Microstructure, crystallography and nucleation mechanism of NANOBAIN steel

The microstructure of bainite ferrite in NANOBAIN steel transformed at different temperatures was investigated by scanning electron microscopy, transmission electron microscopy, electron back-scattered diffraction, and vickers hardness tester in detail. It is found that the average width of bainitic ferrite (BF) plates can be refined to be thinner with the reduction of temperature (473–573 K), and the bainitic ferrite plates can reach up to 20–74 nm at 473 K. Crystallographic analysis reveals that the bainitic ferrite laths are close to the Nishiyama-Wasserman orientation relationship with their parent austenite. Temperature shows a significant effect on the variant selection, and a decrease in temperature generally weakens the variant selection. Thermodynamic analyses indicates that the Lacher, Fowler and Guggenheim (LFG) model is more suitable than the Kaufman, Radcliffe and Cohen (KRC) model dealing with NANOBAIN steel at a low temperature range. The free energy change ΔGγ→BF is about ?1500 J·mol?1 at 473 K, which indicates that nucleation in NANOBAIN steel is the shear mechanism. Finally, the formation of carbon poor regions is thermodynamically possible, and the existence of carbon poor regions can greatly increase the possibility of the shear mechanism.     

Load compensation research on twicetension for loop anchor cable of inner lining in Yellow River-crossing tunnel

The load compensation equipment for anchor cable named low retraction prestressed anchorage system with twice-tension （referred to as twice-tension anchorage system） is proposed in the paper. Calculation results of loop anchorage prestressing loss （PL） values of inner lining （IL）in Yellow River-crossing tunnel under two anchorage systems, including twice-tension anchorage system and HM （Chinese transliteration is huanmao） anchorage system, are introduced. The software ANSYS is selected to realize the three-dimensional （3D） finite element modeling to accomplish simulation and calculation works under the two anchorage systems, respectively. Stress processes of IL under the two working conditions, of which one is completed cable tensioning （CCT） and the other is water in the tunnel with the designed water pressure （DWP）, are contrasted and analyzed. Impacts of prestressing forces of anchor cables on structural safety under the two anchorage systems are contrasted. The calculation results show that the twice-tension anchorage system can reduce PL effectively and then increase prestresses of wall concrete （WC）. Meanwhile, the anchorage system has the advantages of improving security and stability of tunnel structure, reducing project costs and saving steel consumption. The research work is available to related design and construction of anchor cable, and is worthy of promotion and application.     

Recovery of iron from copper slag by deep reduction and magnetic beneficiation

Aiming at recovering iron from high-iron-content copper slag, this article introduced a combination technology of deep reduction and magnetic beneficiation, investigated the iron recovery efficiency and optimized the technical conditions. When coke powder with 86wt% fixed carbon was used as a reductant, iron was successfully extracted from the copper slag. Under the optimized condition of the coke powder content of 14wt%, the calcium-to-silicon mass ratio (Ca/Si) of 0.2, the roasting temperature of 1300℃, the roasting time of 3 h, the grinding time of 20 min, and the magnetic field intensity of 61 kA·m?1, the iron recovery rate of the copper slag can reach 91.82%, and the extracted iron powder has an iron grade of 96.21%. With the characteristics of high iron grade and low impurity content, the extracted iron powder can be used as high-quality raw materials of weathering steel.     

Preparation of composite abrasives by electrostatic self-assembly method and its polishing properties in Cu CMP

The adsorption characteristics of cationic polyelectrolyte poly dimethyl diallyl ammonium chloride （PDADMAC） and anionic polyelectrolyte poly （sodium-p-styrenesulfonate） （PSS） on benzoguanamine formal- dehyde （BGF） particles are investigated. The charging characteristics of BGF particles are changed and con- trolled using electrostatic self-assembly method. A variety of PE,-BGF/SiO2 composite abrasives are obtained. The as-prepared samples are analyzed by zeta potential analysis, transmission electron microscope （TEM） and thermogravimetric （TG） analysis. The composite abrasive slurries are prepared for copper polishing. The poli- shing results indicate that it is SiO2 abrasives, not only coated SiO2 abrasive on polymer particles but also free SiO2 abrasive in slurry, that offer the polishing action. The material removal rates of copper polishing are 264 nm/min, 348 nm/min and 476 nm/min using single SiO2 abrasive slurry, PE0-BGF/SiO2 mixed abrasive slur- ry and PE3-BGF/SiO2 composite abrasive slurry, respectively. The surface roughness Ra of copper wafer （with 5μm×5μm district） is decreased from 0.166 μm to 3.7 nm, 2.6 nm and 1.5 nm, and the surface peak-valley values Rrv are less than 20 nm, 14 nm and 10 nm using these kinds of slurries, respectively. Key words ： chemico-mechanical polishing; polishing slurry; composite abrasives ; polyelectrolyte ; copper     

Exploration on ecological regulation of the reservoirs

Reservoir regulation process in the Yangtze River basin is mainly divided into two types of flood regulation and initiating benefit regulation. The present reservoir management system and operation mode are mainly for dealing with or coordinating of flood control and benefit initiation as well as benefit distribution among various beneficial functions. From the view point of river ecosystem protection, the current regulation mode has two kinds of problems ： firstly, most of the reservoir regulation plans do not consider ecosystem protection at downstream of dams and needs of environment protection in reservoir areas; secondly, integrated regulation or management of water resources is ignored. It is very necessary to improve reservoir regulation mode, bearing problems faced by regulation of the Three Gorges reservoir and issues related to cascade development and regulation in Tuojiang and Minjiang River basins in mind. In accordance with the concept of scientific development, and the philosophy of ＂ensuring a healthy Yangtze River and promoting the harmony between human and water＂, taking flood control, benefit initiation and eco-system as a whole, this paper put forward the basic consideration to improve reservoir regulation as follows ： on the basis of requirements of ecosystem protection at downstream of dams and needs of environment protection in reservoir areas, we should bring the functions of reservoir such as flood control and benefit initiation into full play, control the negative influence to the ecosystem at downstream of dams and the environment in reservoir areas in an endurable scope, and restore the ecosystem and the environment step by step. This paper put forward the relevant regulation process aiming at the idiographic problems such as protection of ecosystem at downstream of dams and environment in reservoir areas, protection of aquatic wildlife species and fish species, regulation of sediment and protection of wetland.     

Influence of Te doping on the dielectric and optical properties of InBi crystals grown by directional freezing

Stoichiometric pure and tellurium (Te) doped indium bismuthide (InBi) were grown using the directional freezing technique in a fabricated furnace. The X-ray diffraction profiles identified the crystallinity and phase composition. The surface topographical features were observed by scanning electron microscopy and atomic force microscopy. The energy dispersive analysis by X-rays was performed to identify the atomic proportion of elements. Studies on the temperature dependence of dielectric constant (?), loss tangent (tanδ), and AC conductivity (σ_ac) reveal the existence of a ferroelectric phase transition in the doped material at 403 K. When InBi is doped with tellurium (4.04 at%), a band gap of 0.20 eV can be achieved, and this is confirmed using Fourier transform infrared studies. The results thus show the conversion of semimetallic InBi to a semiconductor with the optical properties suitable for use in infrared detectors.     

Subsurface macro-inclusions and solidified hook character in aluminum-killed deep-drawing steel slabs

Subsurface macro-inclusions and hooks are detrimental to the surface quality of deep-drawing steel sheets. However, little is known about the relationship between macro-inclusions and hooks. Thus, in this work, two ultralow carbon (ULC) steel slabs and two low carbon (LC) aluminum-killed steel slabs were sampled to study the relationship between hooks and subsurface macro-inclusions, which were detected on the cross-sections of steel samples with an area of 56058 mm2 using an automated scanning electron microscopy/energy-dispersive X-ray spectroscopy system. Results show that subsurface inclusions larger than 200 μm were almost entrapped by hook structures, whereas the location of other inclusions smaller than 200 μm had no obvious dependence on the location of solidified hooks. Furthermore, the number density (ND) of subsurface inclusions larger than 200 μm decreased from 0.02 to 0 cm-2 in ULC steel as the mean hook depth decreased from 1.57 to 1.01 mm. Similar trends were also observed in LC steel. In addition, the detected inclusions larger than 200 μm were concentrated in the region near the slab center (3/8 width-5/8 width), where hook depths were also larger than those at any other locations. Therefore, minimizing the hook depth is an effective way to reduce inclusion-induced sliver defects in deep-drawing steels.     

Automatic Collecting Representative Logo Images from the Internet

With the explosive growth of commercial Iogos, high quality logo images are needed for training logo detection or recognition systems, especially for famous Iogos or new commercial brands. This paper focuses on automatic collecting representative logo images from the internet without any human labeling or seed images. We propose multiple dictionary invariant sparse coding to solve this problem. This work can automatically provide prototypes, representative images, or weak labeled training images for logo detection, logo recognition, trademark infringement detection, brand protection, and ad-targeting. The experiment results show that our method increases the mean average precision for 25 types of Iogos to 80.07% whereas the original search engine results only have 32% representative logo images. The top images collected by our method are accurate and reliable enough for practical applications in the future.     

Dynamic recrystallization and precipitation in high manganese austenitic stainless steel during hot compression

Dynamic recrystallization and precipitation in a high manganese austenitic stainless steel were investigated by hot compression tests over temperatures of 950–1150℃ at strain rates of 0.001 s?1-1 s?1. All the flow curves within the studied deformation regimes were typical of dynamic recrystallization. A window was constructed to determine the value of apparent activation energy as a function of strain rate and deformation temperature. The kinetics of dynamic recrystallization was analyzed using the Avrami kinetics equation. A range of apparent activation energy for hot deformation from 303 kJ/mol to 477 kJ/mol is obtained at different deformation regimes. Microscopic characterization confirms that under a certain deformation condition (medium Zener-Hollomon parameter (Z) values), dynamic recrystallization appears at first, but large particles can not inhibit the recrystallization. At low or high Z values, dynamic recrystallization may occur before dynamic precipitation and proceeds faster. In both cases, secondary phase precipitation is observed along prior austenite grain boundaries. Stress relaxation tests at the same deformation temperatures also confirm the possibility of dynamic precipitation. Unexpectedly, the Avrami’s exponent value increases with the increase of Z value. It is associated with the priority of dynamic recrystallization to dynamic precipitation at higher Z values.     

Effects of basicity and MgO content on the viscosity of the SiO2-CaO-MgO-9wt%Al2O3 slag system

The effects of basicity and MgO content on the viscosity of SiO2-CaO-MgO-9wt%Al2O3 slags with basicity from 0.4 to 1.0 and MgO content from 13wt%to 19wt%were investigated using the rotating cylinder method. A correlation between the viscosity and the slag structure was determined by Fourier transform infrared （FTIR） spectroscopy. It is indicated that the complex network structure of the slag melt is depolymerized into simpler network units with increasing basicity or MgO content, resulting in a continuous decrease in viscosity of the slag. The viscosity is strongly dependent on the combined action of basic oxide components in the slag. Under the present experimental conditions, increasing the basicity is found to be more effective than increasing the MgO content in decreasing the viscosity of the slag. At higher temperatures, the increase of basicity or MgO content does not appreciably decrease the viscosity of the slag, as it does at lower tem-peratures. The calculated activation energy of viscous flow is between 154 and 200 kJ＆#183;mol-1, which decreases with an increase in basicity from 0.4 to 1.0 at a fixed MgO content in the range of 13wt%to 19wt%.     

Influence of Al on the magnetostriction of Fe-Ga polycrystal alloys under compressive stress

Fe₈₀Ga_20?xAl_x (x = 0, 6, 9, 14) ingots were prepared from high purity elements using a vacuum induction system. X-ray diffraction patterns show that the alloys are A2 disordered structures. The influence of the partial substitution of Ga in Fe-Ga alloys with Al on their magnetostrictive properties was investigated, and the effects of different heat treatment conditions on the magnetostriction and microstructure of the alloy rods were also examined. The saturation magnetostriction value of Fe₈₀Ga₂₀ can reach to 240·10?6 under a compressive stress of 20 MPa. The Fe₈₀Ga₁₁Al₉ alloy has many good properties, such as low hysteresis, high linearity of the magnetostriction curve, and low saturated magnetic field, which make it a potential candidate for magnetostrictive actuator and transducer applications. It is found that subgrains have little influence on the magnetostriction of Fe-Ga alloys.     

Low Cost Fabrication of Parallel Grid Electrode Group for Carbon Nanotube Field Emission Display

Based on simple screen printing technique,the parallel grid electrode group was developed. One grid electrode included the left and the right branch electrodes,which were formed with the solidified silver slurry on grid substrate. Under one anode pixel,the left and the right branch electrodes would control respectively the electron emission of two independent carbon nanotube （CNT） field emitters on the same cathode electrode. With the parallel grid electrode group, the capacitance effect between grid-cathode electrodes would be reduced due to the decreased grid electrode fabrication area. And the service life of field emission display （FED） could be prolonged owing to the existence of spare branch electrode. Using CNT as field emitter,the FED with parallel grid electrode group was fabricated,which possessed better grid control performance, high luminescence image brightness, and low fabrication cost. The turn-on electric-field was 2. 13 V /mm and the maximum field emission current had reached 1 506. 2 mA.     

Optimization of Culture Components for Laccase Activity from Pleurotus Ostreatus P40 Using Response Surface Methodology

High enzymatic activity is required for laccase applications.Central composite design （CCD）-based response surface methodology （RSM） can effectively increase the enzymatic activity of Pleurotus ostreatus P40 in liquid substrate fermentation.Initial screening of the nutritional components was performed using a Plackett-Burman design.The variables,namely,bran,bagasse,Tween 80,and yeast extract,were found to have statistically significant effects on laccase activity.These variables were further optimized using CCD-based RSM.Optimal concentrations for the maximum laccase activity were 8.144 2 g/L bran,50 g/L bagasse,0.424 1 mL/L Tween 80,and 2.832 5 g/L yeast extract.Under optimized conditions,the maximum measured laccase activity reached 96 480 U/L,which was close to the predicted value （104 830 U/L） by RSM.Therefore,RSM can be used to optimize culture components for laccase activity from Pieurotus ostreatus P40.     

General design of Sutong Bridge

The main span of Sutong Bridge is a double-pylon, double-plane cable-stayed bridge with steel box girder, which has the world＇ s longest central span of 1 088 m within cable-stayed bridges. To overcome problems caused by severe meteorological conditions, perplexing hydrological conditions, deep buried bedrock and higher navigation level, many new technics and methods were created. Keys including structural system, steel box girder, stayed cable, tower, pier, tower foundation, collision avoidance system, wind-resistance, seismic-resistance, structural nonlinear response and structural static stability were presented individually in this paper.     

The principle of minimization of the equivalent load for design of launching vertical shiplift

Launching vertical shiplift is a type of shiplifts which have the advantages in characteristics of dynamics and statics, safety and simplicity in operation. But their applications are limited as the scales of mechanical equipments are too large. This paper puts forward the principle of minimization of the equivalent load for the general layout design of launching vertical shiplifts, based on the analysis of the load probability of the main hoists and their key mechanical equipments. The principle aims at determining the optimal weight of counterweight so that the equivalent loads of the main hoists of shiplifls are minimized, and larger ships are permitted to pass through. The theory and method presented in this paper have been applied in the design of the first step and third step shiplifts of the Goupitan Hydro Power Station. This has resulted in the breakthrough of the design and manufacture of launching vertical shiplifts so that the ships with tonnage of 500 t can pass through hydro dams for this type of shiplifts, comparing with the largest launching shiplift in Yantan Hydro Power Station with the 250 t shiplift.     

A Rhodamine-Based Sensor-for Chromogenic Detection of Cu^2＋ and Fluorescent Detection of Fe^3＋

A rhodamine-benzimidazole conjugate(RB) as a probe was investigated.UV-Vis analysis showed that a strong absorption band at 552 nm was formed with the addition of Cu~(2+),while other transition metal ions induced a little more absorption.The absorption value of RB solution at 552 nm has a linear correlation with Cu~(2+) concentration between 35-70 μmol/L;the detection limit reached 6.82×10~(-2) μmol/L,which is lower than the settled limitation for copper in the drinking water(~30 μmol/L) standardized by World Health Organization(WHO).Moreover,FL analysis showed that only Fe~(3+) could induce large fluorescence intensity enhancement at 582 nm;other common metal ions including Cu~(2+) cannot induce the enhancement.There was a good linear correlation between relative fluorescence intensity and Fe~(3+) concentration ranging from 2 μmol/L to 20 μmol/L,and the detection limit reached1.70×10~(-2) μmol/L.The results showed that RB could detect Cu~(2+)and Fe~(3+) simultaneously,with the UV-Vis and fluorescence spectroscopy,respectively.     

Cascading failure prevention of complex systems based on brittleness entropy game

A non-cooperative game model based on brittleness entropy is formulated for preventing cascading failure of complex systems.Subsystems of a complex system are mapped to the players of the game.The influence of collapsed subsystems to other subsystems is also taken into account in the definition of payoff function except for their own entropy increase.This influence is named brittleness entropy.Each player has two optional strategies：rational for negative entropy and irrational for negative entropy.The model is designed to identify the players who select an irrational strategy for negative entropy.The players who select the irrational strategy for negative entropy continue to compete for negative entropy after the recovery of ordered state and make other subsystems can＇ t get enough negative entropy to reduce entropy increase.It leads to cascading failure of the complex system in the end.Genetic algorithm is used to seek the solution of game model,and the simulation result verifies the effectiveness of the proposed model.The model provides a new way to prevent cascading failure of complex systems.     

Reality over Web： Pervasive Computing Meets the Web

Reality over Web （ROW） is a novel concept, where a window on the web corresponds to a window onto a real space. Once the correspondence is established, users should be able to interact or manipulate the objects or people in the real space through the web window. In this paper, we introduce the RoW concept and highlight the principles that govern its design and implementation. A system architecture for realizing the RoW concept is described along with a proof-of-concept prototype that implements portions of the RoW concept. One essential part of an RoW implementation is accurate Iocationing of objects and people in a video frame. The Iocationing problem becomes particularly challenging because we want to reuse existing infrastructure as much as possible. We developed a high-frequency sound-based Iocationing scheme and implemented it on the prototype. The results from initial experiments performed on the Iocationing scheme are reported here.     

Cross-layer resource allocation based on potential game theory in multi-cell OFDMA networks

A cross-layer resource allocation scheme based on potential game （CLRA _ PG） is proposed for the downlink multi-cell orthogonal frequency-division multiple-access （OFDMA） system with universal frequency reuse.As a method to mitigate inter-cell interference （ICI）,base station coordination has been considered.In the process of the objective function modeling,this paper adopts a pricing mechanism which not only maximizes the individual utility but also considers the interference to other users.Based on the potential game theory,the objective problem is converted to a potential function which can be easily solved.The Karush-Kuhn-Tucker （KKT） conditions and the iterative water-filling algorithm are employed to solve the constraint objective optimization problem.Moreover,extensive simulations are conducted to evaluate how the pricing factors affect the algorithm.At the same time,comparing with the traditional policy,our simulation results show that the proposed scheme can significantly improve the performance of the system.