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Ag3PO4/ZnO复合物的制备及其降解甲基橙的研究
引用本文:郭玉玮,刘文芳,丁永萍.Ag3PO4/ZnO复合物的制备及其降解甲基橙的研究[J].四川大学学报(自然科学版),2016,53(6):1329-1334.
作者姓名:郭玉玮  刘文芳  丁永萍
作者单位:包头师范学院
基金项目:高等学校博士学科点专项科研基金,其它
摘    要:采用银氨辅助法合成了Ag_3PO_4,超声波分散法制备Ag_3PO_4/ZnO复合物,利用X-射线衍射(XRD)和扫描电镜(SEM)对催化剂进行了表征.在超声照射下,讨论了煅烧温度、煅烧时间、照射时间和染料浓度等对甲基橙降解率的影响.结果表明:Ag_3PO_4/ZnO在煅烧温度为450°C,煅烧时间为60min,超声照射180min时,甲基橙降解率可达85.36%,高于纯ZnO时的降解率.

关 键 词:磷酸银  氧化锌  声催化  降解率  甲基橙
收稿时间:2016/1/17 0:00:00
修稿时间:3/6/2016 12:00:00 AM

Preparation of Ag3PO4/ZnO and Investigation on Degradation of Methyl orange
GUO Yu-Wei,LIU Wen-Fang and DING Yong-Ping.Preparation of Ag3PO4/ZnO and Investigation on Degradation of Methyl orange[J].Journal of Sichuan University (Natural Science Edition),2016,53(6):1329-1334.
Authors:GUO Yu-Wei  LIU Wen-Fang and DING Yong-Ping
Institution:Department of Chemistry, Baotou Normal College,Department of Chemistry, Baotou Normal College and Department of Chemistry, Baotou Normal College
Abstract:Ag3PO4 was synthesized by silver ammonia auxiliary method, and Ag3PO4/ZnO was mixed by ultrasonic dispersion, Ag3PO4 and Ag3PO4/ZnO were characterized by XRD and SEM. The influence of preparation conditions, such as irradiation time, heat-treated temperature, heat-treated time and the concentration of methyl orange on the degradation efficiency were investigated under ultrasound irradiation. The results revealed that the degradation ratio of methyl orange dye in the presence of Ag3PO4/ZnO reached 85.36 % at the 450 °C, 60 min and 180 min, which was obviously higher than the corresponding degradation ratio in the presence of un-doped nanometer ZnO.
Keywords:Ag3PO4  ZnO  Sonocatalytic  Degradation ratio  Methyl orange
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