| 查尔酮衍生物水凝胶模板合成CdS纳米带 |
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| 引用本文： | 谭昌会.查尔酮衍生物水凝胶模板合成CdS纳米带[J].漳州师院学报,2009(4):53-57. |
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| 作者姓名： | 谭昌会 |
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| 作者单位： | 漳州师范学院化学与环境科学系,福建漳州363000 |
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| 基金项目： | 福建省科技厅青年人才项目（2006F3129） |
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| 摘 要： | 本文设计并合成了一个新的含有查尔酮基团的小分子有机凝胶剂,通过熔点,红外光谱,核磁共振波谱等对凝胶剂进行了表征;并以凝胶剂在乙醇水溶液中形成的水凝胶为模板,硫代乙酰胺为硫源,在水凝胶体系中利用离子的原位自组装合成宽度为300-600nm,长度数微米的CdS纳米带,用透射电镜TEM和X射线衍射对CdS的微观结构进行表征,并讨论了初步的形成机理.
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| 关 键 词： | 水凝胶 查尔酮衍生物 CdS纳米带 |
Preparation and Characterization of CdS Nanoribbons Templated by Hydrogel Based on Chalcone Derivatives |
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| TAN Chang-hui.Preparation and Characterization of CdS Nanoribbons Templated by Hydrogel Based on Chalcone Derivatives[J].Journal of ZhangZhou Teachers College(Philosophy & Social Sciences),2009(4):53-57. |
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| Authors: | TAN Chang-hui |
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| Institution: | TAN Chang-hui (Department of Chemistry and Enviromental Science, Zhangzhou Normal University, Zhangzhou, Fujian 363000,China) |
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| Abstract: | This paper presents novel organogelators based on chalcone derivatives consisting of amide moieties.They are measured by melting point（m.p.）,FT-IR spectroscopy,H nuclear magnetic resonance（1HNMR） 1 spectra.Preparation of CdS nanoribbons uses the gel fibers as template in the ethanol-water under mild condition.The resulting samples show a nanoribbon structure with diameter of 300-600 nm and lengths of 1-10μm.These CdS microstructures are examined by transmission electron microscopy （TEM）, X-ray powder diffraction （XRD）. The formation process ofCdS nanoribbons is also discussed. |
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| Keywords: | hydrogel chalcone derivatives CdS nanoribbons |
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