Preparation of ultrafine silicon dioxide by high-gravity technical and its influential factors
HE Qing-yu ;GUO Kai; ZHAO ;Bing-guo ;LENG Ji-bin
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Research Center of the Ministry of Education for High Gravity Engineering and Technology, Beijing University of Chemical Technology, Beijing 100029, China
Ultrafine silica powder was prepared in a rotating packed bed (RPB) reactor using water glass and sulfuric acid as raw materials. The effects of experimental conditions such as pH of reaction, time of ripening, and rotating speed of RPB on the preparation of ultrafine SiO2 particles were investigated. The results revealed that the high gravity environment reduced reaction time enormously and favored the synthesis of ultrafine silica with a welldistributed particle size and a high specific surface area. The suitable conditions for the preparation are pH of the reaction end of 2~3, ripening time of 60~90min, rotating speed of RPB of 800~1000r/min.
HE Qing-yu ;GUO Kai; ZHAO ;Bing-guo ;LENG Ji-bin.
Preparation of ultrafine silicon dioxide by high-gravity technical and its influential factors[J]. Journal of Beijing University of Chemical Technology, 2006, 33(1): 16-19
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