轧制工艺对Mg-Sn-Gd镁合金微观组织与性能的影响

采用光学显微镜、扫描电子显微镜、X射线衍射仪和电子万能试验机研究了不同轧制工艺对Mg-3.2Sn-0.23Gd(质量分数,％)镁合金微观组织和力学性能的影响.结果表明,不同道次变形量(分别为60％和30％)对镁合金的微观组织与力学性能有较大影响:60％道次变形量时轧制态组织中存在剪切带和孪晶,退火后为明显混晶组织,第二...     

异速比对异步轧制AZ31镁合金板材组织和织构的影响

采用不同异速比对AZ31镁合金板材进行异步轧制,并将轧后样品进行显微组织和X射线衍射分析,研究异速比对镁合金板材组织和织构转变的影响. 结果表明:异速比的变化对晶粒形貌影响较大但晶粒细化效果不明显;当异速比为2.800时,板材内出现了长条晶粒;快速辊侧{0002}基面织构强度高于慢速辊侧,且板材两侧表面{0002}晶面的偏转方向相反;异速比对基面织构的强度影响显著,随着异速比的增大,基面织构的强度先增加后下降. 这种特殊的织构变化与异步轧制过程中沿厚度方向引入的剪切变形有关.     

微观组织和织构对H65黄铜带材折弯性能的影响

电子产品关键部件小型化对黄铜合金带材折弯性能提出了更高的要求。研究了微观组织和织构对H65黄铜带材折弯性能的影响规律和影响机制。结果表明：带材平行于轧向折弯较垂直于轧向折弯更易于产生表面褶皱和裂纹,且随着折弯半径的减小,折弯性能降低。折弯变形过程中带材外表面易形成剪切带,所产生的剪切变形是造成表面褶皱和开裂的主要原因。微观组织不均匀、较强的Brass织构易导致带材折弯过程中产生剪切变形,造成带材折弯性能下降。通过调控热处理工艺来调整带材织构,减少或抑制剪切带的产生,能够提升带材的折弯性能。     

交叉轧制对TA1钛箔材组织和性能的影响

采用光学显微镜和室温拉伸试验研究了交叉轧制对TA1钛箔材组织和性能的影响。结果表明：交叉轧制后,晶粒尺寸减小,组织更加均匀。拉伸测试表明：采用交叉轧制后,塑性升高,强度、各向异性和横向屈强比均显著降低。屈服强度与晶粒尺寸的关系遵循Hall—Petch公式。交叉轧制后,σ₀值显著降低,K值为正值。普通轧制后,σ₀值较高,K值都为负值。     

高铌对X80管线钢相变与微观组织的影响

利用Gleeble-1500热模拟实验机,测定了铌含量分别为0.095%和0.045%的X80针状铁素体管线钢过冷奥氏体连续冷却转变点,并绘制了变形条件下高铌钢的CCT曲线并分析了其微观组织.实验结果表明:高铌含量能够延迟X80管线钢的γ/a 转变并减少块状铁素体的体积分数.高铌X80管线钢在较低的冷却速度和较宽的冷速范围内都能获得理想的针状铁素体组织.     

轧制工艺对帘线钢盘条织构的影响

采用X射线衍射法对国内外四家钢厂帘线钢盘条的织构进行了对比研究.结果表明,国内外各钢厂盘条的织构存在明显差异,国内盘条轴向上的{111}织构强度大于国外盘条,然而盘条轴向上的{111}织构是硬取向,不利于盘条的拉拔.通过延长加热炉加热时间、提高加热温度和提高吐丝温度,可以使{111}织构的强度明显降低.     

复合材料微观织构的数学模型

复合材料失效大多数情况都起始于微观水平的破坏,比如微裂纹的萌生、扩展,直到最后的失稳断裂,而微裂纹的扩展只受附近几个晶粒影响,所以不仅要考虑这几个晶粒的取向,还要考虑边界形貌,所谓考虑边界形貌就是要引进3个位置变量.对于位置-取向空间的引出和分析搭建一个数学模型并提供解决问题的思路,基于Voronio增量算法,利用C语言编程获得复合材料微观组织几何数据信息,通过OpenGL进行可视化,模拟结果再现复合材料的真实结构,为采用数值化技术对多晶体集合进行定量分析创造条件.     

5052铝合金轧制织构演变的定量分析

采用X射线衍射仪研究了5052铝合金在冷轧过程中织构的演变规律,建立了织构体积分数与轧制真应变的数学关系式。结果表明,在冷轧过程中初始的cube织构逐渐转化为纤维轧制织构,随冷轧压下量的增加,cube、r-cube、remainder和r-Goss组分的体积分数减少,而纤维组分的体积分数增加;织构体积分数与轧制真应变的数学关系式能很好地模拟铝合金轧制过程中织构的演变;分析了轧制过程中不同织构组分的演变速率,发现随轧制真应变的增加,纤维组分的形成速率先增加而后降低。     

异步轧制对IF钢冷轧及再结晶织构的影响

研究了异步轧制对IF钢的冷轧及再结晶织构的影响,并且将模拟的剪切应变随辊速比的变化规律应用到以Taylor模型为基础的织构模拟中,分析了剪切应变εxz值对形变织构的影响.结果表明:随着异步轧制速比的增加,冷轧的α纤维织构组分逐渐减少,γ纤维织构组分稍有增加.异步轧制时,附加的切应变是造成这种变化的主要原因;{111}〈uvw〉再结晶晶核的形成与{001}〈110〉织构组分无关.异步轧再结晶{111}〈112〉织构组分体积分数明显多于同步轧,这是由于在冷变形状态下,{111}〈112〉织构组分就明显高于同步轧制条件.     

脱碳退火工艺对含铌Hi-B钢组织与织构的影响

借助红外碳硫分析及EBSD技术,研究了含铌Hi-B钢在不同脱碳退火工艺处理后的碳含量及织构变化。结果表明,当炉内气氛和露点温度一定时,含铌Hi-B钢中碳含量随着脱碳温度的升高而下降,随着保温时间的延长先下降,180s以后基本稳定;经850℃×180s工艺退火后钢样的脱碳效果最佳,钢中碳含量为0.0037%。退火试样中均主要含有{411}148、{111}112和{111}110织构组分,少量的Goss晶粒零散地分布在{111}112或{411}148晶粒之间。此外,有利于Goss晶粒异常长大的Σ9及Σ13b晶界的数量,随着脱碳保温时间的延长大致呈增加的趋势,随着脱碳温度的升高先增加后减少,即在840℃退火后出现极大值。     

Copper foils with gradient structure in thickness direction and different roughnesses on two surfaces fabricated by double rolling

Copper foils with gradient structure in thickness direction and different roughnesses on two surfaces were fabricated by double rolling. The two surface morphologies of double-rolled copper foils are quite different, and the surface roughness values are 61 and 1095 nm, respectively. The roughness value of matt surface can meet the requirement for bonding the resin matrix with copper foils used for flexible printed circuit boards, thus may omit traditional roughening treatment; the microstructure of double-rolled copper foils demonstrates an obviously asymmetric gradient feature. From bright surface to matt surface in thickness direction, the average grain size first increases from 2.3 to 7.4 μm and then decreases to 3.6 μm; compared with conventional rolled copper foils, the double-rolled copper foils exhibit a remarkably increased bending fatigue life, and the increased range is about 16.2%.     

Microstructure and texture evolution in commercial-purity Zr 702 during cold rolling and annealing

Microstructure and texture evolution in commercial-purity Zr 702 during cold rolling and annealing was investigated by optical microscopy, transmission electron microscopy, and X-ray diffraction. The results showed that crystallographic slip was the predominant deformation mechanism in the early stage of deformation. Deformation twins started to form when the rolling reduction was larger than 38.9%; both the dislocation density and the number of twins increased with increasing rolling reduction. The initial texture of the Zr 702 plate consisted of the basal fiber component. During cold rolling the strength of the basal fiber first decreased and then increased with increasing rolling reduction. The cold-rolled sheets were fully recrystallized after being annealed at 550°C. The recrystallization temperature and the size of recrystallized grains decreased with increasing rolling reduction. A larger rolling reduction resulted in a higher grain growth rate when the annealing temperature increased from 550°C to 700°C. The recrystallization texture was characterized by a major basal fiber and a minor {0113}<2110> component. The strength of the recrystallization texture increased with increasing rolling reduction.     

工业纯钛板材冷轧及退火微观组织和织构演变规律

采用先进电子背散射衍射（EBSD）技术,深入研究了冷轧工艺变化和道次间退火处理对工业纯钛板材微观组织和织构演变的影响规律。通过对比不同一次冷轧变形量样品经退火和二次冷轧加工后的EBSD取向分布图、取向差角分布图和极图得知,一次冷轧产生的孪晶对退火再结晶晶粒尺寸及晶粒取向（织构）产生重要的影响,进而又影响二次冷轧的变形组织和织构特征,使二次冷轧变形孪晶的生成受到一定程度的抑制,孪晶分数随着轧制变形量的提高呈现先升高后降低的规律,同时会降低二次冷轧组织中{0001}基面织构组分。     

ASP生产Ti-IF钢在不同退火过程中再结晶组织和织构演变

对ASP生产Ti-IF钢的退火再结晶过程分别进行了罩式退火和连续退火模拟实验,通过金相组织观察和力学性能检测,并结合X射线衍射和电子背散射衍射技术,从不同的实验角度对再结晶组织和织构的形成及演变进行了研究.结果表明,由于罩式退火和连续退火两者的热历史过程不同,其再结晶组织转变温度及晶粒度有所不同,但是再结晶核心的形成位置及演变方式趋于一致,形核方式趋向于择优形核.     

Microstructure and texture evolution of Mg-3Zn-1Al magnesium alloy during large-strain electroplastic rolling

Large-strain deformation by single electroplastic rolling (EPR) was imposed on AZ31 magnesium alloy strips. During EPR at low temperature (150-250℃), numerous twins formed in the alloy. After EPR at a high temperature (350℃), the number of twins reduced and some dynamic recrystallization (DRX) grains formed at grain boundaries and twinned regions. The synergic thermal and athermal effects generated by electropulsing, which promoted dislocation motion, induced a few small DRX grains, and ductile bandings were mainly responsible for large-strain deformation during EPR. The inclination angle of the basal pole stemmed from the counterbalance of the inclination direction of the basal pole between the DRX grains and deformed coarse grains.     

金属箔材轧制过程中第二相颗粒的尺寸效应研究

金属箔材轧制时,箔材的厚度最小为几个微米.微米级甚至是亚微米量级尺寸的第二相颗粒都可能对基体的力学性能,甚至是箔材的表面形状造成影响.相对于基体而言,颗粒的软硬程度及其大小对轧制过程中箔材的影响是截然不同的.该文通过有限元模拟的方法研究了单个的硬质及软质第二相颗粒对箔材基体性能及形状的影响.论文中引入参量：颗粒直径/箔材厚度比(以下简称d/T).结果表明,箔轧时,相较于硬质颗粒而言,不同尺寸的软质颗粒对箔材的影响较大.第二相颗粒为软质颗粒时,应力集中程度及箔材表面变形程度随着颗粒尺寸的增大而增大,当d/T小于1/20时,第二相颗粒周边基体应力集中现象不明显;当d/T为1/20～1/5时,应力集中比较明显,箔材表面发生轻微变形;当d/T大于1/5时,基体中应力集中明显,箔材表面变形严重.第二相颗粒为硬质颗粒时,随着d/T的增加应力集中现象越不明显,基体表面几乎没有变形.     

薄板坯连铸连轧工艺下Hi-B钢的组织及织构

采用金相显微镜和扫描电镜研究实验室模拟薄板坯连铸连轧( TSCR)工艺试制的高磁感取向硅钢( Hi- B钢)组织、织构的演变特征. 研究发现实验室模拟薄板坯连铸连轧工艺试制的Hi-B钢热轧板显微组织及织构在厚度方向上存在不均匀性. 常化板表面脱碳层铁素体晶粒明显粗化,常化板织构基本继承了热轧板相应的织构类型,仅织构强度不同. 一次大压下率冷轧后,晶粒及其晶界沿轧向被拉长形成鲜明的纤维组织,织构主要为α纤维织构和γ纤维织构,脱碳退火后试样发生回复和再结晶现象并形成初次晶粒组织,脱碳退火后织构分布较为集中. 温度升高至1000℃时二次再结晶开始,1010℃时钢中晶粒发生异常长大,高斯织构强度达到61. 779. 成品磁感为1. 915 T,铁损为1. 067 W·kg-1 .     

Influence of texture pretreatment on cold rolling texture of ELC-BH sheet

In order to further investigate how cold rolling texture is produced in an extra low-carbon and high strength bake-hardening sheet steel (for short, hereafter, coiled ELC-BH sheet) with r value as high as 2.67, texture change in texture pretreatment and its effects on the cold rolling texture are researched by means of Orientation Distribution Funchon (ODf) method. Experimental results show that the cold rolling texture which Produces very strong {111} annealing texture actually is caused by texture change in the texture pretreatment, and the strong {111} texture obtained rough this texture pretreatment is an essential condition of engendering the cold rolling texture, while the stability of {111} texture components in cold rolling is a sufficient condition of emerging thes one.     

微量元素对高纯铝箔立方织构的影响

采用晶体取向分布函数(ODF)研究和分析了在高纯铝中分别加入不同含量的微量稀土或铍对成品高纯铝箔立方织构的影响．研究结果表明添加微量稀土和铍,能改变高纯铝箔变形织构组分含量,单独加稀土时,形变织构变化不大;在单独加铍时,其S取向{123}<634>和Cu取向{112}<111>变化较大,随铍含量增加,其S取向密度f(g)减少,Bs{110}<112>取向密度增加．再结晶退火后,随稀土加入量增加,立方织构{100}<001>取向密度增加,R织构{124}<211>取向密度减少;铍添加较少时能增加成品箔材中立方织构{100}<001>强度,但随铍含量增加,立方织构含量急剧减少,R织构强度相应增加．稀土和铍在铝中溶解度都极小,与铁等微量杂质元素可能形成化合物析出后,能净化基体,减小铁对形成立方织构的阻碍作用,促进再结晶立方取向核心的形成与长大,增加立方织构比例．     

Microstructure and texture evolution of TRC A8006 alloy by homogenization

The microstructure and texture evolution of twin-roll cast A8006 alloy by homogenization were characterized using scanning and transmission electron microscopy, and the microhardness was tested as well. According to the relationship between dendritic arm spacing and cooling rate the cooling rate of the as-cast twin-roll cast A8006 sheet of 6 mm in thickness was estimated as 1.48×103 K·s?1. It is found that the grains and the nanostructural precipitates of the twin-roll cast sheet become coarser after homogenization at 580℃ for 4 h in comparison with those after homogenization at 500℃ for 8 h. The textures formed after cold rolling and became weaker during homogenization. The increase in hardness of the as-cast twin-roll cast sheets is related to the supersaturated α-Al solid solution and fine microstructure, but the decrease in hardness after homogenization can be attributed to the coarsening of grains and Al₆Fe(Mn) precipitates.