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气相色谱法测定宠物饲料中丙三醇、丙二醇、二甘醇研究
引用本文:肖林霞,李宏伟,于红光,张鹏,张宁,俞挺.气相色谱法测定宠物饲料中丙三醇、丙二醇、二甘醇研究[J].成都大学学报(自然科学版),2013,32(2):128-130.
作者姓名:肖林霞  李宏伟  于红光  张鹏  张宁  俞挺
作者单位:青岛捷安信检验技术服务有限公司,山东青岛,266071;山东出入境检验检疫局,山东青岛,266002
摘    要:用气相色谱仪氢火焰离子化检测器(GC-FID)对宠物饲料中的添加剂丙三醇、丙二醇、二甘醇的检测方法进行了研究,考查了提取试剂、提取方法、提取时间等因素对检测结果的影响,建立了宠物食品中添加剂丙三醇、丙二醇、二甘醇的检测方法,方法的检出限分别为0.05、0.01、0.02g/kg.实验结果表明,本检测方法具有简便、快速、准确、成本低的特点.

关 键 词:气相色谱仪  宠物饲料  丙三醇  丙二醇  二甘醇

Determination of Glycerin,Propylene Glycol and Diethylene Glycol in Pet Food by Gas Chromatography
XIAO Linxia , LI Hongwei , YU Hongguang , ZHANG Peng , ZHANG Ning , YU Ting.Determination of Glycerin,Propylene Glycol and Diethylene Glycol in Pet Food by Gas Chromatography[J].Journal of Chengdu University (Natural Science),2013,32(2):128-130.
Authors:XIAO Linxia  LI Hongwei  YU Hongguang  ZHANG Peng  ZHANG Ning  YU Ting
Institution:1.J & C Testing Services Co.,Ltd.,Qingdao 266071,China;2.Shandong Entry-Exit Inspection and Quarantine Bureau,Qingdao 266002,China)
Abstract:The detection methods for glycerin, propylene glycol and diethylene glycol in pet food by gas chromatography-flame ionization detection(GC-FID) were studied in this paper. We examined the effects of extraction reagent, extraction method and extraction time on test results. The detection method for glycerin, propylene glycol and diethylene glycol was established. The detection limit was 0.05,0.01 and 0.02 g/kg separately. The experimental results show that this method is convenient, rapid, accurate and economical.
Keywords:gas chromatography  pet food  glycerin  propylene glycol  diethylene glycol
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