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Sm~(3+)掺杂氧化锌粉体的制备及光催化性能研究
引用本文:谢桂香,钟南,蔡小泉,王彬红.Sm~(3+)掺杂氧化锌粉体的制备及光催化性能研究[J].贵州师范大学学报(自然科学版),2014,32(5):111-115.
作者姓名:谢桂香  钟南  蔡小泉  王彬红
作者单位:龙岩学院化学与材料学院,福建龙岩,364012
基金项目:福建省大学生创新创业训练计划项目
摘    要:采用水热法制备扇形的钐掺杂的氧化锌粉体,通过XRD衍射仪、TG-DSC同步热分析仪、扫描电镜对所得粉体进行表征。研究了Sm3+的掺杂量,煅烧温度对其光催化降解甲基橙性能的影响。实验表明:当Sm3+掺杂的物质的量比为5.0%,煅烧温度为500℃时对甲基橙的降解率最高,300W紫外灯照射2h,降解率从未掺杂ZnO的77.83%提高到掺杂后的98.75%。

关 键 词:氧化锌  钐掺杂  甲基橙  光催化性能

Preparation of Sm3+/ZnO powders and its photocatalytic performance
XIE Guixiang,ZHONG Nan,CAI Xiaoquan,WANG Binhong.Preparation of Sm3+/ZnO powders and its photocatalytic performance[J].Journal of Guizhou Normal University(Natural Sciences),2014,32(5):111-115.
Authors:XIE Guixiang  ZHONG Nan  CAI Xiaoquan  WANG Binhong
Institution:XIE Guixiang;ZHONG Nan;CAI Xiaoquan;WANG Binhong;School of Chemistry and Materials,Longyan University;
Abstract:Sector-shaped Sm3+/ZnO Composite have been synthesized via hydrothermal method.The catalyst was characterized by X-ray diffraction,simultaneous thermal analyzer(TG-DSC),scanning electron microscopy.On the other hand,the calcination temperatures and different Sm3 + contents influenced the degradation of methyl orange(MO).When Sm3+/ZnO Composite calcine at 500℃ and content 5.0% (mol) Sm3+,the photodegradation of MO increased from 77.83% to 98.75% under 2h UV-light with 300W compared with bare ZnO.
Keywords:ZnO  Sm3+ doped  methyl orange  photodegradation
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