| AMP-95/DMF混合溶剂热条件下镍微纳米链构筑的形成 |
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| 引用本文： | 陈彬,马德荣,胡正水.AMP-95/DMF混合溶剂热条件下镍微纳米链构筑的形成[J].青岛化工学院学报(自然科学版),2014(4):355-359. |
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| 作者姓名： | 陈彬 马德荣 胡正水 |
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| 作者单位： | 青岛科技大学材料科学与工程学院,山东青岛266042 |
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| 摘 要： | ：以NiCl26H2O为镍源,2氨基2甲基1丙醇（AMP-95）和N,N二甲基甲酰胺（DMF）的混合溶剂热条件下,AMP 95和DMF共同作用,把镍离子还原成单质镍,制备了不同形貌的微纳米镍.结果表明,AMP-95和DMF不仅对产物的类型有影响,而且能够促使镍粒子成链状.在AMP-95/DMF的混合溶剂中,可形成镍的珠链结构,且该微纳米珠链结构具有超顺磁性.
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| 关 键 词： | 微纳米镍 AMP-95 溶剂热 |
Build of Chain-like Micro-Nano Nickel by Solvothermal Method in Mixed Solvent of AMP-95 and DMF |
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| CHEN Bin,MA De-rong,HU Zheng-shui.Build of Chain-like Micro-Nano Nickel by Solvothermal Method in Mixed Solvent of AMP-95 and DMF[J].Journal of Qingdao Institute of Chemical Technology(Natural Science Edition),2014(4):355-359. |
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| Authors: | CHEN Bin MA De-rong HU Zheng-shui |
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| Institution: | (College of Materials Science and Engineering, Qingdao University of Science and Technology, Qingdao 266042, China) |
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| Abstract: | Micro-nano nickel of different morphology are synthesized by solvothermal method with NiCl2 6H2O as nickel source, the mixture of AMP-95 and DMF as solvent than the both restore Ni2＋ to Ni. The result shows that AMP-95 and DMF affect not only product but also make particles become chain. The particles can form chain-like structure in the mixture of AMP-95 and DMF. The products exhibit superparamagnetic by SQUID. |
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| Keywords: | micro-nano nickel AMP-95 solvothermal method |
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