用柠檬酸溶胶凝胶法合成SrFeCo_(0.5)O_x氧化物

采用柠檬酸溶胶凝胶法合成SrFeCo0 5Ox混合导体氧化物·利用XRD、TEM以及DTA方法研究与分析了不同条件下样品的晶体结构组成、相貌·确定了最佳制备条件·结果说明在燃料剂/氧化剂比例为0 64,550℃时得到单相钙钛矿氧化物,氧化物为纳米球形颗粒,尺寸分布均匀;加热温度升高850℃晶体结构无变化,颗粒尺寸明显长大但是形状不变·同时分析了溶胶凝胶反应过程及影响因素·     

金属冲击加热的研究

金属冲击加热是对流快速加热的一种新型加热工艺,也是金属加热的一项节能新技术。它是用高温高速气流直接冲击金属表面的快速对流加热方法来完成金属锻前或轧前的加热,金属加热温度均匀、加热速度快、加热时间短,可以大大降低燃耗。本文由金属冲击加热数学模型,用计算机解出了获得最佳加热炉温和断面温差最小的加热时间时换热系数范围为:300～500KKal/m~2·h·℃     

半固态A356合金触变成形件固溶组织与性能

利用电阻炉加热,对半固态A356铝合金触变成形件进行固溶时效处理,并进行组织与性能的观察分析·结果表明:在535℃温度下固溶处理,随固溶时间的延长,强化相溶解充分,合金元素在晶格的分布均匀,强度得到了提高·在180℃温度下时效,强度随时效时间的延长而增大,并达到最大值;进一步延长时效时间,则合金出现软化·触变成形变形带的存在,起到了强化作用·本研究为A356合金液相线半连续铸造生产工业化提供理论指导·     

混合导体氧化物SrFeCo_(0.5)O_(3-x)的微波混合加热合成

采用微波混合加热方法(即微波加热+电阻加热)和常规加热方法合成了混合导体氧化物SrFeCo05O3-x粉末·利用XRD,SEM/EDX测试手段对两种方法合成粉末的物相结构,形貌及化学成分进行了分析·结果表明,微波混合加热与常规加热合成粉末的结晶相结构类型相同,但是结晶相比例存在差异·微波混合加热法得到的主相属于立方钙钛矿结构;常规加热法得到的主相属于正交结构·微波混合加热制备的粉末颗粒尺寸分布较均匀,结晶度较好·     

火焰加热温度对6005A铝合金焊接接头性能的影响

针对铁路交通车辆用 60 0 5A铝合金型材的焊接变形 ,采用火焰加热方法进行矫正·研究了火焰加热温度对焊接接头抗拉强度、硬度及微观组织结构的影响·实验结果表明 ,当加热温度低于 2 0 0℃时 ,焊接接头的抗拉强度、硬度未降低 ,热影响区内软化区的显微组织未发生明显变化 ;当加热温度超过 2 0 0℃时 ,焊接接头的硬度发生较明显降低现象 ,软化区范围加宽·软化区材料性能下降的原因是在火焰加热的热输入过程中过热导致该区晶粒粗大     

垃圾热解中PVC组分HCl的析出特性

以垃圾中的PVC组分为试验物料,在外热式固定床热解试验台上,研究了PVC热解过程中HCl的析出特性·通过改变加热方式、热解终温、加热温度、加热时间等参数研究了HCl的析出过程、析出量和质量分数·试验表明,加热方式对HCl析出有很大的影响,快加热方式析出的HCl量几乎是慢加热方式的2倍;HCl析出过程可分为三个阶段,325℃时开始有HCl析出;热解终温对HCl析出过程有较大的影响,并决定着HCl的析出量,本试验在550℃左右析出的HCl量最多,这说明存在一个HCl析出量最大的峰值温度·并依据试验结果,从理论上进行了初步探讨     

液相线半连续铸造7075铝合金半固态组织演变

研究了液相线半连续铸造法生产的7075铝合金半固态浆料二次加热时组织的演变和主要合金元素的分布·结果表明,液相线铸造7075铝合金在相同加热温度下,随着保温时间的延长,晶粒尺寸与球化倾向增大;在相同保温时间下,随着加热温度的升高,晶粒尺寸与球化倾向也增加·加热温度580℃左右,保温时间在15～30min之间,和加热温度600℃左右,保温时间在5～15min之间,可以将半连续铸造锭坯中的蔷薇状和近球状组织转化为球形晶粒,晶粒的平均直径范围为40～55μm,完全适合于半固态加工·液相线铸造7075铝合金二次加热组织中,主要合金元素M...     

A2017半固态合金二次加热组织演化

对SCR技术制备的A2017半固态坯料进行二次加热,利用光学显微镜,电镜,图像分析仪等手段,对坯料二次加热微观组织的演化进行了研究·实验结果表明,在相同加热温度条件下,随着保温时间的延长,晶粒平均等积圆直径增大,晶粒越来越圆整,液相率增加;提高二次加热温度,晶粒长大和球化速度加快·二次加热最佳工艺条件为加热温度580℃,保温时间40～60min或者加热温度600℃,保温20～40min,晶粒平均等积圆直径为70～90μm,固相率在70%左右,适合于半固态加工·组织演化机制分析表明,加热初期阶段,液相少,晶粒主要通过碰撞熔合快速长大;随着保温时间延长,液相增加,晶粒主要通过原子扩散慢速长大并发生...     

加热温度对高速钢铸轧薄带中共晶碳化物形态的影响

研究了退火加热温度对高速钢双辊铸轧薄带中共晶碳化物形态的影响·试验结果表明,随着加热温度的提高,铸轧薄带中的网状共晶碳化物陆续熔断,粒状碳化物逐渐增多·当加热温度达到950℃后,铸轧薄带中的网状共晶碳化物基本上被粒状碳化物所取代·用汤普森弗瑞锥其(ThompsonFriedrich)方程,对试验结果进行了分析,并得出共晶碳化物层片间距的减小为高速钢铸轧薄带中的共晶碳化物的熔断和球化提供了条件·     

7075Al合金LSC铸锭二次加热中的液固相体积分数

研究了液相线半连续铸造法制备的7075Al合金坯料在二次加热过程中液固相比的变化,分别用电阻法、热涵法测定出不同温度下7075Al合金的液相体积分数,并与图像法进行了比较·结果表明,在600℃左右,电阻法与用热涵法、图像法所测的实验结果基本一致,正确反映了加热过程中合金的液固相变化规律·用电阻法能方便有效地测定二次加热过程中半固态7075Al合金的液固相比,具有实时性强的优点,在600～620℃时,7075Al合金液固相比为30%～50%,完全适于合金的半固态成形·     

Markedness and its Interpretation in Language Use

Language markedness is a common phenomenon in languages, and is reflected from hearing, vision and sense, i.e. the variation in the three aspects such as phonology, morphology and semantics. This paper focuses on the interpretation of markedness in language use following the three perspectives, i.e. pragmatic interpretation, psychological interpretation and cognitive interpretation, with an aim to define the function of markedness.     

Features of Women's language

Language is a means of verbal communication. People use language to communicate with each other. In the society, no two speakers are exactly alike in the way of speaking. Some differences are due to age, gender, statue and personality. Above all, gender is one of the obvious reasons. The writer of this paper tries to describe the features of women＇s language from these perspectives： pronunciation, intonation, diction, subjects, grammar and discourse. From the discussion of the features of women＇s language, more attention should be paid to language use in social context. What＇s more, the linguistic phenomena in a speaking community can be understood more thoroughly.     

An Analysis of Catherine＇s Character——Wuthering Heights

Wuthering Heights, Emily Bronte＇s only novel, was published in December of 1847 under the pseudonym Ellis Bell. The book did not gain immediate success, but it is now thought one of the finest novels in the English language. Catherine is the key character of this masterpiece, because everybody and everything center on her though she had a short life. We can understand this masterpiece better if we know Catherine well.     

Lower Paleozoic oil relationships within Williston Basin, Canada

The Williston Basin is a significant petroleum province, containing oil production zones that include the Middle Cambrian to Lower Ordovician, Upper Ordovician, Middle Devonian, Upper Devonian and Mississippian and within the Jurassic and Cretaceous. The oils of the Williston Basin exhibit a wide range of geochemical characteristics defined as "oil families", although the geochemical signature of the Cambrian Deadwood Formation and Lower Ordovician Winnipeg reservoired oils does not match any "oil family". Despite their close stratigraphic proximity, it is evident that the oils of the Lower Palaeozoic within the Williston Basin are distinct. This suggests the presence of a new "oil family" within the Williston Basin. Diagnostic geochemical signatures occur in the gasoline range chromatograms, within saturate fraction gas chromatograms and biomarker fingerprints. However, some of the established criteria and cross-plots that are currently used to segregate oils into distinct genetic families within the basin do not always meet with success, particularly when applied to the Lower Palaeozoic oils of the Deadwood and Winnipeg Formation.     

低渗透非均质砂岩油藏启动压力梯度研究

理论推导与室内实验相结合,建立了低渗透非均质砂岩油藏启动压力梯度确定方法。首先借助油藏流场与电场相似的原理,推导了非均质砂岩油藏启动压力梯度计算公式。其次基于稳定流实验方法,建立了非均质砂岩油藏启动压力梯度测试方法。结果表明:低渗透非均质砂岩油藏的启动压力梯度确定遵循两个等效原则。平面非均质油藏的启动压力梯度等于各级渗透率段的启动压力梯度关于长度的加权平均;纵向非均质油藏的启动压力梯度等于各渗透率层的启动压力梯度关于渗透率与渗流面积乘积的加权平均。研究成果可用于有效指导低渗透非均质砂岩油藏的合理井距确定,促进该类油藏的高效开发。     

On Tragic Consciousness In The Works By Ernest Hemingway

As an American modern novelist who were famous in the literary world, Hemingway was not a person who always followed the trend but a sharp observer. At the same time, he was a tragedy maestro, he paid great attention on existence, fate and end-result. The dramatis personae's tragedy of his works was an extreme limit by all means tragedy on the meaning of fearless challenge that failed. The beauty of tragedy was not produced on the destruction of life, but now this kind of value was in the impact activity. They performed for the reader about the tragedy on challenging for the limit and the death.     

Achieving Unusual States of Matter Under High Pressure

正The periodicity of the elements and the non-reactivity of the inner-shell electrons are two related principles of chemistry,rooted in the atomic shell structure.Within compounds,Group I elements,for example,invariably assume the+1 oxidation state,and their chemical properties differ completely from those of the p-block elements.These general rules govern our understanding of chemical structures and reactions.Using first principles calcula-     

Exchange-Correlation and Electronic Excitation Energies from Pairing Matrix Fluctuations

We have developed an adiabatic connection to formulate the ground-state exchange-correlation energy in terms of pairing matrix linear fluctuations.This formulation of the exchange-correlation energy opens a new channel for density functional approximations based on the many-body perturbation theory.We illustrate the potential of such approaches with an approximation based on the particle-particle Random Phase Approximation(pp-RPA).This re-     

Density Functional Theory for the Response of Periodic Systems to Electric Fields Based on the Vector Potential Approach

正The electronic and nuclear(structural/vibrational)response of 1D-3D nanoscale systems to electric fields gives rise to a host of optical,mechanical,spectral,etc.properties that are of high theoretical and applied interest.Due to the computational difficulty of treating such large systems it is convenient to model them as infinite and periodic(at least,in first approximation).The fundamental theoretical/computational problem in doing so is that     

Call for Papers

<正>"The Journal of Shanghai Normal University:Mathematics"is published by Shanghai Normal University as regular issues of The Journal of Shanghai Normal University each year from 2014 in English.The editors-in-chief of the issues are professors Yuhao Cong and Maoan Han.The Journal of Shanghai Normal University was started in 1958 with