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心脉通滴丸中葛根素含量的HPLC法测定
引用本文:彭咏梅,何咏梅.心脉通滴丸中葛根素含量的HPLC法测定[J].吉首大学学报(自然科学版),2006,27(3):117-118.
作者姓名:彭咏梅  何咏梅
作者单位:(1.湖南湘泉制药有限公司,湖南 吉首 416000;2.北京燕化凤凰医院药剂科,北京 102500)
摘    要:使用高效液相色谱法测定心脉通滴丸中葛根素的含量,结果表明:在4.16~83.2 mg/L范围内,进样浓度与峰面积值有良好的线性关系,y=3 814.6x-12.716,R2=0.999 9;平均回收率为100.84%,RSD为1.06%.该法准确,重现性好,效率高,操作简便.

关 键 词:心脉通滴丸  葛根素  高效液相色谱法
文章编号:1007-2985(2006)03-0117-02
收稿时间:2006-03-07
修稿时间:2006年3月7日

Determination of Puerarin in Xingmaitong Drop Pills by HPLC
PENG Yong-mei,HE Yong-mei.Determination of Puerarin in Xingmaitong Drop Pills by HPLC[J].Journal of Jishou University(Natural Science Edition),2006,27(3):117-118.
Authors:PENG Yong-mei  HE Yong-mei
Institution:(1.Hunan Xiangquan Pharmaceutical Ltd.,Jishou 416000,Hunan China;2.Medicament Office of Bejing Yanhua Fenghuang Hospital,Bejing 102500,China)
Abstract:Objective To establish a method for determination of Puerarin in xingmaitong.Method HPLC was used,the separation was performed on Luna  C18 (5 μg,250 mm×4.6 mm)  column,a  mixture of  methanol-water(25∶75) was servered  as the mobile phase,and the  detecting wavelength was at 2 250 nm.Results The linearity range was from 4.16~83.2 mg/L,and the mean recovery was 100.84%,RSD 1.06%.Conclusion The method is simple,accurate and good for the determination of Puerarin in Xingmaitong,and it can be used for quality control for Xingmaitong.
Keywords:Xingmaitong drop pills  puerarin  HPLC
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