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1.
在磷酸介质中,在Mn和Tween-80存在下,DApBM与钒生成橙黄色化合物,产物至少可稳定3.5h,最大吸收波长为485nm。摩尔吸光系数ε=4.01×10^5L.mol^-1.cm^-1和ε=1.57×10^4L.mol^-1.cm^-1,钒量在0.5-3.0μg/25ml及3.0-10.0μ/25ml间符合比尔定律。  相似文献   

2.
实验于1996年5月 ̄9月对3种规格养殖中国对虾在不同条件下的耗氧率和排氨率进行了测定。结果表明,温度、体重、盐度和摄食状态对其代谢有显著影响。耗氧率(QO)和排氨率(QN)与温度正相关,lnQo=0.58T-2.894;lnQN=0.076T+1.116;而与体重呈负相关,QO=0.515W^-0.126;QN=25.05W^-0.199。在盐度5 ̄35范围内,中国对虾(3.025g±0.088  相似文献   

3.
BaCe0.95Y0.05O3α固体电解质材料的热性质   总被引:2,自引:0,他引:2  
用甚高温量热计对BaCe0.95Y0.05O3-α固体电解质材料在300-1400℃范围做差热分析,证明其结构是稳定的。在1000-1500℃范围做焓测定,得到焓与温度的关系H=-6598+1.45(J.g^-1)及平均热容c=1.45J.(gK)^-1。  相似文献   

4.
研究了细胞生长过程中微载体的种类、浓度及细胞接种量对培养Px细胞的影响。以GT-3为微载体,当细胞接种量为2.0×10^5细胞/mL,微载体浓度为2.0mg/mL,温度为28℃时,第6天细胞密度可达1.0×10^6细胞/mL,为接种量的5倍,细胞生长旺盛,形态正常。  相似文献   

5.
采用湿化学法制备了粒度在0.2~0.8μm范围的钙钛矿型La1-xSrxMnO3粉末,用室温和高温X衍射法测定其晶体结构,发现其在1 200℃高温发生了四方→立方的相变;制备的粉末粒度与水浴温度有一定的关系,在室温时电阻率在6.0×10^-3~6.9×10^-3Ω.cm范围内,在温度大于450℃后,随着温度的升高,电阻率亦升高。  相似文献   

6.
采用固相合成法直接合成CaZr0.9In0.1O3-a用交流阻抗谱技术,在869~1300K温度范围内,空气气氛下测得其电导率为10^-4~10^-2s.cm^-1制得CaZr0.9In0.1O3-a固体电解质管,以含H2的标准气为参比电极,组装成氢浓差电池。Fe含H2标准气│CaZr0.9In0.1O3-a│(H)AlFe并构成氢传感探头,研究其对熔融铝中氢含量的传感特性,实验证明,该传感器响应  相似文献   

7.
研究了不同Nd^3^+浓度(0.1mol%-2mol%)掺杂的BaTiO3陶瓷的电性能。结果表明,当Nd^3^+逍度为0.1mol%-0.2mol%时,轻度Nd^3^+掺杂的BaTiO3陶瓷呈半导性,而当Nd^3^+为0.6mol%-2mol%时呈绝缘性,BaTiO3陶恣室温下的体电阻率ρv随Nd^3^+浓度的变化呈U型特性曲线,当Nd^3^+=0.15mol%时材料具有最低的ρv和最佳的正温系数  相似文献   

8.
富硼渣硫酸浸出试验研究   总被引:4,自引:0,他引:4  
以富硼渣为原料,在1.5m^3浸出罐中进行硫酸浸出试验,硼的浸出率主要与富硼渣的结构,粒度,加酸量及浸出时间和温度等因素有关,试验结果表明,富硼渣中硼只要以遂安石晶体存在,粒度在0.18~0.16mm加酸量为80%,浸出时间90min温度95~100℃硫酸浸出率可大于90%。  相似文献   

9.
利用^1H-^1HCOSY,^13C-^1HCOSY,^13C-^1H远程COSY以及选择性远程DEPT^13CNMR谱,对2,4-二硝基五环[4.3.0.0^2.5,0^3.8.0^4,7]壬烷的^1H和^13NMR谱进行了完全的归属。  相似文献   

10.
导数示波极谱法测定废水中微量的对硝基苯乙酮   总被引:1,自引:0,他引:1  
对硝基苯乙酮在0.025mol.L^-1乙二胺-0.010mol.L^01EDTA底液中,产生一灵敏的极谱峰电流。峰电位为-0.35V。对硝基苯乙酮浓度在3.00×10^-8-1.00×10^-5mol.L^-1范围内,浓度与峰电流成线性关系。  相似文献   

11.
Language markedness is a common phenomenon in languages, and is reflected from hearing, vision and sense, i.e. the variation in the three aspects such as phonology, morphology and semantics. This paper focuses on the interpretation of markedness in language use following the three perspectives, i.e. pragmatic interpretation, psychological interpretation and cognitive interpretation, with an aim to define the function of markedness.  相似文献   

12.
理论推导与室内实验相结合,建立了低渗透非均质砂岩油藏启动压力梯度确定方法。首先借助油藏流场与电场相似的原理,推导了非均质砂岩油藏启动压力梯度计算公式。其次基于稳定流实验方法,建立了非均质砂岩油藏启动压力梯度测试方法。结果表明:低渗透非均质砂岩油藏的启动压力梯度确定遵循两个等效原则。平面非均质油藏的启动压力梯度等于各级渗透率段的启动压力梯度关于长度的加权平均;纵向非均质油藏的启动压力梯度等于各渗透率层的启动压力梯度关于渗透率与渗流面积乘积的加权平均。研究成果可用于有效指导低渗透非均质砂岩油藏的合理井距确定,促进该类油藏的高效开发。  相似文献   

13.
As an American modern novelist who were famous in the literary world, Hemingway was not a person who always followed the trend but a sharp observer. At the same time, he was a tragedy maestro, he paid great attention on existence, fate and end-result. The dramatis personae's tragedy of his works was an extreme limit by all means tragedy on the meaning of fearless challenge that failed. The beauty of tragedy was not produced on the destruction of life, but now this kind of value was in the impact activity. They performed for the reader about the tragedy on challenging for the limit and the death.  相似文献   

14.
正The periodicity of the elements and the non-reactivity of the inner-shell electrons are two related principles of chemistry,rooted in the atomic shell structure.Within compounds,Group I elements,for example,invariably assume the+1 oxidation state,and their chemical properties differ completely from those of the p-block elements.These general rules govern our understanding of chemical structures and reactions.Using first principles calcula-  相似文献   

15.
We have developed an adiabatic connection to formulate the ground-state exchange-correlation energy in terms of pairing matrix linear fluctuations.This formulation of the exchange-correlation energy opens a new channel for density functional approximations based on the many-body perturbation theory.We illustrate the potential of such approaches with an approximation based on the particle-particle Random Phase Approximation(pp-RPA).This re-  相似文献   

16.
正The electronic and nuclear(structural/vibrational)response of 1D-3D nanoscale systems to electric fields gives rise to a host of optical,mechanical,spectral,etc.properties that are of high theoretical and applied interest.Due to the computational difficulty of treating such large systems it is convenient to model them as infinite and periodic(at least,in first approximation).The fundamental theoretical/computational problem in doing so is that  相似文献   

17.
For molecular systems,the quantum-mechanical treatment of their responses to static electromagnetic fields usually employs a scalar-potential treatment of the electric field and a vector-potential treatment of the magnetic field.Although the potential for each field separately is associated with the choice of an(unphysical)origin,the precise choice of the origin for the electrostatic field has little consequences for the results.This is different for the  相似文献   

18.
Franck-Condon factors bridge the gap between theoretical modeling and experimental observations for molecular electronic spectroscopy and electron transfer.Under the displaced harmonic oscillator approximation,multidimensional Franck-Condon factors are decomposed into a product of many one-dimensional(1D)Franck-Condon(FC)factors,and each 1D-FC factor is associated with one Huang-Rhys factor that determines the leading contribution of  相似文献   

19.
<正>"The Journal of Shanghai Normal University:Mathematics"is published by Shanghai Normal University as regular issues of The Journal of Shanghai Normal University each year from 2014 in English.The editors-in-chief of the issues are professors Yuhao Cong and Maoan Han.The Journal of Shanghai Normal University was started in 1958 with  相似文献   

20.
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