| HPLC测定吴茱萸中吴茱萸碱的含量 |
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| 引用本文： | 王海宁,熊慧林,黄作苏.HPLC测定吴茱萸中吴茱萸碱的含量[J].贵州师范大学学报(自然科学版),2001,19(1):74-75,88. |
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| 作者姓名： | 王海宁 熊慧林 黄作苏 |
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| 作者单位： | 贵州省药品检验所, |
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| 摘 要： | 测定吴茱萸中吴茱萸碱的含量 ,采用高效液相色谱法。色谱柱Sphevisorb -Sio2 (2 5 0mm× 4 6mm )、粒度5 μm(大连依利特公司 ) ,流动相为正庚烷 -异丙醇 -已酸 (89∶10∶1) ,检测波长 2 5 4nm ,流速 1mL·min-1。平均回收率为 10 2 5 % ,RSD =3 14%。线性关系、精密度及重线性都很好。
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| 关 键 词： | 吴茱萸 含量测定 高效液相色谱 吴茱萸碱 |
| 文章编号： | 1004-5570(2001)01-0074-02 |
Determination of evodiamine in evodia rutacecarpa benty by HPLC |
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| WANG Hai lin ,XIONG Hui lin ,HUANG Zuo su.Determination of evodiamine in evodia rutacecarpa benty by HPLC[J].Journal of Guizhou Normal University(Natural Sciences),2001,19(1):74-75,88. |
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| Authors: | WANG Hai lin XIONG Hui lin HUANG Zuo su |
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| Institution: | WANG Hai lin 1,XIONG Hui lin 1,HUANG Zuo su 2 |
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| Abstract: | To determine the content of evodiamine in crude Evodia rutacecarpa Benth A HPLC method was set up.Using sphevisorb-sip 2 C 18 column(250mm×4.6mm,5 μm),n-heptane—iso-propylalconol—caproic acid (89∶10∶1) as mobile phase with a flow rate of 1.0mL·min -1 ,254nm as detection wavelength The average recovery was 102.5%,the RDS was 3.14%. It has good linearity ,precision and repetition |
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| Keywords: | evodia rutacecarpa benth content determination HPLC evodiamine |
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