| 二硫基二苯并噻唑的微波合成 |
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| 引用本文： | 陈先良,王欣,陶金秋,高贺龙.二硫基二苯并噻唑的微波合成[J].科技信息,2009(11). |
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| 作者姓名： | 陈先良 王欣 陶金秋 高贺龙 |
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| 作者单位： | 安徽医科大学基础医学院化学教研室;安徽医科大学第一临床学院;安徽医科大学卫生事业管理学院; |
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| 摘 要： | 2-巯基苯并噻唑(M)溶解于少量丙酮中,加入过氧化氢,在微波促进下进行反应,高产率获得二硫基二苯并噻唑(DM)。
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| 关 键 词： | 2-巯基苯并噻唑 丙酮 微波 二硫基二苯并噻唑 |
Rapid Synthesis of DM Under Microwave Irradiation |
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| CHEN Xian-liang WANG Xin TAO Jin-qiu GAO He-long.Rapid Synthesis of DM Under Microwave Irradiation[J].Science,2009(11). |
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| Authors: | CHEN Xian-liang WANG Xin TAO Jin-qiu GAO He-long |
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| Institution: | 1.Department of Chemistry;College of Basic Medicine;Anhui Medical University;Hefei;230032;2.The First Clinical College;3.School of Health Service Management;230032 |
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| Abstract: | M was used to be resolved in acetone, and hydrogen peroxide is added to the system. After this, the system was placed in Microwave Irradiation Reactor and irradiated for 90 seconds and DM was gained in high yield. |
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| Keywords: | M Acetone DM Microwave irradiation |
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