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| 高效液相色法同时测定丹参酮胶囊中隐丹参酮和丹参酮ⅡA含量 | |
| 引用本文： | 伍庆,卢俊,陈文生,赵杨,黄俊学,梁洁,胡蓉,邹晶.高效液相色法同时测定丹参酮胶囊中隐丹参酮和丹参酮ⅡA含量[J].贵州师范大学学报(自然科学版),2006,24(4):103-105. |
| 作者姓名： | 伍庆 卢俊 陈文生 赵杨 黄俊学 梁洁 胡蓉 邹晶 |
| 作者单位： | 1. 贵州师范大学分析测试中心,贵阳,550001;贵州省山地环境重点实验室,贵阳,550001 2. 贵阳生产力促进中心,贵阳,550002 3. 贵州师范大学分析测试中心,贵阳,550001 4. 贵阳中医学院,贵阳,550003 5. 贵州省山地环境重点实验室,贵阳,550001 |
| 摘 要： | 采用高效液相色谱法同时测定丹参酮胶囊中隐丹参酮和丹参酮ⅡA含量,建立丹参酮胶囊质量控制体系。采用C18柱分离测定;甲醇:水(80∶20)为流动相,检测波长:270nm;流速:1.0m l/m in。结果:隐丹参酮和丹参酮ⅡA分别在0.20~160μg(r>0.999 9)、0.21~1.68μg(r>0.999 8)质量范围内线性关系良好;回收率在98.7%~103.0%之间。 |
| 关 键 词： | 高效液相色谱法 丹参酮胶囊 隐丹参酮 丹参酮ⅡA |
| 文章编号： | 1004-5570（2006）04-0103-03 |
| 收稿时间： | 2006-05-20 |
| 修稿时间： | 2006年5月20日 |
HPLC determination of Cryptotanshinone and Tanshinone ⅡA in Danshentongiaonang |
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| WU Qing,LU Jun,CHEN Wen-sheng,ZHAO Yang,HUANG Jun-xue,LIANG Jie,HU Rong,ZOU Jing.HPLC determination of Cryptotanshinone and Tanshinone ⅡA in Danshentongiaonang[J].Journal of Guizhou Normal University(Natural Sciences),2006,24(4):103-105. | |
| Authors: | WU Qing LU Jun CHEN Wen-sheng ZHAO Yang HUANG Jun-xue LIANG Jie HU Rong ZOU Jing |
| Institution: | 1. Analysis and Testing Center, Guizhou Normal University, Guiyang, Guizhou 550001 China ;2. Guizhou Provincial Laboratory for Mountainous Environment, Guiyang, Guizhou 550001 China; 3. Guiyang Productivity Promotion Center, Guiyang, Guizhou 550002 China ;4. Guiyang College of Traditional Chinese Medicine, Guiyang, Guizhou 550001, China |
| Abstract: | To establish a method for determination of Cryptotanshinone and Tanshinone ⅡA in Danshentongiaonang by HPLC,the chromatographic method was carried out on C_(18) column using CH_3OH-H_2O(80∶20)as the mobile phase.The detection wavelength was 270nm and flow rate was 1.0 ml/min.Results:The linear ranges for Cryptotanshinone and Tanshinone ⅡA were 0.20～(1.60μg)(r>0.999 9)and 0.21～1.68μg(r>0.999 8)respectively.Conclusion:The method is simple,sensitive and rapid with satisfactory recoveries and reproducibilities. |
| Keywords: | HPLC Danshentongjiaonang Cryptotanshinone Tanshinone ⅡA |
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