| 黑骨藤药材薄层色谱检测方法研究 |
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| 引用本文： | 曹桂红,陈华国,赵超,周欣,甘秀海.黑骨藤药材薄层色谱检测方法研究[J].贵州师范大学学报(自然科学版),2009,27(4):98-101. |
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| 作者姓名： | 曹桂红 陈华国 赵超 周欣 甘秀海 |
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| 作者单位： | 贵州师范大学,天然药物质量控制研究中心,贵阳,550001;贵州师范大学,贵州省山地环境信息系统与生态环境保护重点实验室,贵阳,550001 |
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| 基金项目： | 贵州省中药现代化科技产业研究开发专项项目，贵州省科技计划项目 |
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| 摘 要： | 目的建立黑骨藤药材的薄层色谱鉴别方法。方法:黒骨藤经不同方法提取后,分别以:1)石油醚-三氯甲烷(1∶1.5);2)三氯甲烷-甲醇(25∶1)为展开剂,对黒骨藤中β-香树酯醇乙酸酯,β-香树酯醇,滇杠柳苷元A,27-羟基-α-香树酯醇进行薄层鉴别。结果:薄层色谱鉴别斑点清晰,能有效鉴别黒骨藤中β-香树酯醇乙酸酯,β-香树酯醇,27-羟基-α-香树酯醇,滇杠柳苷元A。
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| 关 键 词： | 黑骨藤 薄层色谱鉴别 β-香树酯醇乙酸酯 β-香树酯醇 27-羟基-α-香树酯醇 滇杠柳苷元A |
Experimental research on TLC identification of Periploca forrestii Schltr |
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| CAO Gui-hong,CHEN Hua-guo,ZHAO Chao,ZHOU Xin,GAN Xiu-hai.Experimental research on TLC identification of Periploca forrestii Schltr[J].Journal of Guizhou Normal University(Natural Sciences),2009,27(4):98-101. |
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| Authors: | CAO Gui-hong CHEN Hua-guo ZHAO Chao ZHOU Xin GAN Xiu-hai |
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| Abstract: | Objective:To establish a method of Thin Layer Chromatography(TLC) identification for Periploca forrestii Schltr.Methods:1.Petroleum ether-chloroform(1∶1.5);2.Chloroform-methyl alcohol(25∶1) as developing solvent and identification by TLC for β-amyrin acetate,β-amyrin,periplogenin A,27-hydroxy-α-amyrin in Periploca forrestii Schltr.Result: The spots of TLC distinction were fairly clear which could distinguish effectively β-amyrin acetate,β-amyrin,27-hydroxy-α-amyrin and periplogenin A in Periploca forrestii Schltr. |
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| Keywords: | Periploca forrestii Schltr TLC β-amyrin acetate β-amyrin 27-hydroxy-α-amyrin periplogeninA |
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