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ICP-AES基体匹配法测定高导电铜中的微量元素
引用本文:刘邦夫.ICP-AES基体匹配法测定高导电铜中的微量元素[J].吉首大学学报(自然科学版),2018,39(4):74.
作者姓名:刘邦夫
作者单位:(湖南省电子信息产业研究院,湖南 长沙 410128)
摘    要:用ICP-AES基体匹配法测定了高导电铜中Ni,Be,Mg,Co和Si等微量元素含量,同时对所测元素相对不确定度进行了考察.发现以质量比计,元素Ni,Mg,Be,Co,Si的含量分别为2.13,0.088,0,0,0.22 mg/kg;相对不确定度主要由测量精密度和回收率2个因素决定.

关 键 词:ICP-AES法  高导电铜  基体匹配  不确定度  

Determination of Trace Elements in High ConductivityCopper by Matrix Matching of ICP-AES
LIU Bangfu.Determination of Trace Elements in High ConductivityCopper by Matrix Matching of ICP-AES[J].Journal of Jishou University(Natural Science Edition),2018,39(4):74.
Authors:LIU Bangfu
Institution:(Hunan Electronic Information Industry Institute,Changsha 410128,China)
Abstract:The ICP-AES matrix matching method has been applied to determine the trace elements Ni,Be,Co,and Si in high conductivity copper,and the uncertainty of those elements has been analyzed.The results showed that the mass ratios of those elements were:Ni 2.13 mg/kg,Mg 0.088 mg/kg,Be 0 mg/kg,Co 0 mg/kg,Si 0.22 mg/kg and the main factors which determine the uncertainty were the measurement repeatability and recovery rate.
Keywords:ICP-AES                                                                                                                        high conductivity copper                                                                                                                        matrix matching                                                                                                                        uncertainty
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