2519铝合金热压缩变形过程的动态与静态软化行为

在Gleeble-1500热力模拟机上,采用双道次间隙式等温热压缩试验,对2519铝合金多道次热压缩变形过程中动态与静态软化特性进行了研究,变形温度为300～500 ℃,应变速率为0.05～5.00 s-1,两道次间隙时间在30～120 s内变化,每道次应变控制在0.4.研究结果表明:在500 ℃时,2519铝合金流动应力由于结构软化而存在相当强的动态软化和奇异的静态软化,导致第2道次的起始流动应力比前一道次的起始流动应力低;在热压缩变形道次间保温停歇后,流变应力出现明显的软化现象,保温停歇时间越长,合金软化率越高;变形及停歇保持温度越高,合金软化越严重.     

冷轧Mg-9Li-1Zn合金的退火热处理工艺

以改善冷轧Mg-Li系合金的变形能力为目的,系统研究了冷轧变形后的Mg-9Li-1Zn合金的退火热处理工艺,分析了退火温度和退火时间对合金组织和性能的影响.研究结果表明:Mg-9Li-1Zn合金适宜的退火温度为280~300℃,退火温度过高会出现晶粒长大,表面脱锂等现象.300℃退火60 min后,合金的维氏硬度值为426.7 MPa,充分完成再结晶软化的合金在后续冷轧时总变形率可达70%.合金的退火时间以保证α相的充分球化及组织的均匀化为准则,实验中确定的最佳退火制度为300℃保温60 min.     

变形量对Cu-Ni-Si合金再结晶行为的影响

对经过二级变形时效处理后的Cu-Ni-Si合金进行不同变形量的冷变形后,再进行退火处理,研究了变形量对合金抗软化性、再结晶组织和再结晶动力学行为的影响。研究结果表明:再结晶晶粒在晶界处形成,大的变形量能够提高再结晶的形核速率。经40%变形的合金的软化温度为470℃,再结晶温度在550℃左右;在400℃退火时,合金发生再结晶的激活能为162 kJ/mol。再结晶的激活能随变形量的增加而降低,当变形量由40%增至80%时,再结晶激活能由162 kJ/mol降至140 kJ/mol。     

带钢连续退火温度场数值模拟及其再结晶规律研究

利用有限元软件建立几何模型和有限元模型,对42CrMo带钢高温连续退火温度场进行数值模拟,通过稳态条件下带钢温度及再结晶软化率随时间变化规律的计算,研究非稳态条件下再结晶软化率随时间变化的关系。     

大变形量Al-Zn-Mg-Cu合金的热轧板再结晶行为

采用光学显微镜、维氏硬度计和透射电子显微镜研究Al-Zn-Mg-Cu合金大变形热轧板退火过程中的组织演变和力学性能变化,探讨再结晶形核和长大机制,并通过分析位错和储存能变化规律研究动态回复对再结晶的影响。研究结果表明:Al-Zn-Mg-Cu合金在390℃热轧变形时,其主要软化机理为动态回复;当变形至90%时,其组织由直径为0.3～0.6μm的位错胞和亚晶组成,这种回复时发生的多边形化促进了随后退火过程中静态再结晶的进行。根据硬度曲线和组织分析确定总变形量为90%的Al-Zn-Mg-Cu热轧板再结晶起始温度为400℃,完全再结晶温度为420℃;超过450℃时再结晶晶粒明显长大,再结晶形核机制以亚晶合并形核为主。     

Al-Mn-Si-X合金的再结晶行为研究

对Al-Mn-Si-X合金进行不同温度和不同时间的退火,采用金相显微镜（OM）、扫描电子显微（SEM）和电导率仪对不同状态的合金组织进行观察、能谱（EDS）分析和电导率测试,研究Al-Mn-Si-X合金的再结晶行为.结果表明：随着退火温度的升高,再结晶晶粒尺寸越来越小.Al-Mn-Si-X合金的再结晶晶粒大小主要受再结晶形核数量的影响,再结晶后期的晶粒长大现象不明显.Al-Mn-Si-X合金存在着大量细小弥散的AlMnSi/AlMnSiFe析出相,这些析出相强烈抑制了再结晶形核和再结晶后期的晶粒长大.当退火温度低时,形核激活能较大,形核率低,再结晶晶粒粗大;当退火温度高时,形核激活能较小,形核率增加,再结晶晶粒细小.     

热处理参数对异步轧制硅钢极薄带三次再结晶的影响

采用常规和异步轧制分别将0 3mm厚的成品取向硅钢板冷轧到0 10mm以下,然后在不同气氛的热处理炉中进行三次再结晶高温退火,研究同步、异步轧制条件下,热处理工艺参数(退火温度、保温时间、退火气氛、升温速度)对取向硅钢极薄带的磁性能和三次再结晶行为的影响·结果表明,相同的工艺参数下,真空退火的硅钢极薄带的磁性能优于氢气处理的;退火温度越高,保温时间越长,升温速度越快,磁性能越好,三次再结晶发展得越完善·     

42CrMo钢形变奥氏体的静态再结晶

利用双道次热压缩的方法,在Gleeble-1500热模拟实验机上研究42CrMo钢在高温变形道次间隔时间内的静态软化行为.讨论变形温度、应变速率、变形程度与初始奥氏体晶粒尺寸对其静态再结晶行为的影响.根据实验结果,建立42CrMo钢静态再结晶动力学模型,相应的静态再结晶激活能约为187.68 kJ/mol.结果表明:变形程度对42CrMo钢的静态再结晶影响最大,变形温度和应变速率次之,初始奥氏体晶粒尺寸对其影响较小;在变形温度较低(850 ℃)时,随着道次间隔时间的增加,静态再结晶分数逐渐趋于稳定(约为0.4),这是因为在变形温度较低时,道次间不能发生完全的静态再结晶.在变形程度较小、道次间隔时间较短时,几乎不发生静态再结晶.将静态再结晶动力学模型的预测结果与实验结果进行比较,二者较吻合.     

Cu-Ni-Si-Cr合金动态再结晶行为及组织演变研究

利用Gleeble 1500D热模拟试验机,研究了Cu Ni Si Cr合金在不同应变速率和不同变形温度下流变应力与应变速率、变形温度之间的关系及其组织在热压缩过程中的变化.结果表明,应变速率和变形温度的变化对合金的再结晶影响较大,变形温度越高,合金越容易发生动态再结晶,应变速率越小,合金也越容易发生动态再结晶;在同一应变速率下合金动态再结晶的显微组织受到变形温度的强烈影响;并利用Arrhenius双曲正弦函数求得Cu Ni Si Cr热变形激活能Q为265.9 kJ/mol.     

一种桥梁用耐候钢的静态再结晶模型

在MMS-300热/力模拟实验机上采用双道次压缩法,研究了桥梁用耐候钢在奥氏体区变形后道次间隔时间内的静态软化行为.分析了变形温度与间隔时间对静态软化行为的影响,采用应力补偿法计算了静态再结晶百分数.实验结果表明,在第一道次变形之后的5~10 s就发生了静态再结晶,变形温度、道次间隔时间对耐候钢的静态再结晶行为影响显著,变形温度越高,静态再结晶进行得越迅速.确定了耐候钢的静态再结晶激活能为190.57 kJ/mol,同时建立了静态再结晶动力学数学模型.     

Static Recrystallization Behavior of SCM435 Steel

The static recrystallization behaviors in SCM435 steel were investigated by two-pass hot compression tests on MMS-200 thermosimulation machine. Effects of deformation temperature, strain rate,deformation degree and the initial austenite grain size on static softening were analyzed. The stress compensation method was used to calculate the static recrystallization. The kinetics model of the static recrystallization of SCM435 steel was established and the obtained activation energy for static recrystallization was 182. 8 kJ /mol. Results showed that within a certain time interval( 1-100 s),the static recrystallization fraction X of SCM435 steel increased as the deformation temperature,the deformation rate and the amount of deformation increased,and it decreased as the initial grain size increased and increased as the time interval increased.     

Microstructural evolution of a superaustenitic stainless steel during a two-step deformation process

Single- and two-step hot compression experiments were carried out on 16Cr25Ni6Mo superaustenitic stainless steel in the temperature range from 950 to 1150℃ and at a strain rate of 0.1 s-1. In the two-step tests, the first pass was interrupted at a strain of 0.2; after an interpass time of 5, 20, 40, 60, or 80 s, the test was resumed. The progress of dynamic recrystallization at the interruption strain was less than 10%. The static softening in the interpass period increased with increasing deformation temperature and increasing interpass time. The static recrystallization was found to be responsible for fast static softening in the temperature range from 950 to 1050℃. However, the gentle static softening at 1100 and 1150℃ was attributed to the combination of static and metadynamic recrystallizations. The correlation between calculated fractional softening and microstructural observations showed that approximately 30% of interpass softening could be attributed to the static recovery. The microstructural observations illustrated the formation of fine recrystallized grains at the grain boundaries at longer interpass time. The Avrami kinetics equation was used to establish a relationship between the fractional softening and the interpass period. The activation energy for static softening was determined as 276 kJ/mol.     

TA2钛合金绝热剪切带起始实验研究

本文利用分离式霍普金森压杆加载TA2钛合金扁平帽型试样,结合高速红外测温与金相观察,分析动态加载下帽型试样受迫剪切的力学响应以及绝热剪切带温度演化,并讨论绝热剪切失稳起始条件.结果显示,TA2钛合金绝热剪切带起始时的温度约为470 K.在该温度下,材料热软化不足以引起本构软化,因此热软化可能不是绝热剪切起始必要条件,相反可能是由于剪切局域化带产生导致带内温度的急剧上升.以温度达到470 K时刻作为绝热剪切带起始条件,得到随加载率增大,帽型试样绝热剪切起始时的压缩位移随加载率增大呈下降趋势.     

等温热处理对挤压态镁锂合金组织、硬度及延伸率的影响

采用氩气氛下感应熔炼和正向挤压变形制备了Mg-7.5Li-3.5Al-1Zn-1Ce-0.5Sn镁锂合金板材,然后在真空热处理炉中对挤压态合金进行等温退火,并采用金相观察和布氏硬度测试研究了等温热处理对合金板材显微组织和布氏硬度的影响.通过金相显微镜观察表明,等温处理温度对合金显微组织的影响较大,在较低温度下,只发生两相的形态和体积分数的变化,合金几乎不发生或需要较长时间才发生静态再结晶.在较高温度下,合金快速发生再结晶,合金晶粒细化,但随着保温时间的延长,晶粒有所长大.不同的组织形态对应的硬度不同,α相呈球化时的硬度值最高.     

Mechanical behavior of a near α titanium alloy under dynamic compression: Characterization and modeling

Dynamic compression tests under strain rates from 870 s^?1 to 2100 s^?1 were conducted for a near α Ti–8Al–1Mo–1V titanium alloy with equiaxed microstructure. Compression behavior, adiabatic shearing and band microstructure were investigated via characterization and calculation. The results demonstrate that all dynamic constitutive curves exhibited obvious stress fluctuation phenomenon with double increase-decrease changing stages at the primary stage of compression. The dislocation multiplication theory can be used to explain this phenomenon. After the stress fluctuation period, work hardening coexisted with the thermal softening, resulting in the slow hardening tendency in constitutive curves. J-C model was utilized to quantify the dynamic constitutive curves. The deviations between the predicted and experimental curves under high strain rates may be attributed to the over-consideration of thermal softening effect in J-C model. Adiabatic shearing band (ASB) began to form under the strain rate of 2100 s^?1. A total shearing strain of 8.1 within ASB achieved in 8.9 μs, corresponding to a local strain rate of about 9.1 × 10⁵ s^?1 and is over 430 times of the macro strain rate. Post annealing was conducted on ASB before EBSD characterization. Due to the static recrystallization during annealing, the α phase within ASB generally presented as ultra-fine grains less than 1 μm in diameter.     

热变形奥氏体静态再结晶行为的研究

利用双道次压缩的方法，在Gleeble 1500热模拟实验机上研究了低碳钢SS400在变形间隔时间内奥氏体的软化行为，以便为制定合理的细化晶粒轧制工艺提供实验和理论基础．采用后插法计算了在不同真应变条件下的静态再结晶率，通过双道次压缩测试静态软化动力学的实验表明，实验钢变形后很容易发生静态软化．在真应变为0．4、0．2时，静态再结晶激活能分别是Qmc=189．3、170.2kJ／mol。