but a sharp observer. At the same time, he was a tragedy maestro, he paid great attention on existence, fate and end-result. The dramatis personae's tragedy of his works was an extreme limit by all means tragedy on the meaning of fearless challenge that failed. The beauty of tragedy was not produced on the destruction of life, but now this kind of value was in the impact activity. They performed for the reader about the tragedy on challenging for the limit and the death.     

Achieving Unusual States of Matter Under High Pressure

正The periodicity of the elements and the non-reactivity of the inner-shell electrons are two related principles of chemistry,rooted in the atomic shell structure.Within compounds,Group I elements,for example,invariably assume the+1 oxidation state,and their chemical properties differ completely from those of the p-block elements.These general rules govern our understanding of chemical structures and reactions.Using first principles calcula-