水／NaDEHP／正庚烷微乳体系中水结构的FT—IR研究

运用傅立叶变换红外光谱（ＦＴ－ＩＲ）对水／ＮａＤＥＨＰ／正同乳体系中水的微结构进行了研究。结果表明：随着体系中加水量的增大，水分子Ｏ－Ｈ伸缩振动红外吸收峰的频率由３３８５ｃｍ＾－１向高频在移动至３４１７ｃｍ＾－１（与ＡＯＴ形成的乳体系的变化趋势相反）。进一步地３０５０ｃｍ＾－１至３７５０ｃｍ＾－１范围内的水Ｏ－Ｈ伸缩振动吸收峰进行曲线拟合，得到４个子峰，说明微乳体系中的水分子存在有４种不同的配位环     

氮化碳薄膜的红外吸收光谱（FTIR）研究

测量了采用ＲＦ－ＣＶＤ方法制备的氮化碳薄膜的ＦＴＩＲ曲线，膜层中的Ｃ－Ｎ键、石墨相、Ｃ＝Ｎ键和Ｃ≡Ｎ键的红外吸收峰波数分别为１２５０ｃｍ＾－１，１５７６ｃｍ＾－１，１６８７ｃｍ＾－１和２０５４ｃｍ＾－１。采用技术措施避免石墨相析出的氮化碳薄膜，其红外吸收谱只出现了Ｃ－Ｎ键的伸缩振动吸收峰（９４８ｃｍ＾－１），薄膜中的其它功能基团的存在对Ｃ－Ｎ键的振动频率有一定的影响。     

CO为探针分子的原位FT—IR技术研究Pd／HM表面金属的分散态

以ＣＯ探针分子的ＩＲ研究表明,在Ｐｄ／ＨＭ上,钯还原前后具有不同对ＣＯ的线式吸附态。还原前分别在２１５６ｃｍ＾－１和２０４５ｃｍ＾－１处有两个ＩＲ吸收峰;而还原后在２０００ｃｍ＾－１附近出现几个重叠在一起的ＩＲ吸收峰,２１５６ｃｍ＾－１处小峰几乎消失,这是因为Ｐｄ＾２＋ＰＵＨＣＧＩＰ ＤＲ ＸＨ ＦＨＮ Ｒ     

聚吡咯苯甲烯及其铜螯合物的红外光谱表征

用红外光谱研究吡咯、苯甲醛在常温和酸催化条件下缩聚合成的新型大π共轭高分子，红外光谱信息表明，醛基（２７３４、１７０１ｃｍ－１）已经消失，出现了与苯环共轭的α－碳双键取代基（１５７６ｃｍ－１）和吡咯环的－Ｃ＝Ｎ－键（１４９１ｃｍ－１）．这意味着产物为聚吡咯苯甲烯．吡咯Ｎ－Ｈ（３４２３ｃｍ－１的消失和Ｃ－Ｈ面内变形振动频率的特征位移，启示了含铜产物为聚吡咯苯甲烯一铜螯合物．     

碱土金属邻苯二甲酸氢盐的振动光谱

测定了碱土金属邻苯二甲酸氢盐的晶体结构，Ｃａ（Ｃ８Ｈ５Ｏ４）２．２Ｈ２Ｏ为正交晶系，属Ｃ２ｖ＾７－Ｐｍｎ２１（Ｎｏ．３１）空间群，晶胞参数为α＝２．７４８２，ｂ＝０．９４２５，ｃ＝０．６９２６ｎｍ，Ｚ＝４；Ｓｒ（Ｃ８Ｈ５Ｏ４）２．２Ｈ２Ｏ是正交晶系，属Ｃ２ｖ＾１＾２－Ｃｍｃ２１（Ｎｏ．３６）空间群，晶胞参数为α＝２．８４６５，ｂ＝０．８７９，ｃ＝０．６９８０ｎｍ，Ｚ＝４，Ｂａ（Ｃ８Ｈ５Ｏ４）２．Ｈ     

高温热解聚硅烷制备SiC薄膜初探

用组合成的可溶性聚硅烷１７１０Ａ作涂膜材料,进行不同温度的真空热解或高纯氮下热解实验。通过ＩＲ谱和ＸＰＳ谱分析,在７９０－８１０ｃｍ＾－１和１２７０ｃｍ＾－１红外吸收特征峰分别对应Ｓｉ－ＣＨ３摇摆振动和伸缩振动吸收峰,ＸＰ－Ｓｉ谱给出Ｓｉ（２Ｐ）结合能力为１０１．６ｅＶ,ＣＩＳ为２８４．３ｅＶ,证明有α－ＳｉＣ：Ｈ生成。     

复合增聚型铁铝无机高分子絮凝剂PAFCS的红外光谱研究

利用煤矸石及硫铁矿渣制备出了一种新型无机高分子絮凝剂聚硫酸氯化铁铝（ＰＡＦＣＳ），研究了ＰＡＦＣＳ的红外（ＩＲ）光谱结构特征．ＩＲ谱分析表明ＰＡＦＣＳ是Ｆｅ（Ⅲ）十Ａｌ（Ⅲ）与羟基（－ＯＨ）以双羟桥为主结构连接的较复杂的高聚物．其ＩＲ图谱峰形与α－Ｆｅ２Ｏ３，α－ＦｅＯＯＨ及Ｆｅ（ＯＨ）３等明显不同．比较了ＰＡＦＣＳ，ＰＡＣ，ＰＦＳ，ＰＡＣＳ的光谱特征，表明ＰＡＦＣＳ与已知文献报道的絮凝剂ＰＡＣ，ＰＦＳ，ＰＡＣＳ有类似性，即由３１００～３６００ｃｍ（－１）处的ＯＨ伸缩振动及１６００～１６５０ｃｍ（－１）Ｈ－Ｏ－Ｈ弯曲振动的畸变，表明有结构羟基存在；在１１００ｃｍ（－１）附近Ｍ－ＯＨ－Ｍ伸缩振动峰为中等强度峰，证明有铁羟基或铝羟基以及聚合态存在．     

ZnCl2与POM的合成和结构

ＺｎＣｌ２与ＰＯＭ生成１：２加成物「Ｚｎ（ＰＯＭ）２Ｃｌ２」，Ｃ１２Ｈ１２Ｃｌ２Ｎ４Ｏ６Ｚｎ，晶体必三科晶系，空间群为Ｐ１，晶胞系数为ａ＝１１．７５５（１１）×１０＾－１０ｍ，ｂ＝１２．３５７４（７）×１０＾－１０ｍ，ｃ＝６．５９２（４）×１０＾－１０ｍ，ａ＝１０２。７３２（５）°，β＝９２．０７４（６）°，γ＝１１０．１２４（６０°，Ｖ＝８７６．２×１０＾－３０ｍ，ＭＲ＝４４４．５３，ｚ＝２，ｄ     

负载型水相膦铑配合物催化剂上丙烯氢甲酰化制丁醛

用连续流动加压微反－色谱装置评价了负载型水溶性膦铑催化剂对丙烯氢甲酰化制丁醛的反应活性，结果表明，催化剂活性与体系与中水含量密切相关，适量的水可使催化剂活性明显提高，原位红外光谱考究结果显示，当催化剂吸附ＣＯ时在２０４０，２０１２，１９０１ｃｍ＾－１等处出现一系列可归属于可逆吸附ＣＯ物种的伸缩振动带；通和原料气丙烯／ＣＯ／Ｈ２时，很快可观察到－１７１４ｃｍ＾－１附近的醛基吸收峰。     

高吸水聚丙烯酸钠的表征

对高吸水聚丙烯酸钠进行了ＦＴＩＲ、ＤＳＣ、热稳定性、吸湿性能的分析,结果表明：在１６２９ｃｍ＾－１,１５６２ｃｍ＾－１,１４５７ｃｍ＾－１处出现－ＣＯＯＮａ的羰基伸缩振动峰,在１４０７ｃｍ＾－１出现了－ＣＯＯＨ的羰基弯曲振动峰;残留水分对高吸水聚丙烯酸钠有很大的增塑作用,很难用ＤＳＣ直接对其Ｔｇ进行表征;高吸水聚丙烯酸钠具有良好的热稳定性和较高的吸湿性,并发现水湿在０．５～９９℃范围内对高吸水聚丙     

Markedness and its Interpretation in Language Use

Language markedness is a common phenomenon in languages, and is reflected from hearing, vision and sense, i.e. the variation in the three aspects such as phonology, morphology and semantics. This paper focuses on the interpretation of markedness in language use following the three perspectives, i.e. pragmatic interpretation, psychological interpretation and cognitive interpretation, with an aim to define the function of markedness.     

Lower Paleozoic oil relationships within Williston Basin, Canada

The Williston Basin is a significant petroleum province, containing oil production zones that include the Middle Cambrian to Lower Ordovician, Upper Ordovician, Middle Devonian, Upper Devonian and Mississippian and within the Jurassic and Cretaceous. The oils of the Williston Basin exhibit a wide range of geochemical characteristics defined as "oil families", although the geochemical signature of the Cambrian Deadwood Formation and Lower Ordovician Winnipeg reservoired oils does not match any "oil family". Despite their close stratigraphic proximity, it is evident that the oils of the Lower Palaeozoic within the Williston Basin are distinct. This suggests the presence of a new "oil family" within the Williston Basin. Diagnostic geochemical signatures occur in the gasoline range chromatograms, within saturate fraction gas chromatograms and biomarker fingerprints. However, some of the established criteria and cross-plots that are currently used to segregate oils into distinct genetic families within the basin do not always meet with success, particularly when applied to the Lower Palaeozoic oils of the Deadwood and Winnipeg Formation.     

An Analysis of Catherine＇s Character——Wuthering Heights

Wuthering Heights, Emily Bronte＇s only novel, was published in December of 1847 under the pseudonym Ellis Bell. The book did not gain immediate success, but it is now thought one of the finest novels in the English language. Catherine is the key character of this masterpiece, because everybody and everything center on her though she had a short life. We can understand this masterpiece better if we know Catherine well.     

Characterization of Ordovician carbonate reservoirs, southeastern Saskatchewan, Canada

The discovery of the prolific Ordovician Red River reservoirs in 1995 in southeastern Saskatchewan was the catalyst for extensive exploration activity which resulted in the discovery of more than 15 new Red River pools. The best yields of Red River production to date have been from dolomite reservoirs. Understanding the processes of dolomitization is, therefore, crucial for the prediction of the connectivity, spatial distribution and heterogeneity of dolomite reservoirs.The Red River reservoirs in the Midale area consist of 3～4 thin dolomitized zones, with a total thickness of about 20 m, which occur at the top of the Yeoman Formation. Two types of replacement dolomite were recognized in the Red River reservoir: dolomitized burrow infills and dolomitized host matrix. The spatial distribution of dolomite suggests that burrowing organisms played an important role in facilitating the fluid flow in the backfilled sediments. This resulted in penecontemporaneous dolomitization of burrow infills by normal seawater. The dolomite in the host matrix is interpreted as having occurred at shallow burial by evaporitic seawater during precipitation of Lake Almar anhydrite that immediately overlies the Yeoman Formation. However, the low δ18O values of dolomited burrow infills (-5.9‰～ -7.8‰, PDB) and matrix dolomites (-6.6‰～ -8.1‰, avg. -7.4‰ PDB) compared to the estimated values for the late Ordovician marine dolomite could be attributed to modification and alteration of dolomite at higher temperatures during deeper burial, which could also be responsible for its 87Sr/86Sr ratios (0.7084～0.7088) that are higher than suggested for the late Ordovician seawaters (0.7078～0.7080). The trace amounts of saddle dolomite cement in the Red River carbonates are probably related to "cannibalization" of earlier replacement dolomite during the chemical compaction.     

Features of Women's language

Language is a means of verbal communication. People use language to communicate with each other. In the society, no two speakers are exactly alike in the way of speaking. Some differences are due to age, gender, statue and personality. Above all, gender is one of the obvious reasons. The writer of this paper tries to describe the features of women＇s language from these perspectives： pronunciation, intonation, diction, subjects, grammar and discourse. From the discussion of the features of women＇s language, more attention should be paid to language use in social context. What＇s more, the linguistic phenomena in a speaking community can be understood more thoroughly.     

Design and analysis of generic LBS application developing platform

Location based services is promising due to its novel working style and contents.A software platform is proposed to provide application programs of typical location based services and support new applications developing efficiently. The analysis shows that this scheme is easy implemented, low cost and adapt to all kinds of mobile nework system.     

橡胶颗粒沥青混合料低温抗裂性试验研究

以AC-13级配为基础,将橡胶颗粒代替部分集料掺入混合料中,以低温弯曲试验为评价方法对不同橡胶颗粒掺量下沥青混合料的低温抗裂性进行研究,并引入应变能密度值对混合料的低温抗裂性进行综合评价.试验结果表明:橡胶颗粒沥青混合料试件的破坏微应变均超过2 300,满足冬寒区的技术指标;无论是否掺加橡胶颗粒,随着温度的下降,沥青混合料破坏时的最大弯拉强度增大,弯拉应变降低,劲度模量增大;弯曲应变能密度在胶粒掺量为1%左右时具有较大的弯曲应变能密度值,此时橡胶颗粒沥青混合料具有较好的低温抗裂性.     

A computer generator for randomly layered structures

AcomputergeneratorforrandomlylayeredstructuresYUJia shun1,2,HEZhen hua2(1.TheInstituteofGeologicalandNuclearSciences,NewZealand;2.StateKeyLaboratoryofOilandGasReservoirGeologyandExploitation,ChengduUniversityofTechnology,China)Abstract:Analgorithmisintrod…     

低渗透非均质砂岩油藏启动压力梯度研究

理论推导与室内实验相结合,建立了低渗透非均质砂岩油藏启动压力梯度确定方法。首先借助油藏流场与电场相似的原理,推导了非均质砂岩油藏启动压力梯度计算公式。其次基于稳定流实验方法,建立了非均质砂岩油藏启动压力梯度测试方法。结果表明:低渗透非均质砂岩油藏的启动压力梯度确定遵循两个等效原则。平面非均质油藏的启动压力梯度等于各级渗透率段的启动压力梯度关于长度的加权平均;纵向非均质油藏的启动压力梯度等于各渗透率层的启动压力梯度关于渗透率与渗流面积乘积的加权平均。研究成果可用于有效指导低渗透非均质砂岩油藏的合理井距确定,促进该类油藏的高效开发。     

Quantitative trait loci （QTLs） for quality traits related to protein and starch in wheat

Quality traits in wheat （Triticum aestirum L.） were studied by quantitative trait locus （QTL） analysis in a recombinant inbred line （RIL） population, a set of 131 lines derived from Chuan 35050 × Shannong 483 cross （ChSh）. Grains from RILs were assayed for 21 quality traits related to protein and starch. A total of 35 putative QTLs for 19 traits with a single QTL explaining 7.99-40.52% of phenotypic variations were detected on 10 chromosomes, 1D, 2A, 2D, 3B, 3D, 5A, 6A, 6B, 6D, and 7B. The additive effects of 30 QTLs were positive, contributed by Chuan 35050, the remaining 5 QTLs were negative with the additive effect contributed by Shannong 483. For protein traits, 15 QTLs were obtained and most of them were located on chromosomes 1 D, 3B and 6D, while 20 QTLs for starch traits were detected and most of them were located on chromosomes 3D, 6B and 7B. Only 7 QTLs for protein and starch traits were co-located in three regions on chromosomes 1D, 2A and 2D. These protein and starch trait QTLs showed a distinct distribution pattern in certain regions and chromosomes. Twenty-two QTLs were clustered in 6 regions of 5 chromosomes. Two QTL clusters for protein traits were located on chromosomes 1D and 3B, respectively, three clusters for starch traits on chromosomes 3D, 6B and 7B, and one cluster including protein and starch traits on chromosome 1D.