| 1-(5-甲基异(口恶)唑-3-甲酰基)-4-芳酰基氨基硫脲的合成 |
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| 引用本文： | 杨素君,冯小明,但建明,肖开恩.1-(5-甲基异(口恶)唑-3-甲酰基)-4-芳酰基氨基硫脲的合成[J].西南师范大学学报(自然科学版),1993(2). |
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| 作者姓名： | 杨素君 冯小明 但建明 肖开恩 |
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| 作者单位： | 西南师范大学化学系 重庆630715
(杨素君,冯小明,但建明),西南师范大学化学系 重庆630715(肖开恩) |
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| 摘 要： | 通过5-甲基异(口恶)唑-3-甲酰肼Ⅰ与取代苯甲酰异硫氰酸酯在乙腈溶剂中发生亲核加成反应,制得了9个新的1-(5-甲基异(口恶)唑-3-甲酰基)-4-芳酰基氨基硫脲Ⅱ.Ⅱ经元素分析,IR,~1H-NMR和MS分析确定其结构.
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| 关 键 词： | 5-甲基异(口恶)唑 酰基氨硫脲 合成法 |
SYNTHESIS OF 1-(5-METHYLISOXAZOL-3-YLCARBONYL) -4-AROYLTHIOSEMICARBAZIDES |
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| Yang Shujun Feng Xiaoming Dan Jianming Xiao Kaien.SYNTHESIS OF 1-(5-METHYLISOXAZOL-3-YLCARBONYL) -4-AROYLTHIOSEMICARBAZIDES[J].Journal of Southwest China Normal University(Natural Science),1993(2). |
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| Authors: | Yang Shujun Feng Xiaoming Dan Jianming Xiao Kaien |
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| Abstract: | A series of new l-( 5- methylisoxazol- 3- ylcarbonyl )- 4- aroyl thiosemicarbazides I were synthesized by condensation of aroylisothiocyanates with 5-methylisoxazoles-3-methylhydrazine I "in anhydrous acetonitrile. The structures of the compound I series were characterized by the elemental analyses, IR,'H-NMR and MS. |
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| Keywords: | 5-methylisoxazol acylthiosemlcarbazides synthesis methods |
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