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1.
模板法合成Ag纳米线阵列   总被引:6,自引:0,他引:6  
以多孔阳极氧化铝为模板,用乙二醇作还原剂,将Ag 在模板的纳米孔道内还原并进行限域生长,制得了Ag纳米线.用X-射线衍射光谱(XRD)、扫描电子显微镜(SEM)、透射电子显微镜(TEM)等检测手段对产物进行了表征,结果表明所得Ag纳米线具有面心立方晶体结构,纳米线阵列排列整齐,长度可达10μm,单体纳米线的直径约为60 nm,与所用模板的孔径相当.  相似文献   

2.
对于用十二烷基硫醇包覆的金纳米微粒,用Langmuir-Blodgett(LB)技术制备了二维金纳米微粒有序阵列.在单纯的硫醇包覆的金纳米微粒形成的LB膜中,由于硫醇分子之间的疏水相互作用,容易导致金纳米微粒的自组织而在LB膜中形成缺陷.为了改善金纳米微粒的成膜性能和提高金纳米微粒阵列的有序性,正十二醇作为添加剂和润滑剂加入到金纳米微粒的氯仿溶液中与金纳米微粒一起形成LB膜.用透射电子显微镜对金纳米微粒的二维阵列进行了表征.结果表明,正十二醇的加入可以有效地减少用LB技术制备的二维金纳米微粒阵列中的缺陷,提高金纳米微粒阵列的有序性.  相似文献   

3.
用MMOCAA格式(调整对流的特征线修正方法)处理半导体器件模拟的对流占优扩散问题,通过对对流项进行调整,仅增加少童计算量,使该问题既保持了全局质量守恒性质,又具有MMOC格式(特征线修正技术)的所有优点.进行了理论分析,得到了最优阶L^2模误差估计结果.  相似文献   

4.
以NH4F/乙二醇为电解液对Ti箔进行阳极氧化,通过对溶液中水的含量、氧化电压、时间等参数的控制,制备了高度有序TiO2纳米管.分别利用XRD和SEM对TiO2纳米管阵列的物相组成和形貌结构进行了表征,结合氧化过程电流密度变化探讨了TiO2纳米管的生长机理.研究结果表明:TiO2纳米管阵列的形成须经历致密氧化层的形成、多孔层的形成以及纳米管的形成与稳定生长3个阶段的演化.  相似文献   

5.
首先介绍连接池技术和预编译技术的基本概念及优点,然后通过具体实例分别介绍JSP系统中连接池 和预编译的实现方法,最后通过实验测试得出使用连接池、预编译可提高JSP系统性能的结论.  相似文献   

6.
SnO2纳米线阵列的制备及纳米器件的制作   总被引:4,自引:0,他引:4  
采用简单的溶胶-凝胶方法在多孔阳极氧化铝模板(AAM)的微孔中制备了高度有序的SnO2纳米线阵列。XRD,SEM和TEM对样品进行了结构和形貌的表征,结果表明,高度有序的SnO2纳米线具有四方相的多晶结构,纳米线连续均匀;并对SnO2纳米线阵列的生长机理进行了探讨;最后用聚焦离子束沉积设备制作了单根SnO2纳米线器件。  相似文献   

7.
研制一种基于单片机控制的便携式半导体激光器特性参数测试仪.该仪器由硬件测试电路和上层软件测试系统组成,能够测试各种封装形式的LD电特性参数和特性曲线.包括自动电流控制(ACC)、自动电压控制(AvC)、自动功率控制(APC)和自动背向光电流控制(AMC)四种驱动方式;包括集成的温控电路,能够快速精确控制LD工作温度;保护电路可以使LD免受浪涌冲击等损害;上层软件系统可以很直观绘制LD的各种特性曲线.测试系统还具有体积小、携带方便、操作简单等优点.  相似文献   

8.
An integrated semiconductor device enabling non-optical genome sequencing   总被引:4,自引:0,他引:4  
The seminal importance of DNA sequencing to the life sciences, biotechnology and medicine has driven the search for more scalable and lower-cost solutions. Here we describe a DNA sequencing technology in which scalable, low-cost semiconductor manufacturing techniques are used to make an integrated circuit able to directly perform non-optical DNA sequencing of genomes. Sequence data are obtained by directly sensing the ions produced by template-directed DNA polymerase synthesis using all-natural nucleotides on this massively parallel semiconductor-sensing device or ion chip. The ion chip contains ion-sensitive, field-effect transistor-based sensors in perfect register with 1.2 million wells, which provide confinement and allow parallel, simultaneous detection of independent sequencing reactions. Use of the most widely used technology for constructing integrated circuits, the complementary metal-oxide semiconductor (CMOS) process, allows for low-cost, large-scale production and scaling of the device to higher densities and larger array sizes. We show the performance of the system by sequencing three bacterial genomes, its robustness and scalability by producing ion chips with up to 10 times as many sensors and sequencing a human genome.  相似文献   

9.
In this paper, we report the growth and characteristics of titania nanotube arrays prepared by anodic oxidation and then annealed in an oxygen atmosphere at 500℃. The titania nanotube arrays presented high sensitivity to hydrogen gas. The crystalline phase of the samples was checked by X-ray diffraction (XRD). The differences in the nanotubes morphology attributed to the etched samples due to anodization potential, reaction time and the electrolyte concentration were analyzed by scanning electron mi- croscopy (SEM). The gas sensitive parameters of the samples were obtained from resistance, the response time and the recovery time at different temperatures.  相似文献   

10.
Highly ordered polycrystalline Si nanowire arrays were synthesized in porous anodic aluminum oxide (AAO) templates by the chemical vapor deposition (CVD) method. The morphological structure, the crystal character of Si nanowire arrays and the individual nanowire were analyzed by the transmission electron microscopy (TEM), scanning electron microscopy (SEM), atom force microscopy (AFM) and the X-ray diffraction spectrum (XRD), respectively. It is shown that most fabricated silicon nanowires (SiNWs) tend to be assembled parallelly in bundles and constructed with highly orientated arrays. This method provides a simple and low cost fabricating craftwork and the diameters and lengths of SiNWs can be controlled, the large area Si nanowire arrays can be achieved easily under such a way. The curling and twisting SiNWs are fewer than those by other synthesis methods.  相似文献   

11.
陈俊 《科学技术与工程》2012,12(10):2306-2309
采用金属催化化学腐蚀方法在单晶硅表面制备了有序的纳米线阵列,研究了纳米线长度与腐蚀时间之间的关系,发现纳米线长度随着腐蚀时间的增加而增大。测试了所制备的具有纳米线阵列的硅表面在近红外1000nm~2500nm范围内的减反射性能。测试结果表明,与未处理的光滑硅表面相比,具有纳米线阵列的表面的反射率大辐降低,并随着纳米线长度的增加,反射率减小。  相似文献   

12.
通过模板法制备的一维金属氧化物纳米结构在材料科学领域具有潜在的应用前景。以醋酸锰为前驱体,利用多孔阳极氧化铝膜(anodic aluminum oxide,AAO)为模板,通过溶胶—凝胶法成功制备出Mn3O4纳米线阵列。利用扫描电子显微镜(SEM)、X射线衍射(XRD)、热重分析技术等手段分析合成条件与产物的结构、形貌之间的关系。结果表明,所得产物为四方尖晶石结构,纳米线直径约80 nm,长度约几微米。通过测试产物的磁滞回线,发现其在常温下呈顺磁性。  相似文献   

13.
通过在半导体异质结上的上下表面沉积两条平行的铁磁条带可获得一个巨磁阻器件.为了更好地调控其性能,我们从理论上研究了在该器件中加入δ势后,该器件的透射系数、电导和磁阻比率的变化情况.研究发现,加入δ势后,该器件同样具有明显的巨磁阻效应,且其磁阻比率与加入δ势的权重和位置密切相关.因此,我们可以通过改变加入δ势的权重和位置来调控该巨磁阻器件,设计出磁阻比率可调的磁信息存储器.  相似文献   

14.
Highly ordered nickel monoxide (NiO) nanowire arrays were fabricated by sol-gel synthesis within the pores of anodic alumina membrane (AAM). Scanning electron microscopy (SEM), high resolution transmission electron microscopy (HRTEM) and X-ray diffraction (XRD) were used to characterize the topography and crystalloid structure of NiO nanowire arrays. The length and diameter of the NiO nanowires depended on the thickness of the AAM and the diameter of the pores. The results indicated that the NiO nanowires were uniformly assembled into the ordered nanopores of the AAM and paralleled to each other. Nickel monoxide nanotubes were also fabricated with the same method by changing the immersing time. This new method to prepare NiO nanowire arrays may be important from gas sensors to various engineering materials.  相似文献   

15.
16.
V A Parsegian  S L Brenner 《Nature》1976,259(5545):632-635
We examine the role of electrostatic repulsion and van der Waals' attraction in determining interviral spacings in 'equilibrium' gels of tobacco mosaic virus. The observed spacings are inconsistent with a force-balance model. Experimental probes of the role of forces are suggested.  相似文献   

17.
用于高功率半导体激光器列阵散热的微通道热沉的研制   总被引:1,自引:0,他引:1  
理论分析了微通道热沉的热阻的组成,采用微机械加工技术和铜直接粘接技术(DBC)制作了冷却大功率半导体激光器列阵的5层结构的无氧铜微通道热沉;通过测试,用其封装的808 nm线阵二极管激光器准连续输出功率达38.5 W,无氧铜微通道热沉热阻为0.645℃/W,热沉的表面温度均匀性好,能有效散热,满足散热要求.  相似文献   

18.
行政不作为的实质,是懈怠行政职责。它有行为状态和事实状态两种情形。行政不作为的形式,除传统理论归纳的拒绝、迟延、不予答复以外,还应当包括未作为、假作为和弱作为等3种形式。行政不作为的违法性,既可以表现为行为的违法,也可以表现为结果的违法。  相似文献   

19.
基于稻种胚胎定向排列的排种器及参数优化   总被引:3,自引:0,他引:3  
提出了超级稻种按胚胎部位定向排列播种的思想.利用稻种沿其长轴两个方向摩擦角不同的特性,设计了带有导向板的振动式排种器,实现稻种在振动板上有序排列,分析了稻种在排种过程中胚胎按序排列的机理.运用正交试验法研究了排种器各参数对排序效果的影响,得到各个参数的影响大小次序和一组优化的结构参数.当导向板与播种方向的夹角为35;°筛面角为21°;振幅为3.5 mm;振动方向角为10°;振动频率为3.5 Hz;导向板摩擦角顺行为57.1,°逆行为52.6°时,播种时稻种的定向排列比例为85%以上,振动板对超级稻种摩擦阻力矩的范围为1.89×10-7N.m相似文献   

20.
为了寻找更好的实现光伏发电系统最大功率点跟踪控制方法,基于仿真模型,研究了太阳能光伏电池阵列的特性。采用Matlab/Simulink模块,基于单个光伏电池的物理特性建立了太阳能光伏电池阵列的仿真模型。模型不但能分析太阳能光伏电池阵列所具有的随着光照强度和温度不同而变化的P-V和I-V非线性特性,而且可仿真太阳能光伏电池阵列工作在最大功率点以及稳定工作区域内时具有线性关系,并进行了理论推导。该模型简单明了,计算速度快。仿真结果表明:仿真与实验结果相符合,当光伏阵列工作在稳定区域内的情况下,dP/dV与I存在线性关系,模型具有通用性与实用性。  相似文献   

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