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| 滇桂艾纳香茎和叶中挥发性化学成分的HS-SPME-GC-MS 分析 | |
| 引用本文： | 马芝玉,林翠梧,黄克建,潘智文,蒋双双.滇桂艾纳香茎和叶中挥发性化学成分的HS-SPME-GC-MS 分析[J].中山大学学报(自然科学版),2009,48(1). |
| 作者姓名： | 马芝玉 林翠梧 黄克建 潘智文 蒋双双 |
| 作者单位： | 1. 广西大学化学化工学院,广西,南宁,530004 2. 广西壮族自治区公安厅物证鉴定中心,广西,南宁,530012 3. 柳州市产品质量监督检验所,广西,柳州,545001 |
| 基金项目： | 国家自然科学基金，广西科技攻关项目，教育部大学生创新实验资助项目 |
| 摘 要： | 采用固相微萃取法提取中草药滇桂艾纳香茎和叶中挥发性成分，经气相色谱/质谱测定其化学成分和相对含量，共鉴定了98种化学成分，茎和叶中各82种。主要挥发成分及含量为：大叶香烯 D（茎：36.59%；叶：40.87%）、香木兰烯（茎：13.20%；叶：17.00%）、顺 α 没药烯（茎：6.06%；叶：7.48%）、β 荜澄茄油烯（茎：4.83%；叶：5.85%）、γ 依兰油烯（茎：2.18%；叶：2.58%）和1,2,4a,5,6,8a-六氢-4,7-二甲基-1-（1-甲乙基）-萘（茎：2.03%；叶：2.55%），它们都为倍半萜类化合物。本实验中发现滇桂艾纳香茎和叶的中倍半萜类化合物含量分别占挥发性成分含量的91.75%和94.52%。 |
| 关 键 词： | 滇桂艾纳香 挥发油 顶空固相微萃取 气相色谱/质谱 |
| 收稿时间： | 2008-05-18; |
Analysis of Volatile Components from the Fresh stems and Leaves of Blumea riparia(Bl.)DC.by Headspace Solid Phase Microextraction-Gas Chromatography-Mass Spectrometry |
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| MA Zhiyu,LIN Cuiwu,HUANG Kejian,PAN Zhiwen,JIANG Shuangshuang.Analysis of Volatile Components from the Fresh stems and Leaves of Blumea riparia(Bl.)DC.by Headspace Solid Phase Microextraction-Gas Chromatography-Mass Spectrometry[J].Acta Scientiarum Naturalium Universitatis Sunyatseni,2009,48(1). | |
| Authors: | MA Zhiyu LIN Cuiwu HUANG Kejian PAN Zhiwen JIANG Shuangshuang |
| Institution: | (1.School of Chemistry and Chemical Engineering，Guangxi University，Nanning 530004，China;2.Institute of Forensic Science，Public Security of Guangxi Province，Nanning 530012，China;3.Liuzhou Product Quality Supervision Testing Institute, Liuzhou 545001,China) |
| Abstract: | Volatile components from the fresh stems and leaves of Blumea riparia（Bl)DC.were analyzed by headspace solid phase microextraction gas chromatography mass spectrometry.The volatile constituents were separated and identified by gas chromatography mass spectrometry（GC/MS)．The result showed that 98 kinds of compounds were identified from the volatile constituents（82 from stems and 82 from leaves）．The principal components and relative contents were germacrene D（stem3659%，leaf40.87%)，aromadendrene（stem13.20%，leaf17.00%)，cis .α bisabolene（stem6.06%，leaf:7.48%)，β-cubebene，(stem4.83%，leaf5.85%)，γ-muurolene（stem:2.18%,leaf:2.58%）and 1,2,4a,5,6,8a-hexahydro-4,7-dimethyl-1-(1-methylethyl)-naphthalene（stem2.03%，leaf2.55%)，which were terpene.Sesquiterpenes were the dominant components which relative contents were 91.75% for stems and 94.52% for leaves respectively. |
| Keywords: | Blumea riparia（Bl)DC volatile component headspace solid phase microextraction gas chromatography mass spectrometry |
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