| 微波辅助下5-碘尿嘧啶衍生物的绿色合成 |
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| 引用本文： | 渠桂荣,张志广,夏然,耿明伟.微波辅助下5-碘尿嘧啶衍生物的绿色合成[J].河南师范大学学报(自然科学版),2007,35(2):101-103. |
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| 作者姓名： | 渠桂荣 张志广 夏然 耿明伟 |
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| 作者单位： | 河南师范大学,化学与环境科学学院,河南,新乡,453007 |
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| 摘 要： | 在微波辐射下,尿嘧啶衍生物与ICl在水溶液中快速发生碘化发应,在6 min内以75%~90%的产率得到了6个5-碘嘧啶衍生物.产物结构经1H-NMR和13C-NMR确证.
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| 关 键 词： | 微波 尿嘧啶 碘化 |
| 文章编号： | 1000-2367(2007)02-0101-03 |
| 修稿时间： | 2006-10-19 |
Microwave-assisted Green Synthesis of 5-iodo Uracil Derivatives |
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| QU Gui-rong,ZHANG Zhi-guang,XIA Ran,GENG Ming-wei.Microwave-assisted Green Synthesis of 5-iodo Uracil Derivatives[J].Journal of Henan Normal University(Natural Science),2007,35(2):101-103. |
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| Authors: | QU Gui-rong ZHANG Zhi-guang XIA Ran GENG Ming-wei |
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| Institution: | College of Chemistry and Environmental Science, Henan Normal University, Xinxiang 453007, China |
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| Abstract: | With microwave irradiation,the facile and green iodination of uracil derivatives with ICl in water is described.The desired 5-iodo uracil derivatives(2a～2f) were obtained within 6 minutes in 75%～90% yield.Their structures were confirmed by 1H-NMR and 13C-NMR. |
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| Keywords: | microwave irradiation uracil iodination |
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