| 氨基酸衍生物在胶束电动色谱下的分离研究 |
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| 引用本文： | 程燕,白敏,明永飞,石运伟,尤进茂.氨基酸衍生物在胶束电动色谱下的分离研究[J].曲阜师范大学学报,2005,31(4):77-80. |
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| 作者姓名： | 程燕 白敏 明永飞 石运伟 尤进茂 |
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| 作者单位： | [1]曲阜师范大学化学科学学院,山东省曲阜市273165 [2]兰州化学物理研究所,甘肃省兰州市730000 |
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| 基金项目： | 国家自然科学基金资助项目（20075016） |
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| 摘 要： | 采用新型荧光衍生试剂1,2-苯并-3,4-二氢咔唑-9-乙基氯甲酸酯（BCEOC）作为柱前衍生试剂,利用毛细管电泳在胶束电动模式下对氨基酸进行了分离,考察试剂用于氨基酸分离的几个关键条件,实现了14种氨基酸的快速基线分离.
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| 关 键 词： | 胶束电动色谱 氨基酸 衍生化 |
| 文章编号： | 1001-5337（2005）04-0077-04 |
| 收稿时间： | 2005-03-08 |
| 修稿时间： | 2005-03-08 |
Study on the Separation of Amino Acids by Micellar Electrokinetic Capillary Chromatography |
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| CHENG Yan, BAI Min, MING Yong-fei, SHI Yun-wei, YOU Jin-mao.Study on the Separation of Amino Acids by Micellar Electrokinetic Capillary Chromatography[J].Journal of Qufu Normal University(Natural Science),2005,31(4):77-80. |
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| Authors: | CHENG Yan BAI Min MING Yong-fei SHI Yun-wei YOU Jin-mao |
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| Institution: | College of Chemical Science, Qufu Normal University, 273165, Qufu, Shandong, PRC |
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| Abstract: | A new method for the separation of amino acids by micellar electrokinetic capillary chromatography using 1,2-benzo-3,4-dihydrocarbazole-9-ethyl chloroformate(BCEOC) as derivatization agent has been developed.The effect of several key factors on the separation was studied.Under the proposed conditions,a good baseline resolution for 14 amino acid derivatives was achieved. |
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| Keywords: | Micellar electrokinetic capillary chromatography amino acids derivatization |
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