| 微波消解/等离子发射光谱法测定中成药紫雪散中的微量元素 |
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| 引用本文： | 陈明玉.微波消解/等离子发射光谱法测定中成药紫雪散中的微量元素[J].曲阜师范大学学报,2006,32(1):84-86. |
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| 作者姓名： | 陈明玉 |
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| 作者单位： | 曲阜师范大学校医院,山东省曲阜市273165 |
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| 摘 要： | 采用HNO3-H2O2消解体系对中成药紫雪散样品进行微波消解制样，利用ICP-AES法同时测定了样品中14种微量元素的含量，并对样品的前处理条件进行了探讨，通过添加标准回收实验，验证了分析数据的可靠性．结果表明，该方法快速、简便、数据准确可靠，结果令人满意，适合常规分析。
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| 关 键 词： | 紫雪散 微量元素 微波消解 |
| 文章编号： | 1001-5337（2006）01-0084-03 |
| 收稿时间： | 2005-03-20 |
| 修稿时间： | 2005-03-20 |
Determination of Trace Elements in Zixuesan by Microwave Digestion and ICP-AES |
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| CHEN Ming-yu.Determination of Trace Elements in Zixuesan by Microwave Digestion and ICP-AES[J].Journal of Qufu Normal University(Natural Science),2006,32(1):84-86. |
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| Authors: | CHEN Ming-yu |
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| Institution: | Hospital of Qufu Normal University, Z73165, Qufu, Shandong, PRC |
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| Abstract: | Zixuesan was digested with HNO_3-H_2O_2 system by microwave digestion.The fourteen trace elements of As,Ca,Mg,Al,Mn,Sr,Ba,Se,Ni,Cd,Cu,Zn,Mo and Pb in the solution were determined by ICP-AES.The ICP-AES result was proved to be reliable by adding standard recovery experiment to the process.Compared with the result of chemical experiment,this method was accurate,fast and convenient. |
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| Keywords: | ICP-AES |
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